data_1 _audit_creation_date 2023-03-29 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _shelx_SHELXL_version_number '2019/2' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C22 H19 Br S2' _chemical_formula_sum 'C22 H19 Br S2' _chemical_formula_weight 427.40 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.4017(2) _cell_length_b 5.92106(11) _cell_length_c 24.3917(4) _cell_angle_alpha 90 _cell_angle_beta 90.1424(14) _cell_angle_gamma 90 _cell_volume 1935.53(5) _cell_formula_units_Z 4 _cell_measurement_reflns_used 8131 _cell_measurement_temperature 149.99(10) _cell_measurement_theta_max 73.4510 _cell_measurement_theta_min 3.7850 _shelx_estimated_absorpt_T_max 0.867 _shelx_estimated_absorpt_T_min 0.591 _exptl_absorpt_coefficient_mu 4.904 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.61991 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.28b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.467 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 872 _exptl_crystal_size_max 0.12 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.03 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0221 _diffrn_reflns_av_unetI/netI 0.0204 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -4 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 11318 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 67.053 _diffrn_reflns_theta_max 67.053 _diffrn_reflns_theta_min 3.624 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 149.99(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -62.00 -22.00 0.50 0.50 -- -1.00 -20.00 114.00 80 2 \w -162.00-137.00 0.50 0.50 -- -100.10 -20.00 114.00 50 3 \w -87.00 -62.00 0.50 0.50 -- -100.10 20.00 -80.00 50 4 \w -85.00 14.00 0.50 0.50 -- 1.00 -72.00 -90.00 198 5 \w -8.00 17.00 0.50 0.50 -- 5.00 19.00 30.00 50 6 \w 25.00 50.00 0.50 0.50 -- 5.00 19.00 30.00 50 7 \w -122.00 -92.00 0.50 0.50 -- -100.10 -19.00 60.00 60 8 \w -100.00 -12.00 0.50 0.50 -- -100.10 38.00 150.00 176 9 \w -113.00 -88.00 0.50 0.50 -- -100.10 72.00 60.00 50 10 \w -109.00 -45.00 0.50 0.50 -- -100.10 72.00 90.00 128 11 \w -185.00 -87.00 0.50 0.50 -- -100.10 -19.00-180.00 196 12 \w -153.00-127.00 0.50 0.50 -- -100.10 -19.00 60.00 52 13 \w -86.00 -32.00 0.50 0.50 -- -100.10 57.00 60.00 108 14 \w 4.00 30.00 0.50 0.50 -- 1.00 72.00 30.00 52 15 \w -69.00 2.00 0.50 0.50 -- 1.00 -72.00-150.00 142 16 \w -112.00 -75.00 0.50 0.50 -- -100.10 72.00 -30.00 74 17 \w -123.00 -97.00 0.50 0.50 -- -100.10 -19.00 -60.00 52 18 \w -139.00-113.00 0.50 0.50 -- -100.10 -19.00-150.00 52 19 \w -186.00-160.00 0.50 0.50 -- -100.10 -19.00 -60.00 52 20 \w -150.00-124.00 0.50 0.50 -- -100.10 -19.00 -60.00 52 21 \w -62.00 -13.00 0.50 0.50 -- -100.10 72.00 -30.00 98 22 \w -188.00-162.00 0.50 0.50 -- -100.10 -19.00-150.00 52 23 \w -72.00 -12.00 0.50 0.50 -- -100.10 72.00-120.00 120 24 \w -60.00 -34.00 0.50 0.50 -- -100.10 38.00 0.00 52 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RCD3): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0380798000 _diffrn_orient_matrix_UB_12 0.0687187000 _diffrn_orient_matrix_UB_13 -0.0571506000 _diffrn_orient_matrix_UB_21 -0.1084533000 _diffrn_orient_matrix_UB_22 0.0196710000 _diffrn_orient_matrix_UB_23 -0.0205417000 _diffrn_orient_matrix_UB_31 -0.0018877000 _diffrn_orient_matrix_UB_32 0.2501936000 _diffrn_orient_matrix_UB_33 0.0173165000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3219 _reflns_number_total 3435 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.28b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.28b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.28b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _refine_diff_density_max 1.263 _refine_diff_density_min -0.864 _refine_diff_density_rms 0.076 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 228 _refine_ls_number_reflns 3435 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0357 _refine_ls_R_factor_gt 0.0342 _refine_ls_restrained_S_all 1.074 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0414P)^2^+2.1892P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0887 _refine_ls_wR_factor_ref 0.0897 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C4(H4), C5(H5), C8(H8), C11(H11), C12(H12), C14(H14), C15(H15), C17(H17), C18(H18), C20(H20), C21(H21) 2.b Idealised Me refined as rotating group: C7(H7A,H7B,H7C), C22(H22A,H22B,H22C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.33253(2) 0.76558(5) 0.11459(2) 0.04576(12) Uani 1 1 d . . . . . S1 S 0.39475(5) 0.81635(12) 0.46969(3) 0.03736(17) Uani 1 1 d . . . . . S2 S 0.49015(4) 1.14778(10) 0.38354(2) 0.03127(15) Uani 1 1 d . . . . . C1 C 0.20258(19) 0.7105(4) 0.50033(10) 0.0336(5) Uani 1 1 d . . . . . H1 H 0.185538 0.852576 0.487009 0.040 Uiso 1 1 calc R U . . . C2 C 0.13039(18) 0.5758(5) 0.52428(10) 0.0334(5) Uani 1 1 d . . . . . H2 H 0.065298 0.628843 0.527184 0.040 Uiso 1 1 calc R U . . . C3 C 0.15409(19) 0.3619(4) 0.54407(9) 0.0328(5) Uani 1 1 d . . . . . C4 C 0.2520(2) 0.2881(4) 0.53934(10) 0.0357(6) Uani 1 1 d . . . . . H4 H 0.269073 0.145864 0.552543 0.043 Uiso 1 1 calc R U . . . C5 C 0.32481(19) 0.4215(5) 0.51535(10) 0.0354(6) Uani 1 1 d . . . . . H5 H 0.389817 0.368225 0.512204 0.042 Uiso 1 1 calc R U . . . C6 C 0.30037(18) 0.6347(4) 0.49610(9) 0.0312(5) Uani 1 1 d . . . . . C7 C 0.0751(2) 0.2154(5) 0.56997(13) 0.0497(7) Uani 1 1 d . . . . . H7A H 0.035049 0.305214 0.594196 0.075 Uiso 1 1 calc R U . . . H7B H 0.106449 0.096126 0.590346 0.075 Uiso 1 1 calc R U . . . H7C H 0.033529 0.151698 0.541837 0.075 Uiso 1 1 calc R U . . . C8 C 0.37123(17) 0.7928(4) 0.39980(10) 0.0299(5) Uani 1 1 d . . . . . H8 H 0.324280 0.686734 0.388507 0.036 Uiso 1 1 calc R U . . . C9 C 0.41627(16) 0.9173(4) 0.36092(9) 0.0276(5) Uani 1 1 d . . . . . C10 C 0.39841(15) 0.8800(4) 0.30171(9) 0.0259(5) Uani 1 1 d . . . . . C11 C 0.41899(16) 1.0477(4) 0.26280(10) 0.0296(5) Uani 1 1 d . . . . . H11 H 0.445914 1.184561 0.274247 0.035 Uiso 1 1 calc R U . . . C12 C 0.39991(17) 1.0131(4) 0.20747(10) 0.0325(5) Uani 1 1 d . . . . . H12 H 0.414219 1.125737 0.182108 0.039 Uiso 1 1 calc R U . . . C13 C 0.35963(17) 0.8108(4) 0.19037(10) 0.0302(5) Uani 1 1 d . . . . . C14 C 0.33996(16) 0.6397(4) 0.22764(10) 0.0294(5) Uani 1 1 d . . . . . H14 H 0.313099 0.503334 0.215794 0.035 Uiso 1 1 calc R U . . . C15 C 0.36068(16) 0.6739(4) 0.28255(10) 0.0287(5) Uani 1 1 d . . . . . H15 H 0.349301 0.557461 0.307335 0.034 Uiso 1 1 calc R U . . . C16 C 0.60934(16) 1.0929(4) 0.35497(9) 0.0241(4) Uani 1 1 d . . . . . C17 C 0.67903(19) 1.2672(4) 0.35745(10) 0.0298(5) Uani 1 1 d . . . . . H17 H 0.661908 1.404828 0.373187 0.036 Uiso 1 1 calc R U . . . C18 C 0.77414(18) 1.2349(4) 0.33638(10) 0.0328(5) Uani 1 1 d . . . . . H18 H 0.820550 1.351294 0.338830 0.039 Uiso 1 1 calc R U . . . C19 C 0.80151(17) 1.0330(4) 0.31175(9) 0.0299(5) Uani 1 1 d . . . . . C20 C 0.73135(17) 0.8609(4) 0.31014(9) 0.0293(5) Uani 1 1 d . . . . . H20 H 0.748378 0.723565 0.294206 0.035 Uiso 1 1 calc R U . . . C21 C 0.63631(17) 0.8884(4) 0.33172(9) 0.0273(5) Uani 1 1 d . . . . . H21 H 0.590862 0.769819 0.330563 0.033 Uiso 1 1 calc R U . . . C22 C 0.90383(19) 1.0015(6) 0.28723(11) 0.0438(7) Uani 1 1 d . . . . . H22A H 0.949594 0.953963 0.315279 0.066 Uiso 1 1 calc R U . . . H22B H 0.926202 1.141806 0.271815 0.066 Uiso 1 1 calc R U . . . H22C H 0.900790 0.888798 0.258985 0.066 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0546(2) 0.0522(2) 0.03040(17) 0.00038(12) -0.00580(13) -0.00225(13) S1 0.0378(3) 0.0455(4) 0.0288(3) -0.0034(3) 0.0014(2) -0.0112(3) S2 0.0320(3) 0.0280(3) 0.0338(3) -0.0080(2) 0.0075(2) -0.0018(2) C1 0.0383(13) 0.0333(13) 0.0291(12) 0.0035(10) -0.0029(10) -0.0005(11) C2 0.0326(12) 0.0403(14) 0.0274(12) 0.0028(11) -0.0017(9) -0.0012(11) C3 0.0394(13) 0.0380(14) 0.0211(11) 0.0049(10) -0.0048(9) -0.0061(11) C4 0.0458(14) 0.0311(13) 0.0301(13) 0.0006(10) -0.0054(11) -0.0008(11) C5 0.0359(13) 0.0380(14) 0.0324(13) -0.0052(11) 0.0005(10) 0.0022(11) C6 0.0370(13) 0.0358(14) 0.0208(11) -0.0030(10) 0.0005(9) -0.0053(10) C7 0.0460(16) 0.0548(19) 0.0483(17) 0.0232(14) 0.0004(13) -0.0068(14) C8 0.0264(11) 0.0334(13) 0.0299(12) -0.0013(10) 0.0007(9) -0.0013(10) C9 0.0241(11) 0.0275(12) 0.0314(12) -0.0009(10) 0.0029(9) 0.0011(9) C10 0.0198(10) 0.0278(12) 0.0302(12) 0.0010(10) 0.0021(8) 0.0030(9) C11 0.0260(11) 0.0276(12) 0.0351(12) 0.0017(10) 0.0019(9) -0.0018(9) C12 0.0306(12) 0.0326(13) 0.0343(13) 0.0073(10) 0.0022(10) 0.0001(10) C13 0.0256(11) 0.0362(13) 0.0287(12) 0.0002(10) -0.0002(9) 0.0038(10) C14 0.0245(11) 0.0295(13) 0.0342(12) -0.0029(10) 0.0007(9) -0.0010(9) C15 0.0259(11) 0.0285(12) 0.0318(12) 0.0034(10) 0.0029(9) 0.0005(9) C16 0.0270(11) 0.0250(11) 0.0202(10) -0.0002(9) -0.0021(8) -0.0007(9) C17 0.0378(13) 0.0240(12) 0.0277(12) -0.0026(9) -0.0024(10) -0.0032(10) C18 0.0306(12) 0.0356(14) 0.0321(13) 0.0041(10) -0.0039(10) -0.0106(10) C19 0.0261(11) 0.0393(14) 0.0241(11) 0.0061(10) -0.0043(9) 0.0012(10) C20 0.0306(12) 0.0294(13) 0.0279(11) -0.0039(9) -0.0039(9) 0.0055(10) C21 0.0269(11) 0.0245(12) 0.0303(11) -0.0019(9) -0.0039(9) -0.0015(9) C22 0.0299(13) 0.0608(19) 0.0408(14) 0.0094(13) 0.0017(11) 0.0045(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 C13 1.902(2) . ? S1 C6 1.782(3) . ? S1 C8 1.738(2) . ? S2 C9 1.773(2) . ? S2 C16 1.774(2) . ? C1 H1 0.9300 . ? C1 C2 1.384(4) . ? C1 C6 1.389(4) . ? C2 H2 0.9300 . ? C2 C3 1.392(4) . ? C3 C4 1.388(4) . ? C3 C7 1.509(4) . ? C4 H4 0.9300 . ? C4 C5 1.387(4) . ? C5 H5 0.9300 . ? C5 C6 1.385(4) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8 0.9300 . ? C8 C9 1.346(3) . ? C9 C10 1.480(3) . ? C10 C11 1.401(3) . ? C10 C15 1.401(3) . ? C11 H11 0.9300 . ? C11 C12 1.388(3) . ? C12 H12 0.9300 . ? C12 C13 1.378(4) . ? C13 C14 1.387(4) . ? C14 H14 0.9300 . ? C14 C15 1.382(3) . ? C15 H15 0.9300 . ? C16 C17 1.393(3) . ? C16 C21 1.385(3) . ? C17 H17 0.9300 . ? C17 C18 1.389(4) . ? C18 H18 0.9300 . ? C18 C19 1.388(4) . ? C19 C20 1.387(3) . ? C19 C22 1.509(3) . ? C20 H20 0.9300 . ? C20 C21 1.389(3) . ? C21 H21 0.9300 . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 S1 C6 100.30(11) . . ? C9 S2 C16 103.86(10) . . ? C2 C1 H1 119.8 . . ? C2 C1 C6 120.4(2) . . ? C6 C1 H1 119.8 . . ? C1 C2 H2 119.6 . . ? C1 C2 C3 120.8(2) . . ? C3 C2 H2 119.6 . . ? C2 C3 C7 120.6(2) . . ? C4 C3 C2 118.2(2) . . ? C4 C3 C7 121.2(2) . . ? C3 C4 H4 119.3 . . ? C5 C4 C3 121.5(2) . . ? C5 C4 H4 119.3 . . ? C4 C5 H5 120.1 . . ? C6 C5 C4 119.7(2) . . ? C6 C5 H5 120.1 . . ? C1 C6 S1 120.1(2) . . ? C5 C6 S1 120.3(2) . . ? C5 C6 C1 119.4(2) . . ? C3 C7 H7A 109.5 . . ? C3 C7 H7B 109.5 . . ? C3 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? S1 C8 H8 117.8 . . ? C9 C8 S1 124.5(2) . . ? C9 C8 H8 117.8 . . ? C8 C9 S2 116.98(18) . . ? C8 C9 C10 122.3(2) . . ? C10 C9 S2 120.49(17) . . ? C11 C10 C9 121.6(2) . . ? C15 C10 C9 120.9(2) . . ? C15 C10 C11 117.6(2) . . ? C10 C11 H11 119.4 . . ? C12 C11 C10 121.2(2) . . ? C12 C11 H11 119.4 . . ? C11 C12 H12 120.2 . . ? C13 C12 C11 119.6(2) . . ? C13 C12 H12 120.2 . . ? C12 C13 Br1 119.37(19) . . ? C12 C13 C14 120.8(2) . . ? C14 C13 Br1 119.87(19) . . ? C13 C14 H14 120.3 . . ? C15 C14 C13 119.4(2) . . ? C15 C14 H14 120.3 . . ? C10 C15 H15 119.3 . . ? C14 C15 C10 121.5(2) . . ? C14 C15 H15 119.3 . . ? C17 C16 S2 116.85(18) . . ? C21 C16 S2 123.83(18) . . ? C21 C16 C17 119.3(2) . . ? C16 C17 H17 120.1 . . ? C18 C17 C16 119.9(2) . . ? C18 C17 H17 120.1 . . ? C17 C18 H18 119.3 . . ? C19 C18 C17 121.5(2) . . ? C19 C18 H18 119.3 . . ? C18 C19 C22 121.3(2) . . ? C20 C19 C18 117.7(2) . . ? C20 C19 C22 121.0(2) . . ? C19 C20 H20 119.2 . . ? C19 C20 C21 121.7(2) . . ? C21 C20 H20 119.2 . . ? C16 C21 C20 119.9(2) . . ? C16 C21 H21 120.1 . . ? C20 C21 H21 120.1 . . ? C19 C22 H22A 109.5 . . ? C19 C22 H22B 109.5 . . ? C19 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 C13 C14 C15 179.51(17) . . . . ? S1 C8 C9 S2 -9.8(3) . . . . ? S1 C8 C9 C10 175.84(17) . . . . ? S2 C9 C10 C11 -14.5(3) . . . . ? S2 C9 C10 C15 165.09(17) . . . . ? S2 C16 C17 C18 179.33(19) . . . . ? S2 C16 C21 C20 179.78(17) . . . . ? C1 C2 C3 C4 0.3(4) . . . . ? C1 C2 C3 C7 -179.8(2) . . . . ? C2 C1 C6 S1 -175.54(19) . . . . ? C2 C1 C6 C5 0.9(4) . . . . ? C2 C3 C4 C5 -0.4(4) . . . . ? C3 C4 C5 C6 0.7(4) . . . . ? C4 C5 C6 S1 175.46(19) . . . . ? C4 C5 C6 C1 -1.0(4) . . . . ? C6 S1 C8 C9 172.8(2) . . . . ? C6 C1 C2 C3 -0.6(4) . . . . ? C7 C3 C4 C5 179.7(3) . . . . ? C8 S1 C6 C1 -79.2(2) . . . . ? C8 S1 C6 C5 104.4(2) . . . . ? C8 C9 C10 C11 159.7(2) . . . . ? C8 C9 C10 C15 -20.7(3) . . . . ? C9 S2 C16 C17 168.62(18) . . . . ? C9 S2 C16 C21 -12.5(2) . . . . ? C9 C10 C11 C12 -178.5(2) . . . . ? C9 C10 C15 C14 177.4(2) . . . . ? C10 C11 C12 C13 0.3(3) . . . . ? C11 C10 C15 C14 -2.9(3) . . . . ? C11 C12 C13 Br1 179.43(17) . . . . ? C11 C12 C13 C14 -1.4(3) . . . . ? C12 C13 C14 C15 0.3(3) . . . . ? C13 C14 C15 C10 1.9(3) . . . . ? C15 C10 C11 C12 1.9(3) . . . . ? C16 S2 C9 C8 123.19(19) . . . . ? C16 S2 C9 C10 -62.32(19) . . . . ? C16 C17 C18 C19 1.2(4) . . . . ? C17 C16 C21 C20 -1.4(3) . . . . ? C17 C18 C19 C20 -1.7(4) . . . . ? C17 C18 C19 C22 177.9(2) . . . . ? C18 C19 C20 C21 0.7(3) . . . . ? C19 C20 C21 C16 0.8(3) . . . . ? C21 C16 C17 C18 0.4(3) . . . . ? C22 C19 C20 C21 -178.9(2) . . . . ? _shelx_res_file ; TITL 1_a.res in P2(1)/n 1.res created by SHELXL-2019/2 at 10:36:02 on 29-Mar-2023 REM Old TITL 1 in P21/n #14 REM SHELXT solution in P2(1)/n: R1 0.247, Rweak 0.020, Alpha 0.017 REM 0.601 for 358 systematic absences, Orientation as input REM Formula found by SHELXT: C22 O2 Br CELL 1.54184 13.401735 5.921057 24.391702 90 90.1424 90 ZERR 4 0.000201 0.000105 0.000382 0 0.0014 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Br S UNIT 88 76 4 8 L.S. 20 0 0 PLAN 4 SIZE 0.03 0.05 0.12 TEMP 150 CONF BOND list 4 fmap 2 53 acta MORE -1 HTAB BOND $H SHEL 999 0.837 REM REM REM WGHT 0.041400 2.189200 FVAR 4.30368 BR1 3 0.332531 0.765576 0.114585 11.00000 0.05462 0.05223 = 0.03040 0.00038 -0.00580 -0.00225 S1 4 0.394752 0.816349 0.469688 11.00000 0.03779 0.04551 = 0.02878 -0.00336 0.00139 -0.01119 S2 4 0.490148 1.147776 0.383541 11.00000 0.03204 0.02798 = 0.03383 -0.00799 0.00751 -0.00181 C1 1 0.202583 0.710524 0.500334 11.00000 0.03830 0.03332 = 0.02906 0.00345 -0.00292 -0.00047 AFIX 43 H1 2 0.185538 0.852576 0.487009 11.00000 -1.20000 AFIX 0 C2 1 0.130389 0.575805 0.524283 11.00000 0.03258 0.04034 = 0.02735 0.00278 -0.00171 -0.00118 AFIX 43 H2 2 0.065298 0.628843 0.527184 11.00000 -1.20000 AFIX 0 C3 1 0.154087 0.361941 0.544066 11.00000 0.03936 0.03799 = 0.02112 0.00491 -0.00483 -0.00615 C4 1 0.251961 0.288060 0.539335 11.00000 0.04581 0.03111 = 0.03011 0.00055 -0.00544 -0.00080 AFIX 43 H4 2 0.269073 0.145864 0.552543 11.00000 -1.20000 AFIX 0 C5 1 0.324811 0.421550 0.515352 11.00000 0.03586 0.03796 = 0.03235 -0.00519 0.00048 0.00220 AFIX 43 H5 2 0.389817 0.368225 0.512204 11.00000 -1.20000 AFIX 0 C6 1 0.300370 0.634668 0.496097 11.00000 0.03698 0.03577 = 0.02082 -0.00304 0.00051 -0.00531 C7 1 0.075098 0.215426 0.569966 11.00000 0.04599 0.05481 = 0.04828 0.02322 0.00041 -0.00679 AFIX 137 H7A 2 0.035049 0.305214 0.594196 11.00000 -1.50000 H7B 2 0.106449 0.096126 0.590346 11.00000 -1.50000 H7C 2 0.033529 0.151698 0.541837 11.00000 -1.50000 AFIX 0 C8 1 0.371225 0.792752 0.399801 11.00000 0.02641 0.03337 = 0.02986 -0.00125 0.00070 -0.00126 AFIX 43 H8 2 0.324280 0.686734 0.388507 11.00000 -1.20000 AFIX 0 C9 1 0.416269 0.917341 0.360923 11.00000 0.02409 0.02748 = 0.03137 -0.00091 0.00289 0.00112 C10 1 0.398409 0.879998 0.301709 11.00000 0.01975 0.02778 = 0.03024 0.00096 0.00209 0.00304 C11 1 0.418986 1.047652 0.262795 11.00000 0.02599 0.02763 = 0.03507 0.00169 0.00189 -0.00176 AFIX 43 H11 2 0.445914 1.184561 0.274247 11.00000 -1.20000 AFIX 0 C12 1 0.399909 1.013095 0.207470 11.00000 0.03056 0.03258 = 0.03431 0.00726 0.00221 0.00014 AFIX 43 H12 2 0.414219 1.125737 0.182108 11.00000 -1.20000 AFIX 0 C13 1 0.359632 0.810824 0.190366 11.00000 0.02555 0.03624 = 0.02872 0.00019 -0.00015 0.00379 C14 1 0.339965 0.639744 0.227635 11.00000 0.02450 0.02946 = 0.03423 -0.00289 0.00070 -0.00096 AFIX 43 H14 2 0.313099 0.503334 0.215794 11.00000 -1.20000 AFIX 0 C15 1 0.360676 0.673931 0.282546 11.00000 0.02587 0.02847 = 0.03179 0.00337 0.00289 0.00054 AFIX 43 H15 2 0.349301 0.557461 0.307335 11.00000 -1.20000 AFIX 0 C16 1 0.609345 1.092945 0.354970 11.00000 0.02704 0.02504 = 0.02021 -0.00021 -0.00207 -0.00069 C17 1 0.679035 1.267163 0.357449 11.00000 0.03780 0.02401 = 0.02768 -0.00259 -0.00244 -0.00316 AFIX 43 H17 2 0.661908 1.404828 0.373187 11.00000 -1.20000 AFIX 0 C18 1 0.774144 1.234930 0.336378 11.00000 0.03058 0.03559 = 0.03213 0.00407 -0.00387 -0.01055 AFIX 43 H18 2 0.820550 1.351294 0.338830 11.00000 -1.20000 AFIX 0 C19 1 0.801511 1.033014 0.311747 11.00000 0.02614 0.03929 = 0.02412 0.00606 -0.00426 0.00115 C20 1 0.731349 0.860908 0.310140 11.00000 0.03060 0.02943 = 0.02794 -0.00387 -0.00390 0.00549 AFIX 43 H20 2 0.748378 0.723565 0.294206 11.00000 -1.20000 AFIX 0 C21 1 0.636308 0.888432 0.331719 11.00000 0.02695 0.02450 = 0.03034 -0.00194 -0.00386 -0.00153 AFIX 43 H21 2 0.590862 0.769819 0.330563 11.00000 -1.20000 AFIX 0 C22 1 0.903830 1.001532 0.287226 11.00000 0.02991 0.06078 = 0.04078 0.00937 0.00171 0.00452 AFIX 137 H22A 2 0.949594 0.953963 0.315279 11.00000 -1.50000 H22B 2 0.926202 1.141806 0.271815 11.00000 -1.50000 H22C 2 0.900790 0.888798 0.258985 11.00000 -1.50000 AFIX 0 HKLF 4 REM 1_a.res in P2(1)/n REM wR2 = 0.0897, GooF = S = 1.074, Restrained GooF = 1.074 for all data REM R1 = 0.0342 for 3219 Fo > 4sig(Fo) and 0.0357 for all 3435 data REM 228 parameters refined using 0 restraints END WGHT 0.0414 2.1892 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 1.263, deepest hole -0.864, 1-sigma level 0.076 Q1 1 0.3766 0.6642 0.1203 11.00000 0.05 1.26 Q2 1 0.2956 0.6335 0.3994 11.00000 0.05 0.72 Q3 1 0.9584 1.1054 0.3176 11.00000 0.05 0.24 Q4 1 0.0822 0.2661 0.6185 11.00000 0.05 0.24 ; _shelx_res_checksum 24890 _shelx_hkl_file ; 0 0 2 4352.40 116.967 4 0 0 3 3.72720 13.0989 4 0 0 4 44965.9 1142.96 4 0 0 5 6.88874 19.7819 4 0 0 6 100150. 2535.26 4 0 0 7 43.6130 24.0880 4 0 0 8 265910. 6696.79 4 0 0 9-4.22630 20.9878 4 0 0 10 211288. 5339.45 4 0 0 11-3.95048 21.1481 4 0 0 -12 307110. 7667.69 14 0 0 12 314678. 7667.67 4 0 0 -12 302296. 7685.06 6 0 0 13 3.12157 17.8565 4 0 0 -13 9.90309 23.1266 14 0 0 -14 133488. 3435.04 14 0 0 14 135888. 3508.60 12 0 0 -15 21.4507 53.2461 18 0 0 15 53.6339 62.1851 12 0 0 15 52.1838 46.3969 23 0 0 16 8912.23 325.419 23 0 0 -16 9137.38 371.954 18 0 0 16 8486.06 359.447 12 0 0 -17 40.0592 74.0587 11 0 0 -17 46.6904 62.3360 18 0 0 17 23.4411 45.0508 23 0 0 -18 39632.1 1189.32 18 0 0 -18 38883.4 1209.45 11 0 0 -19-20.3310 86.6825 11 0 0 -19 12.2760 71.2461 18 0 0 -20 9853.86 433.047 18 0 0 -20 9066.04 441.427 11 0 0 -21 61.6911 82.9079 18 0 0 -21 7.64133 89.3314 11 0 0 -22 62106.4 1858.07 11 0 0 -22 62964.8 1828.54 18 0 0 -23-42.4143 85.4976 18 0 0 -23 71.7500 106.086 11 0 0 -24 578.581 134.789 11 0 0 -24 467.469 114.775 18 0 0 -25 74.4375 108.327 11 0 0 -26 66934.2 1933.20 11 0 0 -27-18.3072 85.5053 11 0 0 -28 9193.87 389.684 11 0 0 -29 24.5173 56.6933 11 0 0 -30 3521.77 170.781 11 0 1 0 28.4994 15.8604 5 0 1 -1 6816.12 191.242 6 0 1 -1 7038.07 181.568 1 0 -1 1 6782.30 198.381 14 0 -1 -1 6958.02 181.361 6 0 1 -2 211350. 5277.58 6 0 -1 -2 208330. 5277.05 4 0 -1 -3 338561. 8122.62 15 0 1 -3 334067. 8122.17 6 0 -1 -4 70424.8 1705.45 15 0 1 -4 64372.4 1702.26 6 0 1 4 67616.1 1694.65 4 0 -1 -4 65421.7 1692.89 4 0 1 -5 3845.88 130.184 14 0 -1 5 4121.03 138.287 15 0 1 5 3806.20 128.642 15 0 1 -5 3429.21 124.338 6 0 -1 -5 3914.07 130.077 15 0 -1 -5 3580.37 112.643 4 0 1 5 3880.46 117.648 4 0 -1 -6 852298. 21493.5 15 0 1 6 848985. 21477.0 4 0 1 6 896296. 21493.7 15 0 -1 -6 882752. 21472.6 4 0 1 -6 818170. 21491.5 14 0 -1 6 806891. 21497.2 15 0 1 -6 865685. 21489.4 6 0 1 7 11330.4 320.719 15 0 -1 -7 10936.1 319.457 15 0 1 -7 10617.5 316.905 6 0 -1 7 11139.2 326.444 15 0 -1 -7 11018.9 296.364 4 0 1 7 11518.5 303.314 4 0 -1 -8 126431. 3213.19 15 0 -1 8 122311. 3214.65 15 0 -1 -8 131995. 3184.12 4 0 1 -8 118957. 3207.16 6 0 1 8 123706. 3212.40 15 0 1 -8 122440. 3206.08 14 0 1 8 128923. 3189.15 4 0 -1 -9 385.952 31.6698 4 0 1 9 456.419 36.4001 4 0 1 -9 375.149 47.9503 6 0 -1 -9 420.655 48.9400 15 0 1 -9 373.392 43.2618 14 0 -1 9 379.654 46.6690 15 0 -1 9 419.246 46.0873 4 0 1 9 387.661 48.0052 15 0 1 10 94927.1 2391.19 15 0 1 10 92250.3 2353.96 4 0 -1 10 90854.9 2373.64 4 0 1 -10 90344.3 2374.87 14 0 -1 10 92269.5 2391.53 15 0 -1 -10 94563.2 2390.80 15 0 -1 -11 12630.1 400.545 15 0 1 -11 12612.8 388.082 14 0 1 11 13237.9 367.523 4 0 1 11 13329.4 403.752 15 0 -1 11 13012.9 403.810 15 0 -1 11 12733.9 385.108 4 0 -1 -12 7959.84 252.483 6 0 -1 12 8233.74 258.985 4 0 -1 -12 7260.76 271.657 15 0 -1 12 7225.22 268.176 15 0 1 12 7505.25 271.251 15 0 1 12 7839.48 234.758 4 0 1 -12 7023.82 253.822 14 0 1 -13 1757.17 100.806 14 0 -1 13 1572.65 94.3798 4 0 1 13 2010.49 144.058 16 0 -1 13 1874.92 113.769 15 0 -1 -13 1807.03 99.4192 6 0 -1 13 1762.86 131.183 12 0 1 13 2038.86 120.226 15 0 1 14 61426.5 1764.35 16 0 1 -14 63244.8 1749.23 8 0 1 14 69686.1 1737.65 23 0 -1 14 60663.1 1675.48 4 0 -1 14 66559.9 1753.80 12 0 -1 15 2425.27 168.219 12 0 1 15 2449.09 152.989 23 0 1 -15 2657.60 183.273 11 0 -1 -15 2655.09 162.015 18 0 -1 16 94617.2 2530.42 12 0 -1 -16 94455.5 2511.61 18 0 1 -16 95385.9 2561.96 11 0 1 16 91203.9 2493.72 23 0 1 -17 523.980 111.461 11 0 -1 17 352.356 98.3476 12 0 1 -17 481.919 109.591 18 0 -1 -17 403.807 92.8338 11 0 1 17 514.625 86.8406 23 0 -1 -17 511.514 88.4364 18 0 -1 -18 47628.4 1387.47 18 0 -1 -18 47750.8 1414.84 11 0 1 -18 47130.2 1438.01 11 0 1 -18 47887.7 1432.60 18 0 1 18 48538.3 1365.62 23 0 -1 -19 8702.25 404.294 11 0 1 19 8471.56 356.401 23 0 -1 -19 8559.04 379.247 18 0 1 -19 8919.56 417.594 18 0 1 -19 8790.00 424.586 11 0 1 -20 82421.0 2396.15 11 0 -1 -20 85861.7 2376.00 11 0 -1 -20 84072.2 2337.37 18 0 1 -20 86658.8 2391.39 18 0 1 20 83767.7 2291.70 23 0 1 21 136.524 71.0178 23 0 1 -21 22.5668 95.1291 18 0 -1 -21 149.939 93.5029 11 0 -1 -21 164.766 82.1437 18 0 1 -21 137.441 118.745 11 0 1 -22 1464.14 181.785 18 0 -1 -22 1146.56 141.692 18 0 -1 -22 1482.65 173.162 11 0 1 22 1042.07 119.777 23 0 1 23 3225.31 197.710 23 0 -1 -23 3130.58 224.156 18 0 1 -23 3645.69 268.437 18 0 -1 -23 3543.16 258.816 11 0 1 24 32344.2 977.933 23 0 1 -24 34480.0 1100.81 18 0 -1 -24 33625.6 1083.03 11 0 -1 -25 26.4956 88.1450 11 0 1 25 14.2610 53.5035 23 0 -1 -26 625.324 115.257 11 0 -1 -27 1103.95 127.678 11 0 -1 27 964.396 115.990 3 0 1 27 927.335 111.671 3 0 1 28 36430.6 1024.91 3 0 -1 28 35830.7 1025.63 3 0 -1 -28 35679.2 1049.37 11 0 -1 29 79.5915 53.3105 3 0 -1 -29 140.532 47.8330 11 0 -2 0 496082. 12080.5 14 0 2 0 472722. 12054.6 5 0 2 -1 448.679 37.1909 5 0 -2 1 602.209 50.4457 14 0 -2 2 148353. 3721.55 14 0 -2 -2 144740. 3716.13 4 0 -2 -3 6505.76 223.246 15 0 2 -3 8084.03 208.821 1 0 -2 -3 7267.18 203.922 1 0 -2 3 7286.05 236.606 14 0 -2 -3 8175.39 233.477 4 0 -2 4 226347. 5879.74 14 0 -2 -4 230460. 5850.96 1 0 2 -4 227714. 5853.27 1 0 -2 -4 245127. 5873.74 15 0 -2 -4 230903. 5867.65 4 0 2 -4 238454. 5872.09 6 0 2 -5 4345.66 139.745 1 0 2 -5 4423.93 152.711 6 0 -2 -5 4182.80 139.929 4 0 -2 -5 4380.77 149.551 15 0 -2 -5 3984.71 109.124 5 0 -2 -5 4214.15 136.641 1 0 -2 -5 4041.06 108.074 6 0 -2 -6 11108.3 302.962 4 0 -2 -6 10285.6 276.105 6 0 -2 -6 10452.5 317.656 15 0 2 -6 10602.3 322.065 6 0 2 -6 10420.6 309.377 1 0 -2 -6 11155.0 310.833 1 0 2 -7 88626.3 2344.30 6 0 -2 7 93082.8 2356.52 15 0 -2 -7 87458.1 2332.25 1 0 -2 -7 100249. 2349.40 15 0 -2 -7 87796.3 2296.30 6 0 2 -7 88783.4 2334.30 1 0 -2 -7 97231.3 2318.87 4 0 -2 -8 115615. 2974.89 15 0 2 -8 113106. 2975.07 6 0 -2 -8 113958. 2939.91 4 0 2 -8 116961. 2970.37 1 0 -2 -8 113108. 2969.07 1 0 -2 -8 117938. 2928.74 6 0 -2 8 119238. 2987.12 15 0 -2 -9 7435.66 224.270 6 0 -2 -9 7966.61 231.323 4 0 2 -9 7919.27 263.614 1 0 -2 -9 7816.32 262.725 1 0 2 -9 7165.31 261.916 6 0 -2 9 8214.97 274.318 15 0 -2 -9 8017.00 265.840 15 0 -2 10 21385.1 633.820 15 0 -2 -10 21357.5 627.993 15 0 -2 -10 22454.9 631.848 1 0 2 -10 21985.2 631.673 1 0 -2 11 744.072 73.1560 15 0 -2 -11 783.324 72.7764 1 0 2 -11 799.600 88.4969 8 0 2 -11 721.513 72.2022 1 0 2 11 503.392 80.0504 16 0 -2 -12 47886.7 1337.24 1 0 -2 12 49071.3 1361.56 12 0 2 -12 47843.7 1335.70 1 0 2 -12 49342.6 1387.78 11 0 2 12 51709.7 1389.90 16 0 2 -12 50097.9 1387.70 18 0 2 13 11332.2 427.951 16 0 -2 13 11044.2 406.047 12 0 2 -13 11998.1 437.769 11 0 2 -13 10592.7 422.821 18 0 2 -14 97531.5 2638.09 18 0 2 14 99556.7 2603.58 23 0 2 -14 92264.3 2616.08 8 0 2 14 102821. 2640.58 16 0 2 -14 95995.1 2637.47 11 0 -2 14 97917.8 2606.63 12 0 2 15 327.336 90.2959 16 0 2 -15 258.037 82.5323 8 0 2 15 371.553 83.5193 23 0 -2 15 296.693 84.1376 12 0 2 -15 308.898 86.4194 11 0 2 -15 318.624 90.5178 18 0 2 -16 4182.47 260.926 11 0 2 -16 4019.55 248.120 8 0 -2 16 4644.48 252.120 12 0 2 -16 4529.37 265.998 18 0 2 16 4928.25 250.210 23 0 2 16 5115.68 276.840 16 0 2 17 7405.38 331.309 23 0 2 -17 6712.29 357.709 11 0 2 17 7500.98 361.323 16 0 2 -17 7230.03 362.051 18 0 2 18 53032.4 1506.95 23 0 2 -18 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20539.8 734.820 11 3 3 17 21341.7 750.308 16 3 3 17 21621.8 730.986 23 3 -3 18 16586.7 597.027 12 3 3 18 16246.3 624.120 16 -3 3 -18 16622.3 624.469 8 3 3 18 17086.2 611.783 23 -3 3 -18 15843.9 623.980 18 -3 3 -18 15504.7 610.024 11 3 -3 19 9373.17 404.470 12 3 3 19 9551.32 417.747 23 -3 3 -19 9246.05 427.053 8 -3 3 -19 9165.53 430.015 18 3 3 19 9008.81 435.713 16 -3 3 -19 9569.23 428.839 11 3 3 20 2581.57 225.188 16 -3 3 -20 2860.17 218.932 18 -3 3 -20 2590.54 208.882 11 -3 3 -21 6382.28 327.395 11 -3 3 -21 6204.51 334.255 18 3 3 21 5586.23 329.365 16 -3 3 -22 1518.54 134.877 13 -3 3 -22 1524.00 157.209 11 -3 3 -22 1385.90 153.963 18 -3 3 -23 14341.0 480.614 13 -3 3 -23 13236.0 506.950 11 3 3 23 13143.0 489.300 23 -3 3 -24 4050.42 225.821 11 -3 3 -24 4345.57 200.245 13 3 3 24 4588.85 226.243 23 3 3 25 6808.80 270.089 23 -3 3 -25 6284.30 270.250 11 3 3 26 44.9484 48.5145 23 3 3 27 1224.66 77.2639 23 3 4 -24 453.924 60.6558 22 3 4 -23 430.878 72.6982 22 3 4 -22 643.565 78.6747 13 3 4 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7338.47 347.829 13 3 4 -7 6922.73 322.028 21 3 4 -6 2900.75 193.381 21 3 4 -6 3330.09 220.341 13 3 4 -6 3328.88 212.102 10 3 4 -5 72.4897 75.4617 13 3 4 -5 83.7132 61.9604 21 3 4 -5 231.365 78.3848 10 3 4 -4 54506.9 1605.97 13 3 4 -4 53440.6 1566.35 21 3 4 -4 53223.9 1578.26 10 3 4 -3 4730.19 263.812 13 3 4 -3 5041.97 249.233 21 3 4 -3 4685.44 250.834 10 3 4 -2 5476.95 260.826 21 3 4 -2 5280.48 282.653 13 3 4 -2 5126.19 266.140 10 3 4 -1 12429.7 460.856 21 3 4 -1 12506.5 488.422 13 3 4 -1 13104.1 474.065 10 3 4 0 7493.03 341.846 13 3 4 0 7217.11 317.369 21 3 4 0 7572.93 324.857 10 3 4 1 13591.3 512.541 13 3 4 1 13645.0 493.772 21 3 4 1 14101.0 497.021 10 3 4 2 3850.01 215.992 21 3 4 2 3632.09 220.833 13 3 4 2 3944.80 214.781 10 -3 4 -3 8266.59 317.350 8 3 4 3 8717.28 365.791 13 3 4 3 8339.42 346.981 10 3 4 3 8769.02 359.363 21 -3 4 -4 3026.59 168.276 8 3 4 4 2923.74 193.495 21 3 4 5 174.528 70.2713 21 -3 4 -5 52.5446 50.2861 8 -3 4 -5 155.633 75.7871 10 3 4 6 243.021 77.6486 21 3 4 6 188.036 73.3062 9 -3 4 -6 104.196 57.1173 8 -3 4 -7 618.990 110.004 10 -3 4 -7 590.434 90.9994 8 -3 4 -8 9066.78 383.494 8 -3 4 -8 10535.1 411.602 10 3 4 9 1629.43 145.959 23 -3 4 -9 1772.60 152.302 8 -3 4 -9 1850.53 159.580 10 -3 4 -10 163.649 75.5990 8 3 4 10 220.208 84.5244 23 -3 4 -10 247.348 82.1351 10 3 4 11 19627.2 698.790 16 3 4 11 19935.2 683.232 23 -3 4 -11 19643.2 679.145 8 -3 4 -11 20341.7 674.754 10 -3 4 -12 503.000 104.879 8 3 4 12 640.969 116.272 23 3 4 12 559.360 118.614 16 -3 4 -12 471.808 96.1493 10 3 4 13 16505.2 640.754 16 3 4 13 17906.2 632.477 23 -3 4 -13 17720.6 639.261 8 -3 4 -13 18430.2 620.416 10 -3 4 -14 28393.2 877.623 10 3 4 14 27683.6 894.630 23 3 4 14 26602.4 905.864 16 -3 4 -14 27871.2 908.289 8 3 4 15 457.016 116.364 23 -3 4 -15 333.995 110.342 8 -3 4 -15 364.020 82.2413 10 3 4 15 475.793 121.732 16 -3 4 -16 6321.38 334.199 8 3 4 16 6137.50 315.935 23 -3 4 -16 6371.41 296.185 10 3 4 16 6069.72 332.610 16 3 4 17 16024.6 579.580 23 -3 4 -17 15636.2 541.889 10 -3 4 -17 15900.2 605.674 8 3 4 17 15126.7 590.771 16 -3 4 -18 2419.86 190.675 13 3 4 18 2217.20 180.940 23 3 4 18 2291.35 198.951 16 -3 4 -19 4599.62 254.301 13 3 4 19 4574.57 253.702 23 3 4 19 4667.29 275.384 16 -3 4 -20-13.9417 64.4732 13 3 4 20-9.07742 81.3723 23 3 4 20 10.8249 84.2877 16 -3 4 -21 5382.50 254.322 13 3 4 21 4982.42 249.983 23 3 4 21 4744.25 260.490 16 -3 4 -22 35.7128 57.3599 13 3 4 22 31.6567 62.6887 23 -3 4 -23 1870.12 120.152 13 3 4 23 1771.82 123.345 23 3 4 24 402.234 60.7430 23 3 5 -20 232.470 56.4958 13 3 5 -19 2556.06 160.390 13 3 5 -18 1821.80 145.845 13 3 5 -17 4.75523 70.1288 10 3 5 -17 4.79456 70.0803 13 3 5 -16 5354.47 283.313 13 3 5 -16 5159.75 284.532 10 3 5 -15 836.233 128.610 13 3 5 -15 741.806 125.258 10 3 5 -14 17488.8 639.665 13 3 5 -14 17967.6 652.377 10 3 5 -13 1626.61 172.822 10 3 5 -12 3518.12 247.529 10 3 5 -11 470.843 126.819 13 3 5 -11 655.212 130.248 10 3 5 -10 7621.91 353.740 21 3 5 -10 8212.78 389.595 10 3 5 -10 8097.47 393.481 13 3 5 -9 501.118 120.290 13 3 5 -9 535.059 98.6329 21 3 5 -8 446.630 90.1931 21 3 5 -8 368.875 114.203 13 3 5 -7 479.800 115.922 13 3 5 -7 614.194 101.500 21 3 5 -7 331.342 106.764 10 3 5 -6 117.448 98.2741 13 3 5 -6 132.512 72.1313 21 3 5 -6 162.863 99.5234 10 3 5 -5 4112.20 267.122 13 3 5 -5 4028.48 236.314 21 3 5 -5 4016.87 256.721 10 3 5 -4 5601.34 317.074 13 -3 5 4 5105.76 254.808 10 3 5 -4 5447.10 279.582 21 3 5 -4 5135.84 293.697 10 3 5 -3 8101.17 396.488 13 3 5 -3 7819.41 357.718 21 3 5 -3 8997.51 395.478 10 -3 5 3 8742.47 359.075 10 3 5 -2 7531.35 363.858 13 -3 5 2 6961.64 318.784 10 3 5 -2 6605.04 334.641 10 3 5 -2 6628.70 317.635 21 3 5 -1 835.207 130.514 13 -3 5 1 674.531 109.669 10 3 5 -1 711.643 109.553 21 3 5 -1 647.826 118.246 10 3 5 0 8097.45 370.208 10 3 5 0 7593.71 346.877 21 -3 5 0 8196.38 358.998 10 3 5 0 7363.26 365.958 13 -3 5 -1 255.918 87.1430 10 3 5 1 304.107 87.2362 21 3 5 1 164.142 80.7267 13 3 5 1 368.653 97.9789 10 3 5 2 5817.21 307.462 10 3 5 2 5682.05 303.955 13 3 5 2 6259.22 302.934 21 -3 5 -2 6468.79 315.329 10 3 5 3 2912.45 202.356 21 3 5 3 3265.85 216.117 10 -3 5 -3 3622.55 225.462 10 -3 5 -4 711.358 112.911 13 -3 5 -4 728.777 122.724 10 3 5 5 2541.52 203.640 9 -3 5 -5 2786.13 203.255 13 -3 5 -5 2545.98 195.120 10 -3 5 -6 7631.18 358.338 13 -3 5 -6 7536.04 345.463 10 -3 5 -7 5309.27 297.351 13 -3 5 -7 4680.09 248.040 8 -3 5 -8 26029.0 847.890 8 -3 5 -8 28964.3 916.727 13 -3 5 -9 2824.30 217.194 13 -3 5 -9 2459.21 182.180 8 -3 5 -9 2747.28 200.898 10 3 5 9 2959.77 210.517 16 -3 5 -10 13783.5 543.753 13 -3 5 -10 13480.1 512.698 10 3 5 10 13615.0 525.168 16 -3 5 -10 12820.5 498.229 8 -3 5 -11 2547.56 210.843 13 -3 5 -11 2278.24 180.255 8 -3 5 -11 2627.76 194.098 10 3 5 11 2337.45 190.917 16 -3 5 -12 148.173 103.170 13 -3 5 -12 108.848 87.5176 10 -3 5 -12 53.1772 79.1548 8 3 5 12 114.293 87.2463 16 3 5 13 2404.63 174.799 23 -3 5 -13 2553.98 195.273 8 -3 5 -13 2776.47 205.688 13 3 5 13 2386.73 189.348 16 -3 5 -13 2453.44 183.495 10 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15 -4 1 -9 3269.29 145.892 15 -4 -1 -9 3248.90 137.810 4 4 1 9 3422.66 153.811 4 4 -1 9 3070.67 139.481 4 4 -1 9 2937.04 120.911 15 -4 -1 -9 2972.99 141.666 15 -4 -1 -10 35223.4 902.772 4 4 -1 10 34543.1 910.921 4 4 -1 10 30882.3 876.131 15 -4 -1 -10 30167.6 903.989 15 4 1 10 33981.4 922.105 4 4 -1 11 2523.73 168.213 7 4 1 11 2463.10 137.990 4 -4 1 -11 2549.96 144.855 19 4 1 11 2566.99 156.103 16 4 -1 11 2485.93 115.015 15 -4 1 -12 58358.1 1627.74 8 -4 1 -12 63670.7 1643.69 19 4 1 12 61745.8 1664.29 16 4 -1 12 58819.4 1678.86 7 4 -1 12 59896.6 1589.45 15 -4 1 -13 8405.59 324.116 8 -4 1 -13 9054.96 334.130 19 4 1 13 8435.13 347.461 16 4 -1 13 8208.85 360.521 7 -4 1 -14 3200.98 177.178 8 4 1 14 3114.73 191.278 12 -4 1 -14 2687.60 169.515 19 4 1 14 2909.61 191.084 16 4 1 15 135.668 71.4969 12 -4 1 -15 176.483 60.5696 8 4 1 15 137.594 76.2438 16 -4 1 -16 22094.3 720.203 8 4 1 16 22808.9 744.373 12 4 1 16 23437.3 740.486 23 4 1 16 22898.6 765.842 16 4 1 17 16841.4 576.548 23 -4 1 -17 16036.4 565.181 8 4 1 17 16210.6 579.957 12 4 1 17 15884.2 600.477 16 4 1 18 32675.4 1021.33 12 4 1 18 32851.4 1012.68 23 -4 1 -18 34027.5 1013.83 8 4 1 18 32894.9 1053.66 16 4 1 19 1248.92 141.627 23 4 1 19 1315.44 147.209 12 -4 1 -19 1038.84 125.315 8 4 1 19 1151.93 154.507 16 4 1 20 251.706 97.4575 12 4 1 20 275.408 104.014 16 4 1 20 315.248 93.7387 23 4 1 21 649.306 112.254 23 4 1 22 37562.8 1151.05 23 -4 -1 -22 37325.8 1180.47 18 -4 1 -23 74.1035 111.679 11 -4 -1 -23 80.5395 86.8531 11 -4 -1 -23-23.3570 75.9978 18 4 1 23 28.5332 66.9615 23 -4 -1 -24 82.6614 90.4982 11 -4 1 -24 155.606 111.103 11 -4 -1 -24 218.745 81.1220 18 -4 1 -24 206.238 116.464 18 4 1 24 192.780 78.2937 23 4 1 25 14.8064 60.9833 23 -4 1 -25 84.7979 102.785 11 -4 -1 -25 52.4456 82.8440 11 -4 -1 -25-4.90244 63.0772 18 -4 1 -25 55.0177 104.906 18 -4 -1 -26 15452.8 546.584 11 -4 1 -26 15217.5 566.707 11 4 1 26 14106.2 474.545 23 -4 1 -26 15671.8 561.077 18 -4 -1 -26 14429.7 510.387 18 4 1 27 639.798 68.4086 23 -4 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2 18 1336.02 139.997 3 4 2 -18 1466.13 183.742 11 -4 -2 18 1461.51 143.598 3 -4 -2 17 2105.68 166.926 3 -4 2 17 2184.87 168.239 3 -4 2 17 2380.49 175.983 23 4 2 -17 2251.68 214.555 11 -4 2 16 13302.8 486.857 3 -4 2 16 14038.8 503.356 23 4 2 -16 13468.9 566.235 11 -4 -2 16 13401.5 488.562 3 4 2 -15 4681.95 244.535 13 -4 -2 15 4827.15 243.553 3 -4 2 15 4616.88 238.205 3 -4 2 15 5314.32 259.871 23 4 2 -15 4856.76 298.781 11 -4 2 14 1111.07 120.647 23 4 2 -14 991.798 140.271 11 -4 -2 14 696.594 99.3187 3 -4 2 14 780.539 99.8134 3 4 2 -14 1077.71 111.275 13 4 2 -14 793.265 107.438 10 4 2 -13 202.527 64.0300 13 -4 2 13 116.698 67.0995 23 -4 -2 13 246.118 70.5253 3 -4 2 13 195.104 67.5328 3 4 2 -13 139.081 80.9988 11 4 2 -13 221.992 71.6412 10 -4 2 12 77598.2 2054.91 3 4 2 -12 76717.0 2142.48 11 -4 -2 12 75973.3 2056.92 3 -4 2 12 79235.6 2076.40 23 4 2 -12 76885.7 2074.97 13 4 2 -12 73270.6 2086.43 10 4 2 -11 55886.6 1533.84 13 4 2 -11 54100.5 1540.75 10 4 2 -11 54493.2 1589.96 11 -4 2 11 55804.5 1507.34 3 -4 2 11 55548.7 1528.16 23 -4 -2 11 55287.3 1511.65 3 4 2 -10 4484.89 229.153 10 4 2 -10 4730.64 225.432 13 4 2 -10 4566.89 255.089 11 4 2 -10 4039.03 211.151 1 -4 -2 9 83.6621 30.9790 14 4 2 -9 119.770 54.3056 13 -4 2 9 100.514 55.2682 23 4 2 -9 248.589 74.0230 11 4 2 -9 143.965 58.7070 10 -4 -2 8 27238.2 776.744 14 -4 -2 8 28177.2 775.510 4 -4 -2 7 1515.91 91.6147 14 -4 -2 7 1460.91 91.2712 4 -4 -2 6 9989.66 330.823 14 -4 -2 6 10604.5 342.451 6 -4 -2 6 10382.5 332.482 4 -4 -2 5 814.182 64.8453 14 4 2 -5 772.454 78.1522 5 -4 -2 5 713.753 68.8711 6 -4 -2 5 603.723 59.0787 4 4 -2 -5 552.753 22.1991 4 -4 -2 4 66501.5 1736.30 6 -4 -2 4 67798.0 1731.46 4 4 -2 -4 65381.8 1673.97 4 -4 -2 3 40777.8 1051.12 6 -4 -2 3 40525.6 1045.99 4 -4 2 3 39451.0 1037.82 1 -4 -2 3 40974.8 1041.35 1 4 -2 -3 40180.2 997.401 4 -4 -2 2 82200.6 2216.76 6 -4 2 2 85908.8 2208.93 1 4 -2 -2 87136.3 2174.93 4 -4 -2 2 86344.5 2210.14 1 -4 -2 2 83510.6 2214.72 4 -4 -2 1 122786. 3133.93 1 -4 2 1 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98.8943 4 4 -2 7 1409.41 88.4427 4 -4 2 -8 319.447 58.0589 19 4 2 8 242.446 57.8031 21 4 2 8 381.715 58.3316 4 4 -2 9 22422.2 706.040 7 4 2 9 22114.7 671.265 4 -4 2 -9 23000.9 671.326 8 -4 2 -9 21861.3 670.812 19 -4 2 -10 88316.9 2337.36 8 -4 2 -10 88561.2 2344.43 19 4 -2 10 87853.1 2377.55 7 -4 2 -11 47369.5 1321.09 19 4 2 11 46937.8 1327.77 23 -4 2 -11 47118.7 1314.03 8 4 -2 11 47131.5 1356.28 7 -4 2 -12 14990.1 505.503 8 4 2 12 14469.8 511.954 23 -4 2 -12 15183.9 508.615 19 4 2 12 14073.0 522.851 16 4 -2 12 15085.9 541.835 7 4 2 13 57273.6 1585.63 23 -4 2 -13 55512.1 1569.41 8 4 2 13 56338.2 1598.69 16 4 2 14 128443. 3412.84 23 -4 2 -14 129851. 3402.20 8 4 2 14 128099. 3431.63 16 4 -2 15 23206.9 771.883 12 -4 2 -15 25064.4 759.225 8 4 2 15 23741.8 778.686 16 4 -2 16 9901.21 434.289 12 -4 2 -16 10861.7 422.737 8 4 2 16 9558.74 429.086 16 4 -2 17 1287.57 160.510 12 -4 2 -17 1493.33 146.544 8 4 2 17 1250.22 154.708 16 -4 2 -18 9069.32 403.264 8 4 -2 18 9264.28 422.793 12 4 2 18 9161.82 406.274 23 -4 2 -18 10231.7 445.832 18 4 2 18 9287.89 434.276 16 4 -2 19 2249.07 199.268 12 -4 2 -19 2681.80 215.933 11 4 2 19 2198.44 188.476 23 4 2 19 2041.60 198.187 16 -4 2 -19 2290.49 187.202 8 -4 2 -19 2036.44 197.624 18 4 -2 20 3144.03 237.827 12 -4 2 -20 3129.43 243.703 11 -4 2 -20 3190.34 226.145 8 -4 2 -20 3219.59 244.656 18 4 2 20 3149.77 224.306 23 4 2 20 3245.66 241.472 16 4 2 21 128.321 100.362 23 4 -2 21 136.095 106.192 12 -4 2 -21 113.949 107.817 18 -4 2 -21 136.414 103.550 11 4 2 21 27.1160 104.763 16 4 -2 22 6410.08 336.748 12 -4 -2 -22 6397.45 326.859 11 4 2 22 6644.44 324.410 23 -4 2 -22 6668.88 357.588 18 -4 2 -22 6185.45 348.224 11 -4 -2 -23 18330.0 635.283 11 4 2 23 17005.7 609.525 23 -4 2 -23 18372.7 672.751 11 -4 2 -23 17853.0 667.141 18 -4 2 -24 48942.9 1434.67 11 -4 2 -24 48433.6 1435.18 18 -4 -2 -24 48851.2 1389.94 11 4 2 24 46691.5 1364.61 23 -4 -2 -25 5138.41 249.332 11 4 2 25 5271.13 241.762 23 -4 2 -25 5028.16 276.995 11 -4 2 -25 5122.53 284.442 18 4 2 26 111.342 61.4311 23 -4 2 -26 94.8154 70.9009 18 -4 2 -26 164.190 78.9650 11 4 2 27 2309.38 117.748 3 4 2 27 2434.60 127.727 23 -4 2 -27 2482.71 158.729 11 4 3 -26 3104.32 159.973 11 4 3 -26 3327.95 176.245 22 4 3 -25 55.7480 62.9783 22 4 3 -25 57.7487 60.4451 11 4 3 -24 9260.75 377.516 11 4 3 -24 8918.05 385.481 22 4 3 -23 46.6150 90.4081 22 4 3 -23 120.042 77.9699 11 4 3 -22 10249.4 458.171 22 4 3 -22 10410.5 447.847 11 4 3 -21 6747.32 357.521 22 4 3 -21 6384.60 345.531 11 4 3 -20 5019.58 308.152 11 4 3 -19 1236.26 133.801 13 4 3 -19 1560.14 181.530 11 4 3 -18 4590.28 259.865 13 4 3 -18 4853.08 304.026 11 4 3 -17 33382.6 1018.35 13 4 3 -17 33416.5 1079.33 11 4 3 -17 30858.9 1010.74 10 -4 3 16 691.568 118.970 23 4 3 -16 849.154 120.362 13 4 3 -16 948.657 144.678 11 4 3 -16 832.472 125.870 10 4 3 -15 6748.62 330.219 13 4 3 -15 6579.02 358.433 11 4 3 -15 5849.68 320.495 10 4 3 -14 63820.8 1804.64 13 4 3 -14 63088.3 1850.41 11 4 3 -14 63624.8 1810.76 10 4 3 -13 1909.02 167.503 13 4 3 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21410.4 756.809 10 6 3 -5 21785.3 753.490 11 -6 3 4 4578.91 208.369 8 6 3 -4 3835.22 237.244 11 6 3 -4 4286.51 238.694 21 6 3 -4 4079.82 249.286 22 6 3 -4 4750.02 267.856 10 6 3 -3 3786.36 228.202 11 6 3 -3 3811.37 238.783 13 -6 3 3 3920.91 192.519 8 6 3 -3 4252.24 249.004 10 6 3 -2 16746.0 609.871 13 -6 3 2 17417.0 539.782 8 6 3 -2 16612.0 585.201 11 6 3 -2 16185.2 607.639 10 6 3 -1 3570.22 229.637 13 -6 3 1 3677.59 182.787 8 6 3 -1 3605.95 226.961 10 6 3 0 991.451 125.471 10 6 3 0 919.853 126.512 9 6 3 0 948.819 124.159 13 -6 3 0 1046.43 96.3949 8 6 3 1 11918.3 469.074 9 6 3 1 11009.9 457.429 13 -6 3 -1 11274.3 396.355 8 6 3 1 11290.7 452.348 10 6 3 2 74017.5 2108.71 9 -6 3 -2 77949.6 2023.39 8 6 3 2 78236.6 2101.48 24 6 3 2 70868.9 2079.23 10 6 3 3 230.024 83.7907 9 -6 3 -3 357.019 67.2745 8 6 3 3 288.522 90.3167 24 6 3 4 45693.1 1343.42 9 -6 3 -4 44811.8 1257.71 8 -6 3 -4 44455.9 1248.63 19 6 3 4 44981.1 1328.76 24 6 3 5 1804.43 167.119 9 -6 3 -5 1631.95 126.067 8 6 3 5 1757.08 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6001.39 311.778 8 -6 3 -14 6886.02 307.167 10 6 3 14 5376.73 318.384 16 -6 3 -15 1703.79 140.930 10 6 -3 15 1421.65 161.271 12 6 3 15 1602.94 163.418 23 -6 3 -15 1577.48 162.435 8 -6 3 -15 1279.12 142.183 18 6 3 15 1456.77 168.894 16 6 -3 16 24799.6 822.824 12 6 3 16 24540.3 820.165 23 -6 3 -16 24809.4 819.717 8 -6 3 -16 23789.8 815.250 18 6 3 16 25017.3 841.457 16 6 -3 17 21281.3 750.449 12 -6 3 -17 22043.4 757.056 8 6 3 17 23194.5 766.444 23 -6 3 -17 22661.0 764.514 18 6 3 17 22390.4 780.091 16 6 -3 18 8756.06 395.088 12 6 3 18 9445.84 406.440 23 -6 3 -18 9425.59 407.443 18 -6 3 -18 8545.31 394.038 8 6 3 18 9110.91 419.287 16 6 -3 19 4861.08 270.870 12 6 3 19 5420.58 282.061 23 -6 3 -19 4806.13 276.323 8 -6 3 -19 4970.35 277.459 18 6 3 19 4683.61 286.987 16 6 -3 20 4072.51 234.451 12 6 3 20 4057.14 235.743 23 -6 3 -20 4342.96 244.740 8 -6 3 -20 3357.59 226.400 18 6 3 20 4252.41 259.083 16 6 -3 21 1047.84 122.644 12 6 3 21 950.129 122.834 23 -6 3 -21 804.763 113.857 18 6 3 21 844.239 131.419 16 6 3 22 770.332 105.693 23 -6 3 -22 580.778 97.2239 18 6 3 22 592.667 104.379 16 -6 3 -23 3276.85 164.885 13 6 3 23 2819.51 169.420 23 -6 3 -23 3175.53 180.624 18 -6 3 -24 2939.62 140.187 13 6 4 -22 322.215 52.3852 21 6 4 -21 39.2274 54.1969 22 6 4 -21-14.5087 44.4657 21 6 4 -20-4.18732 58.6731 22 6 4 -20 45.8048 53.7734 21 6 4 -19 556.717 83.6175 13 6 4 -19 533.029 97.3504 22 6 4 -19 564.167 92.6271 21 6 4 -18 1617.16 154.057 22 6 4 -18 1827.85 147.020 13 6 4 -18 1465.51 135.119 11 6 4 -18 2020.43 156.751 21 6 4 -17 30.4232 69.6626 13 6 4 -17 102.858 73.5417 22 6 4 -17 90.5217 68.7389 11 6 4 -17 67.4881 76.9205 21 6 4 -16 10000.1 416.312 13 6 4 -16 9739.25 428.227 22 6 4 -16 9317.09 405.817 11 6 4 -16 10031.6 421.057 21 6 4 -15 9058.99 382.353 9 6 4 -15 8840.31 398.059 13 6 4 -15 8791.43 406.174 22 6 4 -15 9535.52 408.662 21 6 4 -14 3270.55 219.317 9 6 4 -14 3062.98 225.133 21 6 4 -14 3203.64 229.139 13 6 4 -14 3000.83 229.386 22 6 4 -13 3031.46 230.983 13 6 4 -13 3160.41 239.485 22 6 4 -13 3576.51 247.591 21 6 4 -12 274.071 121.330 10 6 4 -12 206.621 96.3128 13 6 4 -12 276.872 106.264 22 6 4 -12 288.015 108.957 21 6 4 -11 119.982 111.626 10 6 4 -11 128.202 101.754 13 6 4 -11 173.850 95.0888 22 6 4 -11 155.341 103.561 21 6 4 -10 682.608 130.190 13 6 4 -10 532.246 119.360 21 6 4 -10 588.892 120.014 22 6 4 -10 915.495 150.318 10 6 4 -9 1324.99 164.835 13 6 4 -9 1267.69 154.942 21 6 4 -9 1175.71 153.093 22 6 4 -9 1443.23 180.506 10 6 4 -8 5377.56 316.340 13 6 4 -8 5010.84 298.244 21 6 4 -8 5129.99 302.394 22 6 4 -7 12.8768 84.2678 21 6 4 -6 15417.2 587.668 21 6 4 -6 14783.1 606.630 10 6 4 -5 26247.6 875.496 13 6 4 -5 24720.4 879.549 10 6 4 -5 25689.8 853.494 21 6 4 -4 30198.9 1011.65 13 6 4 -4 30222.0 980.746 21 6 4 -4 32407.9 1029.36 10 6 4 -3 3445.96 251.335 13 -6 4 3 3468.04 187.612 8 6 4 -3 3161.36 226.676 21 6 4 -3 3592.73 255.406 10 6 4 -2 800.142 134.287 13 -6 4 2 862.891 94.4116 8 6 4 -2 885.901 127.608 21 6 4 -2 815.079 136.904 10 6 4 -1 1406.95 167.446 13 -6 4 1 1540.55 122.560 8 6 4 -1 1505.55 156.476 21 6 4 -1 1464.51 165.436 10 6 4 0 676.541 120.593 10 6 4 0 549.333 109.384 24 6 4 0 782.585 138.319 9 6 4 0 614.680 125.493 13 6 4 0 457.507 108.570 21 -6 4 0 637.216 87.4196 8 6 4 1 4635.35 291.316 9 6 4 1 4338.65 277.744 13 -6 4 -1 4203.45 219.374 8 6 4 1 4815.96 272.496 24 6 4 1 4567.58 264.878 21 6 4 1 4037.80 264.061 10 6 4 2 726.848 120.752 10 6 4 2 844.816 145.229 9 6 4 2 911.757 126.204 24 6 4 2 973.641 131.025 21 -6 4 -2 727.154 95.6750 8 6 4 3 28.7113 89.6299 9 6 4 3 59.9358 72.9737 24 6 4 3 5.89152 80.0920 21 -6 4 -3 58.3434 54.5548 8 6 4 4 21103.9 755.343 9 -6 4 -4 21101.2 669.077 8 6 4 4 20892.4 716.532 21 6 4 4 19231.7 702.942 24 6 4 5 1203.10 140.249 24 6 4 5 1186.44 154.222 9 -6 4 -5 1204.07 121.736 8 6 4 5 1122.61 140.756 21 6 4 6 11589.6 500.252 9 -6 4 -6 11314.3 441.588 8 6 4 6 11773.1 481.322 21 6 4 7 3812.64 262.084 9 -6 4 -7 3949.42 228.111 8 6 4 7 3706.99 247.685 21 6 4 8 4322.40 273.432 9 -6 4 -8 4210.71 243.215 8 -6 4 -9 1782.75 161.983 8 -6 4 -10 10545.7 434.466 8 6 4 11 763.525 117.997 23 -6 4 -11 703.154 117.821 8 -6 4 -11 940.139 129.917 10 6 4 12 6531.73 325.952 23 -6 4 -12 6350.83 326.060 8 6 4 12 5738.98 333.146 16 6 4 13 2868.60 204.521 23 -6 4 -13 2232.00 191.803 8 -6 4 -13 2476.26 181.289 10 6 4 14 658.643 116.786 23 -6 4 -14 912.270 132.146 8 -6 4 -14 773.060 106.276 10 6 4 15 2172.59 179.489 23 -6 4 -15 2101.01 181.489 8 -6 4 -15 2000.30 149.844 10 6 4 16 3044.79 206.249 23 -6 4 -16 2833.81 172.708 10 6 4 17 245.220 96.6754 23 -6 4 -17 330.248 66.3754 10 6 4 18 56.3434 77.2501 23 6 4 19 144.142 72.3477 23 -6 4 -19 32.5643 80.3854 8 -6 4 -20 4125.66 208.500 13 6 4 20 3833.32 197.526 23 -6 4 -21 7071.26 277.299 13 6 4 21 6927.60 269.585 23 -6 4 -22 1260.49 93.2892 13 6 4 22 970.140 81.9980 23 6 5 -17 863.241 95.3739 13 6 5 -17 863.113 82.5997 21 6 5 -16 227.004 71.3410 13 6 5 -16 206.837 63.1689 21 6 5 -15 1264.86 114.792 9 6 5 -15 1318.98 132.229 13 6 5 -15 1374.73 123.685 21 6 5 -14 4111.75 225.434 9 6 5 -14 4340.39 244.398 13 6 5 -14 4141.35 229.734 21 6 5 -13 70.3644 73.4884 9 6 5 -13 32.2603 85.7229 13 6 5 -13 115.320 73.9685 21 6 5 -12 8756.82 386.253 9 6 5 -12 8650.01 391.904 13 6 5 -12 8606.41 385.145 21 6 5 -11 880.817 128.440 9 6 5 -11 793.434 139.462 13 6 5 -11 690.217 122.082 21 6 5 -10 156.199 118.910 10 6 5 -10 203.610 98.1007 9 6 5 -10 228.302 103.221 21 6 5 -9 6894.58 346.466 21 6 5 -8-85.1723 116.927 10 6 5 -8-20.2513 104.287 13 6 5 -8 25.1690 83.7321 21 6 5 -7 1739.15 186.263 13 6 5 -7 1841.02 177.759 21 6 5 -7 1718.12 195.125 10 6 5 -6 7356.24 377.556 13 6 5 -6 6850.47 355.720 21 6 5 -6 7234.69 379.721 10 6 5 -5 446.729 128.512 10 6 5 -5 664.899 134.293 13 6 5 -5 693.129 124.427 21 6 5 -4 1243.23 170.700 10 6 5 -4 1315.64 175.441 13 6 5 -4 1138.18 152.728 21 -6 5 4 1349.36 131.958 10 6 5 -3 905.045 148.182 10 6 5 -3 871.237 157.974 9 6 5 -3 682.850 141.104 13 6 5 -3 747.746 130.291 21 -6 5 3 844.218 117.344 10 6 5 -2 2249.24 219.008 9 6 5 -2 2169.18 202.822 13 6 5 -2 1928.27 181.360 21 -6 5 2 2456.06 190.737 10 6 5 -2 1987.95 194.489 10 6 5 -1 6911.09 380.056 9 6 5 -1 6707.88 343.105 21 -6 5 1 7337.62 354.883 10 6 5 -1 6046.76 348.761 10 6 5 0 5567.70 341.400 9 6 5 0 5321.45 305.030 21 -6 5 0 6246.12 326.938 10 6 5 1 884.158 155.590 9 6 5 1 1058.05 148.902 21 -6 5 -1 1199.62 158.544 10 6 5 2 2034.75 202.895 9 -6 5 -2 1688.46 140.332 8 6 5 2 1474.80 162.131 21 -6 5 -2 1837.92 187.830 10 6 5 3 2726.31 224.795 9 -6 5 -3 2449.53 172.881 8 6 5 3 2710.45 205.668 21 -6 5 -3 3129.76 234.143 10 6 5 4 2146.84 198.900 9 -6 5 -4 2167.84 163.989 8 6 5 4 1976.48 184.853 21 -6 5 -4 2535.16 208.041 10 6 5 5 4961.88 303.952 9 -6 5 -5 4831.25 255.781 8 -6 5 -5 5616.89 314.304 10 -6 5 -6 1157.27 132.919 13 6 5 6 1434.78 164.215 9 -6 5 -6 1460.70 166.531 10 -6 5 -6 1237.49 134.366 8 -6 5 -7 1590.88 157.114 13 6 5 7 2151.90 184.680 9 -6 5 -7 2003.45 157.914 8 -6 5 -8 247.535 80.1979 8 -6 5 -9 62.9424 76.0236 8 -6 5 -9 109.014 89.9755 10 -6 5 -10 285.998 86.0996 8 6 5 10 166.772 93.9433 16 -6 5 -10 305.391 89.5912 10 -6 5 -11 593.951 110.623 13 -6 5 -11 957.084 121.697 8 6 5 11 791.690 128.416 16 -6 5 -11 871.786 113.744 10 -6 5 -12 11413.4 468.221 13 -6 5 -12 11796.8 449.496 8 -6 5 -12 12153.0 440.853 10 6 5 12 11608.6 463.992 16 -6 5 -13 7400.07 342.182 13 -6 5 -13 7199.97 325.805 8 -6 5 -13 7538.01 313.885 10 6 5 13 7397.10 340.708 16 -6 5 -14 120.716 78.1542 13 -6 5 -14 87.5642 71.3887 8 6 5 14 67.5951 82.8844 16 -6 5 -14 80.7253 58.9699 10 -6 5 -15 7176.55 312.145 13 -6 5 -15 6436.97 293.288 8 -6 5 -15 6586.41 271.932 10 6 5 15 7105.30 315.560 16 -6 5 -16 83.4745 61.6678 13 -6 5 -16 61.9057 60.0259 8 6 5 16 45.3165 70.7062 16 -6 5 -16 24.9218 43.6500 10 6 5 17 4130.19 211.929 16 -6 5 -18 35.8698 46.1856 13 6 5 18 25.4999 52.3295 16 -6 5 -19 479.331 65.1043 13 6 5 19 565.309 72.4144 16 6 6 -12 1306.00 101.839 9 6 6 -11 3509.66 184.475 9 6 6 -10 1060.49 111.797 9 6 6 -9 941.391 110.065 9 6 6 -8 1916.47 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10.4949 63.8986 11 7 0 -7 166271. 4416.46 11 -7 0 7 171538. 4326.97 6 7 0 -7 165413. 4398.34 22 -7 0 6 10.4148 38.7417 6 7 0 -6 36.2757 59.0167 22 7 0 -6 43.4997 60.7235 11 -7 0 5 55698.7 1444.37 6 7 0 -5 50200.9 1510.61 11 -7 0 4 31.7534 23.9926 15 -7 0 3 9318.69 330.926 5 7 0 -3 9367.14 297.619 4 7 0 -2 3.24536 24.3701 4 -7 0 2 6.60465 24.7972 4 -7 0 1 26357.8 798.326 5 7 0 -1 27564.5 766.223 4 7 0 0 10.9482 24.9345 4 -7 0 0 22.7337 28.0644 4 -7 0 0-2.75601 42.5784 5 -7 0 -1 38896.2 1068.78 5 7 0 1 37651.6 1029.40 4 -7 0 -1 40664.1 1039.17 4 -7 0 -1 37047.5 1005.70 15 -7 0 -2 5.12909 20.2070 15 7 0 2 3.88711 29.6615 4 -7 0 -2 34.4165 33.0979 4 -7 0 -2 14.8924 41.9381 5 7 0 3 79499.8 2091.16 4 -7 0 -3 81292.6 2102.99 4 7 0 4 35.0013 27.1594 4 7 0 5 39134.0 1062.18 4 -7 0 -5 38573.7 1082.29 20 -7 0 -6 8.86007 44.1302 20 -7 0 -7 124436. 3235.32 20 -7 0 -8 55.9697 48.4432 20 7 0 9 2046.19 164.261 7 7 0 10 56.4711 74.0304 7 7 0 11 1001.38 124.403 7 7 0 12 16.8463 73.9111 7 -7 0 -12 33.4624 53.8578 19 -7 0 -13 18774.1 608.000 19 7 0 13 18713.7 666.536 7 7 0 14-24.5084 84.5779 7 -7 0 -14 12.2939 53.6351 19 -7 0 -15 58227.0 1646.88 19 7 0 15 61520.0 1735.21 7 -7 0 -16 48.4442 63.5075 19 -7 0 -17 9529.47 380.483 19 7 0 18-37.7979 97.7186 12 7 0 19 27881.8 900.470 12 7 0 19 26335.6 852.800 23 7 0 20 12.0372 93.3545 12 7 0 20-9.78962 77.4270 23 7 0 21 29335.8 915.434 12 7 0 21 27265.2 867.046 23 7 0 22 88.1442 73.4473 23 7 0 22 37.0817 91.8089 12 7 0 23 19196.0 639.293 12 7 0 23 18064.2 592.116 23 -7 0 -24 70.6716 73.7906 18 7 0 24 24.9366 49.1262 23 -7 0 -25 1104.70 131.592 11 7 0 25 913.393 80.8275 23 -7 0 -25 1148.99 123.510 18 -7 0 -26-45.5457 65.4969 11 -7 0 -26 11.0936 54.2951 18 -7 0 -27 19066.9 572.133 11 -7 0 -27 17043.3 548.007 18 7 1 -27 478.815 66.2580 11 7 1 -26 1916.37 128.122 22 7 1 -26 2135.02 146.887 11 7 1 -25 390.864 81.2024 22 7 1 -25 348.522 89.1100 11 -7 -1 25 364.915 52.4373 17 7 1 -24 3912.59 230.728 22 7 1 -24 4047.42 247.373 11 7 1 -23 9205.84 407.124 22 7 1 -23 10195.0 444.386 11 7 -1 -23 9248.53 376.271 11 7 1 -22 2613.12 228.864 11 7 -1 -22 2421.41 181.996 11 7 1 -22 2489.85 203.662 22 7 1 -21 28828.8 963.242 11 7 1 -21 27248.2 932.392 22 7 -1 -21 27670.1 898.755 11 7 1 -20 2855.16 244.511 11 7 -1 -20 2751.99 211.426 11 7 1 -20 3056.70 247.749 22 -7 -1 20 2939.37 204.638 3 7 1 -19 3254.81 268.551 11 7 -1 -19 3044.77 227.303 11 7 1 -19 3010.98 250.449 22 -7 -1 19 3551.24 224.508 3 -7 1 19 3243.20 221.885 3 7 1 -18 1800.89 203.455 11 7 -1 -18 1758.88 179.032 11 7 1 -18 2155.46 212.807 22 -7 -1 18 2239.47 182.615 3 -7 1 18 2065.14 176.356 3 7 -1 -17 1167.79 148.016 11 7 1 -17 1386.94 174.784 22 7 1 -17 904.034 161.075 11 -7 -1 17 952.158 133.125 3 -7 1 17 1055.75 136.538 3 7 1 -16 2828.31 237.294 22 7 1 -16 3501.51 268.538 11 7 -1 -16 2841.11 217.768 11 -7 1 16 3144.30 210.705 3 -7 -1 16 3139.76 212.005 3 -7 1 15 19126.4 640.398 3 7 1 -15 17594.3 684.734 22 7 1 -15 17460.8 704.040 11 7 -1 -15 17225.7 655.698 11 -7 -1 15 18530.4 628.745 3 7 1 -14 10435.1 476.210 11 7 -1 -14 9650.88 437.355 11 7 1 -14 10674.3 471.588 22 -7 -1 14 10317.3 415.644 3 -7 1 14 10245.9 413.170 3 7 1 -13 67691.3 2028.74 11 7 -1 -13 68169.0 1979.25 11 7 1 -13 70834.7 2023.97 22 -7 -1 13 70462.3 1940.63 3 -7 1 13 73596.1 1945.96 3 7 1 -12 10470.5 479.932 11 7 -1 -12 11244.3 459.893 11 -7 -1 12 11166.0 430.244 3 7 1 -12 11766.2 488.726 22 -7 1 12 11783.7 435.632 3 7 1 -11 2098.06 192.377 11 7 -1 -11 2459.31 184.628 11 -7 1 11 2499.97 149.069 17 7 -1 -10 6164.82 298.156 11 7 1 -10 5896.60 311.561 22 -7 1 10 5853.43 246.485 17 7 1 -9 31861.7 1011.87 22 7 -1 -9 32797.2 988.615 11 -7 1 9 32299.2 924.037 17 7 1 -8 5427.07 256.404 13 7 -1 -8 5968.68 279.346 11 7 1 -8 5776.08 295.822 22 -7 1 8 5558.63 234.263 17 7 -1 -7 1765.25 141.101 11 7 1 -7 1691.44 152.300 22 -7 1 7 1698.25 117.207 17 -7 1 6 1645.94 98.0848 6 -7 -1 6 1745.48 118.673 6 7 1 -6 2082.71 163.065 22 -7 1 6 1780.46 117.628 17 -7 -1 5 24945.2 718.889 6 -7 1 5 24725.4 689.530 6 7 1 -5 23564.5 778.942 22 -7 1 5 23361.7 706.017 17 7 1 -4 26502.7 894.700 22 -7 -1 4 30340.3 803.104 4 -7 1 3 14813.7 445.951 5 7 1 -3 14688.2 527.856 11 -7 -1 3 14152.3 431.079 4 -7 1 2 23375.1 664.194 5 -7 -1 2 23555.0 707.176 1 -7 1 2 22916.2 701.953 1 7 1 -2 22389.0 741.645 11 -7 -1 2 23808.8 650.997 4 -7 -1 2 21414.5 677.035 17 -7 1 1 177328. 4488.88 5 7 1 -1 182821. 4483.14 4 7 1 -1 170446. 4573.32 11 7 -1 -1 168290. 4448.78 4 -7 -1 1 175876. 4473.04 4 -7 -1 1 179701. 4535.02 1 -7 1 1 177483. 4530.73 1 -7 1 0 15080.1 467.657 5 -7 1 0 14958.5 497.001 1 7 1 0 15250.7 459.685 4 7 1 0 14901.8 532.351 11 7 -1 0 15575.0 439.322 4 -7 -1 0 14452.1 494.911 1 -7 -1 0 15077.6 454.846 4 7 1 1 42281.5 1326.86 9 -7 -1 -1 47157.1 1292.91 5 7 1 1 45582.5 1339.40 11 7 1 1 48517.3 1265.12 4 7 -1 1 46782.2 1239.98 4 -7 -1 -1 48477.9 1314.72 1 -7 1 -1 47739.8 1310.51 1 -7 -1 -1 46423.6 1258.27 4 -7 1 -1 47422.1 1273.96 5 -7 1 -2 5703.88 231.435 8 7 1 2 5930.10 279.280 11 -7 -1 -2 6010.15 249.186 5 7 1 2 5877.20 225.951 4 -7 1 -2 6226.47 244.038 20 7 -1 2 5732.22 209.234 4 -7 1 -3 14478.7 448.088 8 7 1 3 13296.3 495.971 24 -7 1 -3 12841.4 445.843 20 7 -1 3 14186.2 423.483 4 7 1 3 14773.9 446.781 4 7 1 3 14918.1 509.796 11 -7 -1 -3 15412.5 475.234 5 -7 -1 -3 13211.3 428.510 15 -7 -1 -4 40.0655 31.5074 15 7 -1 4 16.5551 26.9500 4 7 1 4 37.0186 68.2495 24 -7 -1 -4 65.8420 45.6202 5 -7 1 -4 39.9291 40.2983 8 -7 1 -4 83.1568 48.7616 20 -7 1 -5 70603.2 1815.88 8 7 1 5 69014.0 1888.88 24 -7 -1 -5 69277.9 1817.11 20 -7 1 -5 68917.1 1825.05 20 7 -1 5 65978.3 1791.99 4 -7 -1 -5 66619.5 1794.35 15 -7 1 -6 3575.09 167.212 8 7 1 6 3343.82 207.204 24 -7 -1 -6 3398.76 166.307 20 -7 1 -6 3021.54 167.807 20 7 1 7 38412.5 1125.37 24 -7 1 -7 38048.1 1046.58 8 7 1 7 37789.2 1064.68 21 7 1 7 35265.8 1089.98 2 7 -1 7 36085.1 1094.88 2 -7 -1 -7 38175.6 1046.39 20 7 1 8 2851.11 186.136 2 7 -1 8 2919.28 188.645 2 -7 1 -8 2874.57 152.667 8 -7 -1 -8 2766.04 150.078 20 7 1 8 2712.81 179.265 7 7 1 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41196.4 1151.09 8 -8 -1 -7 42924.0 1157.32 20 8 1 7 42229.9 1243.77 24 8 1 7 38574.9 1204.39 2 8 -1 7 38913.1 1208.40 2 8 1 8 7491.81 350.364 2 8 -1 8 7196.95 348.479 2 -8 1 -8 8387.03 312.153 8 -8 -1 -8 8629.39 316.613 20 8 1 8 7796.00 348.438 7 8 1 9 2434.72 190.720 2 8 -1 9 2390.59 190.619 2 -8 1 -9 2695.69 158.617 8 -8 -1 -9 3089.14 166.443 20 8 1 9 2829.39 193.997 7 8 1 10 55479.7 1593.80 2 8 -1 10 54879.1 1596.69 2 -8 1 -10 55620.8 1521.51 8 8 1 10 55228.3 1583.22 7 8 1 11 2203.98 183.343 2 8 -1 11 1971.90 179.160 2 -8 1 -11 1972.80 139.030 8 -8 1 -11 2219.44 160.176 19 8 1 11 2116.39 159.036 16 8 1 11 1917.55 167.674 7 8 1 12 113.602 87.0082 2 8 -1 12 6.05325 82.7197 2 8 1 12 67.9656 76.5971 7 -8 1 -12 27.1221 51.2932 8 -8 -1 -12 58.2220 48.9618 19 -8 1 -12 9.33221 61.0837 19 8 1 12 107.323 68.3642 16 -8 1 -13 4848.52 241.018 8 -8 -1 -13 5233.12 239.719 19 -8 1 -13 5437.99 270.651 19 8 1 13 5620.37 277.513 16 8 1 13 5253.62 288.558 7 -8 1 -14 9550.77 368.269 8 -8 -1 -14 8959.55 348.828 19 -8 1 -14 9009.54 387.718 19 8 1 14 9395.81 391.281 16 8 -1 14 8117.55 421.780 7 8 1 14 9787.20 415.714 7 -8 1 -15 1832.46 145.692 8 -8 1 -15 1827.00 161.009 19 8 1 15 2037.27 165.920 16 8 -1 15 1903.36 193.697 7 8 1 16 243.803 98.5488 12 -8 1 -16 506.393 101.675 19 -8 1 -16 210.461 63.6846 8 8 1 16 411.772 93.2788 16 8 1 17-16.7192 84.6979 12 -8 1 -17-15.3790 74.5920 19 8 1 17 61.4655 70.6264 16 8 -1 18 17483.4 672.263 12 8 1 18 17882.6 636.239 12 8 1 18 18556.2 646.966 23 8 1 18 18489.2 639.842 16 8 -1 19-37.7713 105.899 12 8 1 19 81.8741 80.6435 12 8 1 19 117.329 95.3383 23 8 -1 20 250.170 117.300 12 8 1 20 269.538 87.9629 12 8 -1 20 206.360 74.0617 23 8 1 20 216.202 90.3294 23 8 -1 21 6245.52 323.136 12 8 1 21 6153.23 283.030 12 8 -1 21 6022.00 262.648 23 8 1 21 6554.54 299.634 23 8 -1 22 3611.96 227.774 12 8 -1 22 3570.04 177.364 23 8 1 22 3703.21 210.265 23 8 -1 23 722.614 113.110 12 8 1 23 873.023 103.765 23 -8 1 -23 812.915 121.005 11 -8 1 -23 888.342 121.297 18 -8 -1 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463.868 11 8 2 -11 9689.64 456.931 22 8 2 -10 17902.3 653.805 13 8 2 -10 19422.2 711.924 11 8 2 -10 18328.0 700.239 22 8 2 -9 438.042 90.0155 9 8 2 -9 551.780 104.438 13 8 2 -9 511.632 120.784 11 8 2 -8 13179.7 502.984 9 8 2 -8 12652.8 505.856 13 8 2 -8 13254.5 550.437 11 8 2 -8 13249.7 543.261 22 8 2 -7 61500.6 1747.85 9 8 2 -7 61495.2 1759.71 13 8 2 -7 62457.8 1800.56 11 8 2 -7 60816.2 1790.61 22 8 2 -6 18851.6 658.394 9 8 2 -6 18271.8 693.604 11 8 2 -6 19059.8 691.611 22 8 2 -5 2836.26 206.214 9 8 2 -5 3296.29 234.496 11 8 2 -4 1406.53 159.877 11 8 2 -4 1145.51 125.411 21 -8 2 4 1119.14 105.709 20 8 2 -3 28223.9 902.702 9 8 2 -3 27999.6 869.527 21 -8 2 3 27231.1 825.611 20 8 2 -3 27974.0 924.459 11 -8 -2 3 28706.3 840.575 17 8 2 -2 54908.0 1632.55 9 -8 2 2 58592.1 1567.05 8 -8 2 2 55297.6 1550.91 20 8 2 -2 57759.4 1655.95 11 8 2 -2 57138.0 1597.41 21 -8 -2 2 57029.9 1563.32 17 8 2 -1 21507.5 728.866 9 -8 2 1 21074.1 654.526 8 8 2 -1 21602.3 735.554 11 8 2 -1 20430.1 679.008 21 -8 2 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18030.6 665.547 7 8 2 8 10825.1 430.573 2 8 -2 8 10406.8 425.652 2 -8 2 -8 11040.8 403.631 8 8 2 8 11161.7 432.184 21 -8 2 -8 10015.5 403.673 19 8 -2 8 10778.2 467.741 7 -8 2 -9 2458.14 164.411 8 8 2 9 2417.39 181.717 2 8 -2 9 2306.91 177.776 2 -8 2 -9 2562.11 177.345 19 8 -2 9 2222.59 203.018 7 8 -2 10 8770.60 383.995 2 -8 2 -10 8779.53 355.884 8 -8 2 -10 9152.76 372.008 19 8 2 10 7977.49 372.105 2 8 -2 10 9103.05 417.991 7 -8 2 -11 4094.49 225.895 8 -8 2 -11 3591.26 223.173 19 8 -2 11 4307.62 275.170 7 -8 2 -12 23339.4 750.033 8 -8 2 -12 22573.5 764.768 19 8 2 12 24389.8 793.181 16 8 -2 12 23294.8 823.954 7 -8 2 -13 64600.0 1743.48 8 8 2 13 65126.4 1792.53 16 8 -2 13 64512.7 1829.58 7 -8 2 -14 9636.80 395.990 8 8 2 14 9351.24 420.821 16 8 -2 14 9450.54 450.189 7 8 2 15 4431.47 268.292 23 -8 2 -15 4406.88 247.471 8 8 2 15 4599.82 277.736 16 8 -2 15 4048.94 280.657 7 8 2 16 19611.1 693.252 23 -8 2 -16 20219.7 680.667 8 8 2 16 20084.8 712.834 16 8 -2 17 6273.89 344.444 12 8 2 17 6527.49 329.039 23 -8 2 -17 6369.41 306.625 8 8 2 17 6945.85 343.261 16 8 -2 18 3908.94 260.783 12 8 2 18 3851.00 242.673 23 -8 2 -18 4165.34 235.401 8 8 2 18 4302.53 258.581 16 8 -2 19 3580.32 247.502 12 -8 2 -19 4039.08 226.321 8 8 2 19 4002.29 246.961 23 8 2 19 4358.23 255.641 16 8 -2 20 10114.2 421.173 12 -8 2 -20 9619.29 379.459 8 -8 2 -20 9772.81 414.398 18 8 2 20 9166.28 399.965 16 8 -2 21 587.497 111.755 12 -8 2 -21 615.215 102.694 11 -8 2 -21 563.638 101.609 18 8 -2 22 490.765 103.329 12 8 2 22 343.136 88.8495 23 -8 2 -22 453.812 87.0620 11 -8 -2 -22 409.037 68.7836 18 -8 2 -22 446.597 94.3467 18 8 -2 23 1515.91 133.460 12 -8 -2 -23 1544.48 120.859 11 -8 2 -23 1513.06 125.353 11 8 2 23 1678.81 126.286 23 -8 2 -23 1614.22 134.366 18 8 2 24 15763.6 480.684 23 -8 2 -24 15375.6 502.786 18 -8 -2 -24 14575.9 472.709 11 8 2 25 710.182 66.1853 23 -8 2 -25 684.892 71.0696 18 8 3 -23 1205.98 95.3427 11 8 3 -23 1283.10 90.3439 21 -8 -3 23 1115.92 80.2493 17 8 3 -22 5718.05 252.105 11 8 3 -22 5706.68 236.739 21 8 3 -21 867.794 108.315 11 8 3 -21 819.517 111.430 22 8 3 -20 1186.86 132.334 11 8 3 -20 1196.70 134.529 22 8 3 -19 1304.92 144.801 22 8 3 -19 1184.37 139.186 11 8 3 -18 8789.14 408.599 22 8 3 -18 8789.67 401.563 11 8 3 -17 8690.89 414.709 11 8 3 -17 10059.4 441.164 22 8 3 -16 5639.33 318.152 11 8 3 -16 5462.12 328.199 22 8 3 -15 11980.4 514.392 11 8 3 -15 11644.9 518.091 22 8 3 -14 5.91191 72.4385 13 8 3 -14 59.2779 106.833 22 8 3 -14 14.5761 93.2205 11 -8 3 13 22815.1 710.883 8 8 3 -13 22220.3 781.228 13 8 3 -13 22614.4 816.719 11 8 3 -13 23119.5 823.914 22 8 3 -12 14083.2 538.089 9 -8 3 12 14589.3 503.299 8 8 3 -12 14362.2 565.045 13 8 3 -12 13972.8 586.476 11 8 3 -12 14055.0 592.777 22 8 3 -11 6401.10 326.450 9 -8 3 11 6544.79 292.075 8 8 3 -11 6069.38 338.117 13 8 3 -11 6367.21 361.754 11 8 3 -11 6260.23 361.862 22 8 3 -10 8220.84 387.231 9 -8 3 10 8384.74 345.764 8 8 3 -10 8538.48 405.304 13 8 3 -10 8187.85 415.989 11 8 3 -10 7632.94 412.839 22 8 3 -9 1153.36 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8 3 7 51575.1 1475.32 21 -8 3 -7 51037.8 1422.69 19 8 -3 7 49616.0 1474.28 7 8 3 8 25108.5 843.531 23 8 3 8 26353.8 868.868 21 -8 3 -8 26472.0 829.064 19 8 -3 8 27099.6 880.154 7 8 3 9 35279.3 1069.41 23 8 -3 9 32623.6 1076.67 7 -8 3 -9 35065.5 1041.82 19 -8 3 -10 72684.9 2088.30 8 8 3 10 76058.9 2116.01 23 -8 3 -10 76830.9 2094.96 19 8 -3 10 78354.7 2150.45 7 8 3 11 1302.73 146.182 23 -8 3 -11 1338.39 144.548 8 -8 3 -11 1547.67 146.966 19 8 -3 11 1232.89 159.093 7 8 -3 12 546.027 122.054 7 8 3 12 670.425 115.922 23 -8 3 -12 650.593 116.443 8 -8 3 -12 683.521 108.323 19 8 3 13 6192.84 322.178 23 -8 3 -13 6546.76 311.986 8 8 3 13 6467.60 336.774 16 8 -3 13 5725.72 325.295 7 8 3 14 4468.55 268.750 23 -8 3 -14 5267.86 284.288 8 8 3 14 5051.81 297.028 16 8 -3 15 2952.22 222.666 12 8 3 15 2929.17 212.883 23 -8 3 -15 3566.73 223.291 8 -8 3 -15 3495.59 200.844 10 8 3 15 2995.63 228.240 16 8 -3 16 1724.26 171.154 12 8 3 16 1968.31 176.749 23 -8 3 -16 1972.83 170.163 8 -8 3 -16 1880.44 159.402 18 8 3 16 1986.72 187.454 16 8 -3 17 131.636 89.8424 12 8 3 17 277.038 96.6497 23 -8 3 -17 75.9905 82.0484 8 -8 3 -17 133.919 72.2663 18 8 3 17 169.421 100.650 16 8 -3 18 9942.10 405.489 12 8 3 18 9884.11 401.446 23 -8 3 -18 10305.3 408.391 8 -8 3 -18 9511.97 392.592 18 8 3 18 10257.3 427.225 16 8 -3 19 1348.31 133.409 12 8 3 19 1441.26 138.196 23 -8 3 -19 1488.43 138.333 8 -8 3 -19 1347.52 125.773 18 8 3 19 1587.16 151.959 16 8 -3 20 5524.39 254.187 12 8 3 20 5282.29 250.795 23 -8 3 -20 5323.89 252.754 8 -8 3 -20 4827.90 238.394 18 8 3 20 5743.16 273.150 16 8 -3 21 10016.8 350.780 12 8 3 21 9614.58 347.184 23 8 3 21 9509.92 362.052 16 8 3 22 4049.94 188.950 23 -8 3 -23 1785.55 102.216 13 8 3 23 2548.50 124.866 23 8 4 -20 387.857 60.4575 21 8 4 -19 14217.5 462.535 21 8 4 -18 3316.68 182.135 21 8 4 -17 385.557 85.3899 21 8 4 -17 369.436 72.9133 11 8 4 -16 984.765 107.851 11 8 4 -16 794.317 109.778 21 8 4 -15 29.5602 69.0358 21 8 4 -15 37.7578 64.1616 11 8 4 -14 18819.1 660.321 11 8 4 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896.245 109.850 8 -8 4 2 18434.5 613.759 8 8 4 -2 17934.5 696.303 24 -8 4 1 3983.17 223.166 8 8 4 -1 3753.65 272.826 24 8 4 0 34647.2 1120.73 9 -8 4 0 33175.9 1009.43 8 8 4 0 34241.6 1110.54 24 8 4 1 31381.3 1040.94 9 -8 4 -1 29794.8 931.087 8 8 4 1 31024.9 1029.28 24 8 4 2 29042.5 980.305 9 -8 4 -2 27844.1 871.790 8 8 4 2 27739.7 949.869 24 8 4 3 6723.67 379.246 9 -8 4 -3 6612.78 309.976 8 8 4 3 7164.28 376.052 24 8 4 4 35755.4 1157.29 9 -8 4 -4 34955.6 1058.19 8 8 4 4 35653.0 1134.09 24 8 4 5 53.6186 100.261 9 8 4 5 48.5857 101.459 24 -8 4 -5 48.3699 65.4185 8 8 4 6 9962.26 449.479 21 -8 4 -6 10656.5 418.555 8 -8 4 -7 2015.36 166.418 8 -8 4 -8 10953.3 433.956 8 -8 4 -9 8138.30 359.886 8 -8 4 -10 1119.24 132.990 8 -8 4 -11 497.281 113.534 8 -8 4 -11 561.942 106.652 10 -8 4 -12 23683.1 808.917 8 8 4 12 23517.7 835.944 16 -8 4 -13 12945.5 448.226 10 8 4 13 12151.4 484.670 16 8 4 14 105.406 68.1812 23 -8 4 -14 129.081 66.3005 10 8 4 14 91.4575 92.8632 16 8 4 15 7997.94 337.833 23 -8 4 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802.431 9 8 5 -8 23550.0 794.952 24 8 5 -8 24994.0 804.625 21 8 5 -7 599.454 120.815 9 8 5 -7 646.697 122.366 21 8 5 -7 545.489 116.231 24 8 5 -6 13951.9 543.179 9 8 5 -6 13127.8 528.195 24 8 5 -6 14391.7 542.799 21 8 5 -5 16496.7 620.643 9 8 5 -5 15334.7 593.417 24 8 5 -5 16400.6 604.669 21 8 5 -4 9319.20 427.587 24 8 5 -4 10016.0 438.182 21 8 5 -3 2275.35 199.840 21 8 5 -3 1982.14 182.762 24 -8 5 3 2626.77 188.549 10 8 5 -2 6339.92 352.855 9 8 5 -2 6685.55 339.408 21 8 5 -2 6123.65 320.930 24 -8 5 2 7040.90 331.903 10 8 5 -1 1506.04 180.621 9 8 5 -1 1263.75 145.173 24 8 5 -1 1211.19 155.323 21 -8 5 1 1204.70 144.792 10 8 5 0 13526.3 538.895 9 8 5 0 11651.1 478.916 24 -8 5 0 11387.6 434.887 8 8 5 0 12524.8 501.307 21 -8 5 0 12599.0 502.259 10 8 5 1 48.5396 90.2613 9 8 5 1 38.5925 71.3630 24 8 5 1 30.0367 89.3911 21 -8 5 -1 152.405 68.7660 8 -8 5 -1 25.0791 90.4120 10 8 5 2 12641.1 528.650 9 -8 5 -2 12261.0 452.337 8 8 5 2 12504.0 503.926 21 -8 5 -2 12549.5 511.552 10 8 5 3 135.315 103.735 9 8 5 3 116.905 95.3274 21 -8 5 -3 114.615 72.1886 8 -8 5 -3 213.281 98.5227 10 8 5 4 6720.94 349.623 9 -8 5 -4 6740.58 302.962 8 8 5 4 6098.17 322.997 21 -8 5 -5 44.9522 65.1172 8 -8 5 -5 24.3065 90.4108 10 -8 5 -6 19771.2 662.352 8 -8 5 -6 21125.3 708.976 10 -8 5 -7 12451.7 459.195 8 -8 5 -8 423.937 82.4621 13 -8 5 -8 327.033 85.4986 8 -8 5 -8 471.533 103.652 10 -8 5 -9 5244.62 258.019 13 -8 5 -9 5146.67 255.078 8 -8 5 -9 5538.53 270.870 10 8 5 9 5272.53 281.624 16 -8 5 -10 13538.1 493.854 13 -8 5 -10 13717.5 487.934 8 -8 5 -10 15009.2 499.333 10 8 5 10 13668.3 515.675 16 -8 5 -11 249.418 72.9954 13 -8 5 -11 196.817 72.6578 8 8 5 11 223.488 89.9013 16 -8 5 -11 222.127 73.1512 10 -8 5 -12 40.0212 58.7635 13 -8 5 -12-7.64138 58.7899 8 8 5 12 98.4698 82.8490 16 -8 5 -12 13.5548 47.9480 10 -8 5 -13 152.382 66.9406 13 -8 5 -13 93.8342 66.5333 8 -8 5 -13 192.366 56.2298 10 -8 5 -14 20978.7 644.266 13 -8 5 -14 20953.3 643.948 8 -8 5 -14 20678.9 616.357 10 -8 5 -15 2004.10 126.629 13 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0 -19 3876.07 244.383 22 9 0 -18 42.2926 101.159 11 -9 0 18 54.9817 62.7002 17 9 0 -18-6.11579 73.9724 22 9 0 -17 18661.4 696.430 11 -9 0 17 17419.0 587.347 17 9 0 -17 18845.5 671.146 22 9 0 -16-19.9375 80.9057 22 9 0 -16-7.49635 95.8837 11 -9 0 16 16.3200 65.0329 17 9 0 -15 16744.4 659.407 11 9 0 -15 17111.9 635.883 22 -9 0 15 16338.8 559.230 17 9 0 -14 22.6072 87.4706 11 -9 0 14 8.49754 70.2420 17 9 0 -14 6.79429 82.7137 22 9 0 -13 142973. 3808.90 11 9 0 -13 140636. 3778.33 22 -9 0 13 138938. 3683.78 17 9 0 -12 26.7413 78.1536 22 9 0 -12-21.9173 92.3417 11 -9 0 12 42.6222 66.9023 17 9 0 -11 1292.49 161.267 11 9 0 -11 1554.13 168.237 22 -9 0 11 1312.36 127.613 17 9 0 -10 83.9964 85.0407 22 9 0 -10-13.9082 75.3520 11 -9 0 10-8.35860 67.1192 17 9 0 -9 10585.6 465.165 11 -9 0 9 10493.9 398.807 17 9 0 -8 250.913 91.2915 11 -9 0 8 175.050 73.8173 17 9 0 -7 6301.44 326.896 11 -9 0 7 5297.93 258.972 17 9 0 -6 37.8620 77.3456 11 -9 0 6 118.737 71.4121 17 9 0 -5 98840.6 2697.54 11 -9 0 5 97802.2 2608.70 17 9 0 -4 97.6208 82.9412 11 -9 0 4 3.85591 61.9317 17 9 0 -3 14022.8 542.438 11 -9 0 3 13831.0 479.456 17 9 0 -2 106.892 86.8277 11 -9 0 2 76.5989 68.0814 17 9 0 -1 162913. 4154.96 11 9 0 -1 159552. 4112.76 24 -9 0 1 150015. 4058.85 17 9 0 0-10.0218 64.8425 24 9 0 0 23.4501 76.7298 11 9 0 1 100189. 2740.28 24 9 0 1 103607. 2779.08 11 9 0 2-25.8505 67.3003 24 -9 0 -2 79.7081 46.8323 8 -9 0 -2 99.9021 67.6867 20 -9 0 -3 16020.3 508.114 8 -9 0 -3 16716.9 541.003 20 9 0 4 53.9244 68.5672 24 -9 0 -4 15.5382 41.3550 8 -9 0 -4-16.2150 61.0929 20 -9 0 -5 34216.0 993.168 8 -9 0 -5 36759.5 1038.52 20 -9 0 -6 53.4197 65.0157 20 -9 0 -6 57.9197 41.4618 8 -9 0 -7 42889.2 1229.16 20 -9 0 -8 4.21187 64.0105 20 9 0 9 141063. 3778.42 7 9 0 10 85.2010 97.5302 7 9 0 11 12211.1 512.763 7 9 0 12 13.5136 93.2720 7 -9 0 -12 22.7660 63.4856 19 -9 0 -13 88792.6 2375.36 19 9 0 13 86092.4 2448.72 7 9 0 14 103.349 104.280 7 -9 0 -14 28.2045 62.5642 19 -9 0 -15 8803.59 361.976 19 9 0 15 8106.37 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3 -4 7006.36 313.155 8 9 3 4 7159.38 352.662 21 -9 3 -4 6548.32 306.407 19 9 3 4 7637.51 396.200 24 9 3 5 18.7053 82.0816 21 -9 3 -5 75.9741 75.1309 8 9 3 5 78.2698 104.732 24 -9 3 -5 112.727 69.2912 19 9 -3 5 53.1361 84.9738 7 9 3 6 16983.6 667.170 24 9 3 6 16534.6 619.091 21 -9 3 -6 16998.4 580.559 19 9 -3 6 15621.9 619.008 7 9 3 7 10066.1 438.868 21 -9 3 -7 9710.18 398.170 19 9 -3 7 9976.59 450.414 7 9 -3 8 680.936 132.214 7 9 3 8 691.514 116.463 23 -9 3 -8 775.526 114.637 19 -9 3 -9 1213.61 135.765 8 9 3 9 1164.82 135.319 23 -9 3 -9 1268.62 135.853 19 9 -3 9 1334.11 163.782 7 -9 3 -10 1323.98 139.572 8 9 3 10 1254.93 144.134 23 -9 3 -10 1302.77 138.925 19 9 -3 10 1387.02 165.151 7 9 3 11 9267.53 410.249 23 -9 3 -11 10170.7 412.152 8 -9 3 -11 9361.98 397.978 19 9 -3 11 10077.2 448.041 7 9 -3 12 692.148 135.393 7 9 3 12 604.352 110.648 23 -9 3 -12 741.780 113.700 8 -9 3 -12 667.905 109.667 19 9 3 12 713.733 126.920 16 9 -3 13 12.6733 88.3580 7 9 3 13 70.7964 86.4829 23 -9 3 -13 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180.075 8 9 4 -4 2963.38 246.684 24 9 4 -3 830.467 153.434 9 9 4 -3 954.912 152.039 24 9 4 -3 751.678 140.387 21 -9 4 3 685.413 103.434 8 9 4 -2 362.959 120.775 9 9 4 -2 263.782 114.678 24 9 4 -2 463.590 124.871 21 -9 4 2 248.021 77.2050 8 9 4 -1-38.6766 102.373 24 9 4 -1-39.7149 94.9910 21 -9 4 1 9.43104 61.0212 8 -9 4 0 1430.40 135.352 8 9 4 0 1276.32 173.964 24 9 4 0 1276.35 164.810 21 9 4 1 740.391 151.256 9 9 4 1 895.844 149.311 24 9 4 1 1040.21 152.486 21 -9 4 -1 755.507 107.537 8 9 4 2 8676.93 445.042 9 -9 4 -2 8851.29 371.754 8 9 4 2 9107.94 416.256 21 9 4 2 8811.74 432.354 24 9 4 3 2380.44 220.621 9 9 4 3 2407.33 219.196 24 -9 4 -3 2094.02 167.092 8 9 4 3 2329.57 205.593 21 -9 4 -4 1049.92 124.443 8 9 4 4 1144.79 161.427 24 9 4 4 1237.94 157.543 21 -9 4 -5 10421.9 422.047 8 9 4 5 10797.0 464.271 21 -9 4 -6 6655.09 309.649 8 9 4 6 6501.28 341.741 21 -9 4 -7 1428.54 147.278 8 -9 4 -8-19.6731 77.1990 8 -9 4 -9 10135.9 410.993 8 -9 4 -10 3006.31 205.168 8 -9 4 -11 4347.45 250.955 8 9 4 11 4537.52 273.432 16 -9 4 -12 9594.76 375.223 10 9 4 12 8082.51 382.618 16 -9 4 -13 4014.76 209.613 10 9 4 13 3410.67 231.599 16 -9 4 -14 822.736 91.2178 10 9 4 14 752.123 116.368 16 9 4 15 1803.79 126.071 23 -9 4 -15 1794.69 118.298 10 9 4 15 1908.59 162.018 16 9 4 16 83.8009 48.0002 23 -9 4 -16 115.473 68.2225 8 9 4 16 119.088 74.9115 16 9 4 17 965.379 81.3993 23 -9 4 -17 1111.47 104.956 8 9 4 17 1210.13 116.319 16 -9 4 -18 2501.30 145.430 8 9 4 18 2450.40 149.163 16 9 4 19 1689.37 109.810 16 9 5 -14 173.117 45.7231 21 9 5 -13 188.038 55.7468 24 9 5 -13 180.237 57.2815 21 9 5 -12-13.8183 54.4347 24 9 5 -12 20.2770 51.1459 21 9 5 -11 5435.36 242.703 9 9 5 -11 5902.52 261.377 24 9 5 -11 5612.15 257.696 21 9 5 -10 2577.74 168.823 9 9 5 -10 2673.99 176.101 24 9 5 -10 3062.55 184.758 21 9 5 -9 1535.50 135.672 9 9 5 -9 1677.15 146.438 24 9 5 -9 1740.41 149.129 21 9 5 -8 2016.99 161.293 9 9 5 -8 2097.51 167.779 21 9 5 -8 2263.51 172.697 24 9 5 -7 1619.93 151.825 9 9 5 -7 1886.64 163.751 24 9 5 -7 1964.42 165.004 21 9 5 -6 216.552 94.8213 9 9 5 -6 185.362 83.2566 24 9 5 -6 160.122 84.6129 21 9 5 -5 50.9025 85.9785 9 9 5 -5 70.4893 78.2023 24 9 5 -5 127.995 93.3178 21 9 5 -4 2406.01 199.656 9 9 5 -4 2202.42 180.626 24 9 5 -4 2313.68 188.051 21 -9 5 4 1943.70 141.399 10 9 5 -3 801.206 120.235 24 9 5 -3 635.234 118.475 21 -9 5 3 972.505 113.064 10 9 5 -2 7422.71 357.958 24 9 5 -2 7781.78 368.737 21 9 5 -1 4093.06 259.966 9 9 5 -1 3978.79 244.159 21 9 5 -1 3767.50 234.207 24 -9 5 1 4352.93 239.992 10 9 5 0 1646.18 173.342 9 -9 5 0 1477.85 123.778 8 9 5 0 1947.78 179.208 21 9 5 0 1893.22 162.270 24 -9 5 0 1825.77 170.097 10 9 5 1 893.990 135.885 9 -9 5 -1 996.122 106.730 8 9 5 1 912.041 130.810 21 -9 5 -1 1054.86 140.696 10 9 5 2-38.1432 90.0876 21 -9 5 -2 64.1233 58.0544 8 -9 5 -2 51.0508 85.4879 10 -9 5 -3 1574.03 131.403 8 9 5 3 1299.35 150.613 21 -9 5 -3 1686.78 166.864 10 -9 5 -4 7075.16 307.112 8 -9 5 -4 7695.10 357.917 10 -9 5 -5 1472.80 130.162 8 -9 5 -5 1708.88 169.456 10 -9 5 -6 826.254 104.079 8 -9 5 -6 847.587 125.109 10 -9 5 -7 84.1157 59.8881 8 -9 5 -8 298.118 74.1375 8 -9 5 -8 225.380 76.9780 10 -9 5 -9 1324.28 118.653 8 -9 5 -9 1394.71 122.652 10 -9 5 -10 90.7929 51.2345 13 -9 5 -10 10.7502 57.3558 8 -9 5 -10 87.5814 61.3065 10 -9 5 -11 3651.22 182.409 13 -9 5 -11 3812.96 196.436 8 -9 5 -11 4040.79 189.788 10 -9 5 -12 239.369 55.7676 13 -9 5 -12 192.823 63.1413 8 -9 5 -12 227.840 56.6329 10 -9 5 -13 1129.75 87.5292 13 -9 5 -13 1056.87 95.2930 8 -9 5 -13 988.253 81.6595 10 9 5 13 915.164 102.379 16 -9 5 -14 658.757 73.4554 8 9 5 14 862.064 88.5756 16 -9 5 -15 161.561 45.5084 8 9 5 15 206.026 52.8890 16 -9 6 -1 496.548 57.1613 10 -9 6 -2 1394.22 92.5554 10 -9 6 -3 1739.17 106.201 10 9 6 3 1541.96 113.248 16 9 6 4 364.531 64.1446 16 -9 6 -4 385.852 57.5153 10 -9 6 -5 4080.19 168.971 10 9 6 5 3173.42 162.159 16 -9 6 -6 2526.08 125.977 10 9 6 6 2169.14 123.824 16 10 0 -23 13.3844 36.0078 11 10 0 -22 7631.41 305.085 11 10 0 -21 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6.10637 66.1720 11 -10 -1 5-4.51098 77.1629 17 -10 1 5 107.198 71.8856 17 10 1 -4 46566.7 1412.79 11 10 -1 -4 46301.5 1368.53 11 -10 -1 4 48576.2 1317.68 17 10 -1 -3 1151.75 143.899 11 -10 1 3 1345.71 131.123 20 10 1 -3 1032.91 160.511 11 -10 -1 3 1370.94 134.674 17 -10 1 2 1332.06 130.896 20 -10 -1 2 1342.83 134.098 17 -10 1 1 2446.34 162.646 8 10 1 -1 2089.88 194.200 24 -10 1 1 2199.49 166.111 20 -10 -1 1 2170.41 165.137 17 -10 1 0 62187.3 1669.26 8 10 1 0 58636.3 1753.85 24 -10 1 0 58700.4 1675.10 20 -10 -1 0 60524.8 1678.49 17 -10 1 -1 30470.1 915.120 8 10 1 1 30903.1 1003.74 24 -10 1 -1 29877.3 929.373 20 -10 -1 -1 30822.8 928.151 17 10 1 2 771.895 138.635 24 -10 -1 -2 952.408 117.912 20 -10 1 -2 936.220 118.910 20 -10 1 -3 6875.44 294.519 8 10 1 3 6174.75 347.176 24 -10 -1 -3 6802.62 306.449 20 -10 1 -3 6345.26 301.266 20 -10 1 -4 82275.3 2167.76 8 10 1 4 78758.2 2266.60 24 -10 -1 -4 82244.7 2184.67 20 -10 1 -4 76645.0 2180.70 20 10 1 5 237.189 106.705 24 -10 1 -5 325.560 75.3176 8 -10 -1 -5 287.210 85.8545 20 -10 1 -5 255.815 85.7352 20 -10 1 -6 5343.32 251.185 8 10 1 6 4686.75 301.161 24 -10 -1 -6 5536.88 263.676 20 -10 1 -6 4585.62 259.334 20 10 1 6 4813.93 300.149 2 10 -1 6 5588.66 316.902 2 -10 1 -7 723.891 94.9402 8 -10 -1 -7 656.136 102.754 20 10 1 7 773.502 138.305 2 10 -1 7 697.371 133.047 2 10 1 7 748.207 122.184 7 10 1 8 19235.4 706.777 2 10 -1 8 18757.5 703.392 2 -10 1 -8 19454.5 627.712 8 -10 -1 -8 19723.0 638.978 20 10 1 8 18798.9 688.580 7 10 1 9 2847.15 226.588 2 10 -1 9 2601.96 217.031 2 -10 1 -9 2798.47 174.499 8 10 -1 9 2809.15 240.103 7 10 1 9 2728.56 213.872 7 10 -1 10 671.809 147.282 7 10 1 10 796.162 130.321 7 -10 1 -10 587.398 87.8384 8 -10 1 -10 617.836 107.435 19 10 1 10 851.533 141.128 2 10 -1 10 522.983 126.985 2 -10 1 -11 6471.48 285.565 8 10 1 11 6296.92 347.025 2 10 -1 11 6772.29 359.029 2 -10 1 -11 6441.55 308.438 19 10 -1 11 6412.72 364.951 7 10 1 11 6144.59 328.790 7 -10 1 -12 37380.7 1087.37 8 10 1 12 38414.5 1177.16 2 10 -1 12 36316.6 1181.54 2 -10 -1 -12 35984.5 1081.30 19 -10 1 -12 36377.0 1120.50 19 10 -1 12 38014.3 1202.22 7 10 1 12 38570.8 1158.27 7 -10 1 -13 9248.30 368.788 8 -10 -1 -13 9657.59 372.877 19 -10 1 -13 10032.3 410.411 19 10 -1 13 9478.89 460.208 7 10 1 13 9256.43 417.052 7 -10 1 -14 11193.5 410.034 8 -10 -1 -14 10096.2 395.844 19 -10 1 -14 10752.2 436.728 19 10 -1 14 11632.8 504.135 7 10 1 14 10844.6 454.768 7 10 -1 15 437.803 131.374 7 -10 -1 -15 363.475 72.3534 19 -10 1 -15 511.663 108.050 19 10 1 16 7780.77 355.251 12 -10 1 -16 8466.15 358.037 19 10 1 17 57.4946 73.1321 12 10 -1 18 10471.1 449.476 12 10 1 18 10431.2 403.685 12 10 -1 19 1103.58 143.997 12 10 1 19 831.930 101.193 12 10 1 19 851.114 115.353 23 10 -1 20 2833.48 195.706 12 10 -1 20 2849.46 162.211 23 10 1 20 2780.99 180.602 23 10 -1 21 33.0677 74.9946 12 10 -1 21 26.6955 44.1429 23 10 1 21 64.0719 68.2553 23 10 -1 22 8725.60 331.528 12 10 1 22 8383.62 313.626 23 -10 1 -22 8349.42 336.209 18 10 -1 23 189.736 60.7367 12 10 1 23 189.487 49.5119 23 -10 1 -23 112.102 55.2816 11 -10 -1 -23 120.572 47.6458 18 -10 1 -23 181.555 57.2054 18 10 2 -22 6.79756 35.5699 21 -10 -2 22 41.0410 35.9646 17 10 2 -21 6758.42 259.773 21 -10 -2 21 6597.90 244.925 17 -10 -2 20 491.284 74.2397 17 -10 2 19 4183.42 175.777 8 10 2 -19 4083.43 245.024 11 -10 -2 19 4309.92 205.444 17 10 2 -18 1339.63 157.782 11 -10 -2 18 1321.87 121.494 17 10 2 -17 891.674 135.399 11 -10 -2 17 703.792 104.169 17 10 2 -16 16840.1 623.678 11 -10 -2 16 14703.1 524.907 17 10 2 -15 15337.9 613.658 11 10 2 -14 1919.24 203.733 11 10 2 -13 428.913 136.087 11 10 2 -12 10572.6 498.813 11 10 2 -11 166.194 109.852 11 -10 -2 11 125.022 92.5063 17 10 2 -10 4966.42 322.611 11 -10 -2 10 4602.08 253.414 17 10 2 -9 1922.98 207.707 11 10 2 -9 1534.30 151.856 21 -10 -2 9 1522.21 151.711 17 10 2 -8 1476.41 148.008 21 10 2 -8 1490.80 190.681 11 -10 -2 8 1467.23 145.292 17 10 2 -7 10399.1 484.642 11 -10 -2 7 10735.5 409.905 17 -10 2 6 15232.5 531.922 8 10 2 -6 14983.6 619.488 11 10 2 -6 13810.7 538.573 21 -10 2 6 15076.5 517.913 20 -10 -2 6 14643.2 528.651 17 -10 2 5 28032.5 912.613 8 10 2 -5 28962.5 1012.22 11 10 2 -5 31031.9 949.105 21 -10 2 5 31262.1 908.924 20 -10 -2 5 29727.0 916.291 17 -10 2 4 3496.96 208.369 8 10 2 -4 3580.00 265.689 11 10 2 -4 2896.89 206.067 21 -10 2 4 2607.39 180.514 20 -10 -2 4 2815.69 192.440 17 -10 2 3 19776.0 672.642 8 10 2 -3 20899.1 768.400 11 10 2 -3 20437.2 694.133 21 -10 2 3 20582.0 669.131 20 -10 -2 3 20326.8 669.494 17 10 2 -2 125421. 3330.33 11 10 2 -2 124795. 3237.13 21 -10 2 2 121157. 3197.89 20 -10 -2 2 127843. 3206.52 17 10 2 -1 1448.54 181.690 24 10 2 -1 1728.66 154.932 21 -10 2 1 1501.61 138.558 20 10 2 -1 1140.47 170.561 11 -10 -2 1 1444.80 141.522 17 10 2 0 10873.7 500.499 24 10 2 0 12004.4 518.837 11 10 2 0 10673.1 440.065 21 -10 2 0 10718.0 421.538 20 -10 -2 0 11542.5 427.814 17 -10 2 -1 1315.59 139.083 8 10 2 1 1316.88 174.034 24 10 2 1 1585.61 147.790 21 -10 2 -1 1434.93 136.426 20 -10 -2 -1 1505.15 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10 2 9 2002.63 181.970 2 10 -2 9 1684.52 171.599 2 -10 2 -9 2433.92 184.358 19 10 -2 9 2037.13 214.782 7 10 2 10 43872.4 1324.40 2 10 -2 10 44154.3 1328.41 2 -10 2 -10 45308.6 1285.17 8 -10 2 -10 43332.9 1290.82 19 10 -2 10 42788.8 1372.88 7 10 -2 11 883.940 157.790 7 -10 2 -11 1021.84 121.060 8 -10 2 -11 1235.09 140.700 19 10 2 11 1071.79 133.853 16 10 -2 12 983.912 165.736 7 -10 2 -12 653.618 110.942 8 -10 2 -12 902.820 131.378 19 10 2 12 776.993 120.199 16 -10 2 -13 1780.93 156.231 8 -10 2 -13 1557.68 162.146 19 10 2 13 1936.30 166.037 16 10 -2 13 1849.05 202.070 7 10 2 14 2915.45 211.585 23 -10 2 -14 3344.63 205.004 8 10 2 14 3091.19 206.209 16 10 -2 14 3178.00 252.678 7 10 2 15 804.188 127.381 23 -10 2 -15 690.175 105.442 8 10 2 15 735.195 109.341 16 10 2 16 8676.29 373.670 23 -10 2 -16 8460.55 350.541 8 10 2 16 8604.32 361.164 16 10 -2 17 6112.81 315.517 12 10 2 17 5406.83 279.726 23 -10 2 -17 6342.00 277.867 8 10 -2 18 3018.42 211.477 12 10 2 18 2971.83 190.771 23 -10 2 -18 3095.13 175.535 8 10 -2 19 4681.01 249.550 12 10 2 19 4341.02 228.125 23 -10 2 -19 4433.76 232.354 18 10 -2 20 10990.9 407.117 12 -10 2 -20 10252.4 381.736 11 10 2 20 10746.3 388.891 23 -10 2 -20 10894.6 396.445 18 10 -2 21 2237.11 151.239 12 10 2 21 2641.24 150.030 23 -10 2 -21 2523.52 148.936 18 10 -2 22 623.045 78.1861 12 -10 2 -22 560.676 66.6587 18 10 3 -21 6653.81 231.422 21 10 3 -20 246.561 51.1065 21 10 3 -20 279.079 59.7684 11 10 3 -19 565.237 74.6766 21 10 3 -19 492.038 78.1415 11 -10 -3 19 563.175 70.0660 17 10 3 -18 5096.23 248.530 11 10 3 -18 4827.65 224.788 21 -10 -3 18 4967.92 211.427 17 10 3 -17 1946.78 143.538 21 -10 -3 17 1926.83 133.599 17 10 3 -16 958.640 111.554 21 10 3 -16 834.934 118.603 11 -10 -3 16 984.366 107.319 17 10 3 -15 2791.22 204.444 11 10 3 -15 2771.05 186.603 21 -10 -3 15 2452.63 165.557 17 -10 3 14 2104.16 130.582 8 10 3 -14 1983.60 187.372 11 10 3 -14 2149.34 168.962 21 -10 -3 14 2006.85 151.693 17 -10 3 13 15129.8 489.233 8 10 3 -13 14546.4 572.967 11 10 3 -13 14284.0 534.364 21 -10 -3 13 14423.1 502.989 17 -10 3 12 1313.62 114.966 8 10 3 -12 1318.83 158.262 11 10 3 -12 1090.68 135.273 21 -10 -3 12 1093.60 124.657 17 -10 3 11 1440.88 128.137 8 10 3 -11 1330.07 166.765 11 10 3 -11 1776.05 168.576 21 -10 -3 11 1482.68 138.381 17 -10 3 10 2212.74 157.289 8 10 3 -10 1991.53 199.278 11 10 3 -10 1786.65 171.413 21 -10 -3 10 1828.60 152.021 17 -10 3 9 5170.33 252.073 8 10 3 -9 5044.32 308.384 11 10 3 -9 4475.86 270.404 21 -10 -3 9 4541.83 242.435 17 10 3 -8 9832.93 436.438 9 -10 3 8 9935.58 393.767 8 10 3 -8 9523.02 461.037 11 10 3 -8 9948.99 432.304 21 -10 -3 8 9756.17 387.178 17 10 3 -7-13.4751 76.5186 9 10 3 -7 67.0330 84.1266 21 -10 3 7 56.7788 66.9516 8 10 3 -7 22.5556 84.1027 11 -10 -3 7 83.7974 76.1850 17 10 3 -6 9052.43 425.112 9 -10 3 6 9092.27 369.862 8 10 3 -6 9017.68 437.669 11 10 3 -6 8419.46 391.670 21 -10 -3 6 8067.54 349.638 17 10 3 -5-14.3842 95.7052 9 10 3 -5 12.3666 77.6812 21 -10 3 5-29.1772 66.1025 8 10 3 -5 90.6727 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1020.07 8 10 3 13 33874.3 1034.99 16 10 3 14 69.1612 76.2970 23 -10 3 -14 159.930 80.5236 8 10 3 14 188.065 93.1551 16 10 -3 15 2356.90 179.986 12 10 3 15 2275.39 165.546 23 -10 3 -15 2047.22 159.423 8 10 3 15 2464.84 178.267 16 10 -3 16 11830.3 452.262 12 10 3 16 11717.2 436.816 23 -10 3 -16 12824.7 448.038 8 10 3 16 12460.5 456.516 16 10 -3 17 1275.60 124.722 12 10 3 17 1152.05 113.758 23 -10 3 -17 1359.06 120.810 8 10 3 17 1198.57 119.976 16 10 -3 18 1557.53 127.217 12 10 3 18 1635.46 123.821 23 -10 3 -18 1823.72 127.854 8 10 3 18 1599.77 122.074 16 10 -3 19-2.94448 53.2649 12 10 3 19 52.7033 52.0618 23 -10 3 -19 16.9378 45.5081 8 10 -3 20 1389.85 96.5225 12 10 3 20 1396.18 94.7776 23 10 4 -18 969.373 78.9964 24 -10 -4 17 27.4630 30.7546 17 -10 -4 16 4834.01 182.752 17 10 4 -15 3880.75 184.666 11 -10 -4 15 4450.35 176.881 17 10 4 -14 517.864 74.0158 11 -10 -4 14 551.864 69.2312 17 10 4 -13 1920.29 137.435 11 -10 -4 13 2001.83 121.521 17 10 4 -12 3192.92 188.744 11 -10 -4 12 3090.01 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299.276 8 -10 4 -14 7536.50 273.565 10 10 4 14 7501.78 315.526 16 -10 4 -15 1468.15 121.608 8 10 4 15 1773.33 133.370 16 -10 4 -16 18.2491 48.6673 8 10 4 16 34.8866 55.1352 16 -10 4 -17 1117.44 88.9462 8 10 4 17 948.385 83.7551 16 10 5 -13 8.12408 29.8207 21 10 5 -12 51.4442 41.3660 21 10 5 -11 555.308 68.0993 24 10 5 -11 582.467 72.1178 21 10 5 -10 1116.05 99.8446 24 10 5 -10 1071.45 98.4431 21 10 5 -9 39.3404 53.9051 24 10 5 -9 31.2724 53.6876 21 10 5 -8 364.875 79.9089 24 10 5 -8 404.142 82.9127 21 10 5 -7 2124.45 156.016 24 10 5 -7 2199.21 152.990 21 10 5 -6 5213.38 254.935 24 10 5 -6 4970.07 249.766 21 10 5 -5 671.550 107.164 21 10 5 -5 599.966 97.9542 24 10 5 -4 774.137 110.117 24 10 5 -4 707.379 113.770 21 -10 5 4 441.721 65.0196 10 10 5 -3 260.103 85.0653 24 -10 5 3 283.403 66.1017 10 10 5 -2 7944.94 356.553 24 -10 5 2 9542.38 353.478 10 -10 5 1 1589.99 115.232 8 10 5 -1 1297.28 136.320 24 -10 5 0 1447.26 115.093 8 -10 5 0 1906.98 154.592 10 -10 5 -1 1032.33 100.670 8 -10 5 -1 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3 -8 3934.92 233.809 21 -11 -3 8 3490.60 201.442 17 -11 3 7 9294.33 377.841 8 11 3 -7 9572.88 444.200 11 11 3 -7 9668.76 409.208 21 -11 -3 7 9131.12 365.997 17 11 3 -6 563.064 108.409 21 -11 3 6 591.140 100.644 8 11 3 -6 523.154 129.335 11 -11 -3 6 658.811 102.622 17 -11 3 5 20090.0 659.832 8 11 3 -5 20716.5 742.689 11 11 3 -5 18591.8 678.164 21 -11 -3 5 19413.5 636.198 17 11 3 -4 654.029 117.363 21 -11 3 4 444.869 90.0085 8 11 3 -4 439.655 122.683 11 -11 -3 4 565.526 99.0999 17 -11 3 3 4515.78 250.921 8 11 3 -3 4593.19 272.601 21 -11 -3 3 4759.85 237.733 17 -11 3 2 18988.1 661.202 8 11 3 -2 20827.5 706.629 21 -11 -3 2 20091.6 643.693 17 -11 3 1 2998.29 200.649 8 11 3 -1 2745.53 211.101 21 -11 -3 1 3197.59 190.067 20 -11 3 0 5044.60 276.609 8 11 3 0 5957.04 359.961 24 11 3 0 5906.34 313.831 21 -11 -3 0 6296.18 273.295 20 -11 3 0 5951.95 271.961 19 -11 3 -1 12622.0 472.235 8 11 3 1 11897.4 553.692 24 11 3 1 12615.6 496.327 21 -11 3 -1 11381.0 440.918 19 -11 3 -2 5568.70 277.889 8 11 3 2 5325.88 337.392 24 11 3 2 5389.55 293.616 21 -11 3 -2 4872.63 254.041 19 11 3 3 852.618 167.883 24 11 3 3 716.413 119.980 21 -11 3 -3 843.063 111.767 19 11 -3 3 758.062 145.132 7 11 -3 4 1415.61 178.519 7 11 3 4 1935.91 208.099 24 11 3 4 1879.90 170.977 21 -11 3 -4 1662.65 143.790 19 11 3 5 14404.8 526.718 21 -11 3 -5 12705.3 486.129 19 11 -3 5 13251.8 554.058 7 11 -3 6 189.619 111.638 7 -11 3 -6 144.877 86.1585 8 -11 3 -6 166.798 78.8936 19 11 -3 7 735.641 137.307 7 -11 3 -7 841.918 115.511 8 -11 3 -7 865.165 119.482 19 -11 3 -8 9318.77 383.942 8 -11 3 -8 9279.65 383.620 19 11 -3 8 9256.62 424.748 7 -11 3 -9 14363.7 510.680 8 -11 3 -9 13209.3 499.390 19 11 -3 9 14218.7 553.838 7 11 3 10 1713.28 144.885 23 -11 3 -10 2068.85 162.422 8 -11 3 -10 1787.10 153.609 19 11 3 10 2115.32 174.129 16 11 -3 10 2134.91 191.689 7 11 3 11 7290.06 312.893 23 -11 3 -11 7389.29 325.062 8 -11 3 -11 6962.37 314.658 19 11 3 11 7247.84 334.148 16 11 -3 11 7126.83 349.292 7 11 3 12 31839.6 957.368 23 -11 3 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168.242 101.043 24 11 4 1 98.3256 83.0833 21 -11 4 -1 139.809 78.2673 8 11 4 2 445.794 113.723 24 11 4 2 303.269 91.1462 21 -11 4 -2 278.178 83.3092 8 -11 4 -3 9428.72 376.077 8 11 4 3 9663.92 407.990 21 -11 4 -4 2649.13 174.797 8 -11 4 -5 1721.37 142.387 8 -11 4 -6 9090.41 366.428 8 -11 4 -7 2556.42 172.169 8 -11 4 -8 53.2463 65.0516 8 11 4 9 14854.7 528.147 16 -11 4 -10 1419.25 122.272 10 11 4 10 1124.09 123.663 16 -11 4 -11 16946.9 525.290 10 11 4 11 14510.1 522.927 16 -11 4 -12 194.109 66.9416 8 -11 4 -12 263.102 57.1503 10 11 4 12 297.483 74.5766 16 -11 4 -13 12217.5 414.852 8 -11 4 -13 11572.4 379.060 10 11 4 13 12530.4 416.354 16 -11 4 -14 3365.11 168.065 8 11 4 14 3468.75 167.099 16 -11 4 -15 15271.4 471.605 8 11 5 -8 1045.57 86.6251 24 11 5 -7 5551.09 230.549 24 11 5 -6 107.932 54.5428 24 11 5 -5 1353.63 113.185 24 11 5 -4 4924.98 223.171 24 11 5 -4 4314.75 214.634 21 11 5 -3 11429.8 337.989 21 -11 5 3 5705.82 234.204 10 11 5 -2 6821.15 278.410 21 -11 5 2 6041.86 238.447 10 11 5 -1 153.810 66.0578 21 -11 5 1 18.3750 36.6275 8 -11 5 1 34.0938 44.0830 10 -11 5 0 1073.17 86.2085 8 -11 5 0 1388.52 110.335 10 -11 5 -1 7041.43 271.383 8 -11 5 -1 8337.36 305.746 10 -11 5 -2 64.7788 48.2686 8 -11 5 -2 50.7192 57.4719 10 -11 5 -3 211.840 55.4054 8 -11 5 -3 182.963 64.4760 10 -11 5 -4 32.9619 47.4512 8 -11 5 -4 32.7129 51.3529 10 -11 5 -5 15078.2 487.780 8 -11 5 -5 16683.4 510.356 10 -11 5 -6 2887.50 149.080 8 11 5 6 3153.55 173.263 16 -11 5 -7 888.617 80.5940 8 11 5 7 1153.07 103.042 16 -11 5 -8-11.8680 35.7719 8 -11 5 -8 28.8086 39.6897 10 11 5 8 19.9461 45.2468 16 -11 5 -9 2498.44 127.047 8 -11 5 -9 2782.00 130.133 10 11 5 9 2478.07 135.287 16 12 0 -19 2.94653 42.8738 11 12 0 -18 13915.7 474.074 11 12 0 -17 25.7775 66.1060 11 -12 0 17 19.2254 49.0031 17 12 0 -16 830.076 114.422 11 -12 0 16 839.558 86.9118 17 12 0 -15 48.3138 80.2207 11 -12 0 15 44.0700 58.6029 17 12 0 -14 16199.8 595.574 11 -12 0 14 15455.8 514.632 17 12 0 -13-6.17347 76.6054 11 -12 0 13 11.2048 65.9516 17 12 0 -12 568.673 121.178 11 -12 0 12 774.586 103.799 17 12 0 -11 26.8690 85.4115 11 -12 0 11-16.7011 65.7908 17 12 0 -10 4651.76 287.080 11 -12 0 10 4085.89 229.567 17 12 0 -9-14.1153 97.4254 11 -12 0 9-31.4287 75.2670 17 12 0 -8 29821.8 960.984 11 -12 0 8 27127.5 868.938 17 12 0 -7 94.3155 97.5946 11 -12 0 7 14.0860 89.5623 17 12 0 -6 5280.25 317.207 11 -12 0 6 4632.68 256.068 17 12 0 -5 29.6229 96.9305 11 12 0 -4 30814.9 1031.77 11 -12 0 3 30.9609 79.7222 20 -12 0 2 1695.89 142.705 8 -12 0 2 1874.67 167.515 20 -12 0 1 25.5025 57.7800 8 -12 0 0 49481.0 1359.73 8 12 0 0 45545.3 1407.28 24 -12 0 -1 37.3758 56.4584 8 -12 0 -2 6556.18 283.717 8 -12 0 -2 5510.13 299.834 20 -12 0 -3-27.9676 54.0273 8 -12 0 -3 31.9039 90.0481 20 -12 0 -4 27350.0 827.060 8 -12 0 -4 27382.6 871.960 20 -12 0 -5 45.1508 52.2131 8 -12 0 -5 52.8190 92.9871 20 -12 0 -6 44564.2 1312.32 20 12 0 7-54.1693 112.608 7 12 0 8 25766.9 908.161 7 12 0 9-7.43994 107.763 7 12 0 10 244.802 120.775 7 -12 0 -10 139.958 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307.651 8 12 2 -14 8005.94 314.948 21 -12 2 13 1191.65 106.996 8 12 2 -13 1102.46 105.600 21 12 2 -13 1174.74 149.990 11 -12 2 12 1178.14 110.550 8 12 2 -12 1256.42 118.117 21 12 2 -12 1166.26 153.743 11 -12 -2 12 1074.48 118.761 17 -12 2 11 1464.03 126.119 8 12 2 -11 1444.27 177.531 11 12 2 -11 1499.50 127.513 21 -12 -2 11 1511.86 136.810 17 -12 2 10 6345.23 278.936 8 12 2 -10 6346.38 343.264 11 12 2 -10 5838.93 275.699 21 -12 -2 10 5957.34 279.507 17 -12 2 9 1825.21 148.718 8 12 2 -9 1971.24 199.714 11 12 2 -9 1998.79 154.313 21 -12 -2 9 2108.11 161.101 17 -12 2 8 9050.96 366.564 8 12 2 -8 9260.07 441.826 11 12 2 -8 9125.54 371.691 21 -12 -2 8 9215.22 371.550 17 -12 2 7 1535.53 141.485 8 12 2 -7 1723.61 181.278 24 12 2 -7 1642.40 195.392 11 12 2 -7 1700.94 142.565 21 -12 2 7 1603.94 126.092 20 -12 -2 7 1779.49 155.775 17 12 2 -6 234.686 109.554 24 12 2 -6 229.397 81.0385 21 -12 2 6 200.701 82.9250 8 -12 2 6 182.874 65.4445 20 12 2 -6 158.938 112.238 11 -12 -2 6 299.013 95.4724 17 -12 2 5 32230.3 1004.79 8 12 2 -5 34040.9 1092.58 24 12 2 -5 34620.1 1113.46 11 12 2 -5 32654.7 1002.97 21 -12 2 5 33447.8 984.791 20 -12 -2 5 33883.8 1007.46 17 12 2 -4 8727.40 442.394 24 12 2 -4 9039.50 457.949 11 12 2 -4 8551.81 367.402 21 -12 2 4 9337.13 363.208 20 -12 -2 4 8970.50 369.903 17 12 2 -3 368.948 130.298 24 12 2 -3 329.325 83.0878 21 -12 2 3 272.938 83.0045 20 -12 -2 3 340.197 98.5119 17 12 2 -2 1419.08 190.386 24 12 2 -2 1504.64 139.495 21 -12 2 2 1683.33 144.726 20 -12 2 1 5576.79 278.833 8 12 2 -1 5266.32 331.920 24 12 2 -1 5508.57 276.614 21 -12 -2 1 5297.91 274.750 20 -12 2 1 5754.67 274.615 20 -12 2 0 11949.0 458.409 8 12 2 0 11849.8 530.601 24 12 2 0 11419.7 449.552 21 -12 -2 0 12300.7 458.928 20 12 2 1 204.503 117.725 24 12 2 1 227.313 74.9325 21 -12 2 -1 347.069 93.6357 8 -12 -2 -1 310.330 91.1141 20 12 2 2 2476.23 232.334 24 -12 2 -2 2379.52 176.575 8 -12 -2 -2 2545.15 177.309 20 12 2 2 1960.83 195.388 2 12 -2 2 1960.41 192.472 2 12 2 3 403.048 134.089 24 -12 2 -3 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115.749 19 -12 2 -11 2434.61 165.620 8 -12 2 -11 2126.73 168.427 19 12 -2 11 2263.54 211.901 7 12 2 12 22859.7 752.448 23 -12 2 -12 24940.3 744.684 8 -12 2 -12 22345.0 752.502 19 12 -2 12 24874.0 823.669 7 12 2 13 5247.31 253.478 23 -12 2 -13 5107.91 238.166 8 -12 2 -13 4351.97 239.539 19 12 -2 13 4919.59 286.669 7 12 2 14 10075.7 389.842 23 -12 2 -14 10481.2 373.416 8 12 2 15 37.5641 66.5373 23 -12 2 -15 11.9663 47.3242 8 12 -2 16 985.738 123.566 12 12 2 16 949.473 103.158 23 12 -2 17 2323.39 158.457 12 12 2 17 2290.38 139.534 23 -12 2 -17 1945.28 121.857 18 12 -2 18 2035.83 135.842 12 12 2 18 1771.75 116.100 23 12 -2 19 2065.00 122.823 12 12 2 19 2083.87 111.491 23 12 3 -17 288.107 51.8347 24 -12 -3 17 360.392 43.8647 17 12 3 -16 68.4896 54.0260 24 12 3 -16-2.09357 31.5559 21 12 3 -16 39.5399 44.8499 11 12 3 -15 391.879 76.6640 24 12 3 -15 355.225 56.9196 21 12 3 -15 392.669 72.0993 11 -12 -3 15 492.748 62.1597 17 12 3 -14 6206.89 270.854 24 12 3 -14 6180.24 266.172 11 12 3 -14 6222.65 240.316 21 -12 -3 14 6232.09 228.674 17 12 3 -13 379.909 90.2898 24 12 3 -13 386.639 69.0880 21 -12 3 13 414.137 56.4078 8 12 3 -13 494.278 89.9096 11 -12 -3 13 478.775 72.2197 17 -12 3 12 619.168 70.5925 8 12 3 -12 420.109 98.2288 24 12 3 -12 454.575 79.0652 21 12 3 -12 642.873 99.4763 11 -12 -3 12 512.491 77.0490 17 -12 3 11 8998.40 318.658 8 12 3 -11 9108.53 387.974 24 12 3 -11 8783.15 376.500 11 12 3 -11 8772.66 342.857 21 -12 -3 11 8636.48 322.766 17 -12 3 10 1999.93 132.206 8 12 3 -10 1605.17 165.708 24 12 3 -10 2088.68 171.106 11 12 3 -10 1903.60 143.416 21 -12 -3 10 1897.61 132.702 17 -12 3 9 15341.5 487.576 8 12 3 -9 14027.7 551.889 24 12 3 -9 14591.7 549.860 11 12 3 -9 14100.4 503.987 21 -12 -3 9 14273.1 481.021 17 12 3 -8 394.731 115.584 24 12 3 -8 525.427 95.0671 21 -12 3 8 311.255 73.4965 8 12 3 -8 336.378 99.8037 11 -12 -3 8 534.780 88.1283 17 12 3 -7 19.2471 100.702 24 12 3 -7-4.58823 64.6038 21 -12 3 7-7.64268 63.8402 8 -12 -3 7-49.8457 65.5314 17 -12 3 6 11721.4 418.216 8 12 3 -6 11272.3 490.830 24 12 3 -6 10960.6 431.969 21 -12 -3 6 11000.2 401.940 17 -12 3 5 3301.10 191.068 8 12 3 -5 3165.36 242.100 24 12 3 -5 2828.35 194.382 21 -12 -3 5 2835.23 173.010 17 12 3 -4 63.2223 118.562 24 12 3 -4-4.94475 69.9603 21 -12 3 4 17.0447 67.6638 8 -12 3 3 2386.59 173.979 8 12 3 -3 2593.46 185.179 21 -12 -3 3 2476.77 161.700 20 -12 3 2 15729.5 537.321 8 12 3 -2 15110.9 552.934 21 -12 -3 2 15084.1 512.899 20 -12 3 1 2176.46 166.711 8 12 3 -1 2439.18 184.076 21 -12 -3 1 2498.86 158.589 20 12 3 0 372.226 95.4889 21 -12 3 0 233.930 83.6301 8 -12 -3 0 302.604 71.1062 20 -12 3 0 338.078 70.9354 19 -12 3 -1 1685.18 149.008 8 12 3 1 1796.52 156.102 21 -12 3 -1 1813.92 136.765 19 12 3 2 4938.75 267.950 21 -12 3 -2 5084.58 245.277 19 12 -3 2 5565.33 311.256 7 12 3 3 4698.02 255.321 21 -12 3 -3 5075.53 245.576 19 12 -3 3 5047.05 299.868 7 12 -3 4 537.298 124.817 7 -12 3 -4 628.511 92.2561 19 12 -3 5 62.6766 103.984 7 -12 3 -5 31.0716 70.7545 8 -12 3 -5 8.48958 56.7947 19 -12 3 -6 9237.81 369.518 8 -12 3 -6 8522.21 355.818 19 12 -3 6 9279.56 414.185 7 12 -3 7 112.401 96.9010 7 -12 3 -7 160.573 76.3333 8 -12 3 -7 319.850 79.7975 19 -12 3 -8 2277.22 163.635 8 -12 3 -8 2313.16 161.369 19 12 3 8 2333.61 166.596 16 12 -3 8 2094.74 185.935 7 -12 3 -9 1842.06 146.578 8 -12 3 -9 1576.33 134.580 19 12 3 9 1634.19 136.965 16 12 -3 9 1626.51 159.979 7 -12 3 -10 9023.19 356.556 8 -12 3 -10 8570.52 348.402 19 12 3 10 9385.85 355.494 16 12 -3 10 9289.95 391.456 7 -12 3 -11 1409.40 124.920 8 12 3 11 1270.73 112.721 16 12 -3 11 1457.53 146.531 7 -12 3 -12 9867.93 369.350 8 12 3 13 5.16496 41.1653 23 -12 3 -13-6.67577 52.8009 8 -12 3 -13 44.9121 43.2143 10 12 -3 14 374.174 79.0931 12 12 3 14 401.157 57.6338 23 -12 3 -14 329.161 65.5111 8 12 -3 15 5712.92 236.062 12 -12 3 -15 6333.10 230.503 8 12 -3 16 392.941 60.0430 12 12 4 -13 2171.04 123.082 24 12 4 -12 1813.50 124.582 24 12 4 -12 2003.39 111.483 21 12 4 -11 112.167 54.2625 24 12 4 -11 126.926 45.4158 21 12 4 -10 180.669 68.1712 24 12 4 -10 112.256 51.2538 21 12 4 -9 1557.26 116.243 21 -12 4 8 1510.36 92.8779 8 12 4 -8 1602.78 140.690 24 12 4 -8 1405.79 116.580 21 12 4 -7 304.685 92.6324 24 12 4 -7 282.700 72.0819 21 -12 4 7 211.687 50.5303 8 -12 4 6 580.482 71.0819 8 12 4 -6 478.941 103.955 24 12 4 -6 612.070 91.3916 21 -12 4 5 3269.89 162.397 8 12 4 -5 2837.83 200.804 24 12 4 -5 3147.23 185.823 21 12 4 -4 458.088 102.549 24 12 4 -4 335.169 79.7264 21 -12 4 4 356.467 68.1301 8 -12 4 3 3636.53 183.101 8 12 4 -3 3210.01 223.347 24 12 4 -3 3475.40 199.345 21 -12 4 2 2822.48 165.762 8 12 4 -2 3348.25 224.022 24 12 4 -2 3162.17 192.870 21 12 4 -1 376.975 108.598 24 12 4 -1 382.575 85.3150 21 -12 4 1 398.751 79.2513 8 -12 4 0 2604.55 157.428 8 12 4 0 2400.42 194.331 24 12 4 0 2325.99 167.217 21 -12 4 -1 694.187 90.0234 8 12 4 1 622.791 96.8512 21 -12 4 -2 8525.46 329.891 8 -12 4 -3 1274.68 117.234 8 -12 4 -4 3636.72 193.620 8 -12 4 -5 9762.32 363.720 8 -12 4 -6 716.197 91.4960 8 -12 4 -7 1218.00 110.517 8 12 4 7 1335.58 118.288 16 12 4 8 123.715 62.7855 16 -12 4 -9 253.163 65.0161 10 12 4 9 231.057 64.2232 16 -12 4 -10 181.189 52.0086 10 12 4 10 187.436 53.2076 16 -12 4 -11 183.094 53.9456 8 -12 4 -11 178.134 45.0004 10 12 4 11 188.700 49.9469 16 -12 4 -12-2.45050 40.6544 8 -12 5 -1 824.064 67.2237 10 -12 5 -2 112.431 38.0226 10 -12 5 -3 281.528 46.1454 10 12 5 3 283.125 53.8514 16 -12 5 -4 3041.99 132.956 10 12 5 4 2460.37 129.583 16 -13 0 19 3128.16 123.580 8 -13 0 17 1369.38 80.2104 20 -13 0 16 39.6619 39.2942 20 13 0 -16 30.0431 49.6715 11 13 0 -15 4529.77 223.652 11 -13 0 15 4144.26 183.982 20 -13 0 14 51.4949 52.6596 20 13 0 -14 4.42402 58.2317 11 -13 0 13 600.315 83.0288 20 13 0 -13 790.786 110.888 11 13 0 -12 142.732 86.8511 11 13 0 -11 24826.7 822.416 11 13 0 -10-23.7949 81.7023 11 13 0 -9 10149.9 444.724 11 -13 0 9 10087.5 392.994 20 -13 0 8 26.2766 73.4146 20 13 0 -8-12.8576 90.0779 11 -13 0 7 4975.80 258.949 20 -13 0 6-12.2113 60.8217 8 -13 0 6 60.6407 83.8809 20 -13 0 5 1977.79 147.828 8 -13 0 5 1964.87 167.592 20 -13 0 4 20.4544 59.2555 8 -13 0 4 14.6455 84.5934 20 -13 0 3 5455.48 255.103 8 -13 0 3 4682.78 272.138 20 -13 0 2 52.9290 61.0994 8 -13 0 2-50.3574 86.1339 20 -13 0 1 1665.07 134.712 8 -13 0 0 3.97743 56.8121 8 -13 0 -1 37232.6 1079.52 8 -13 0 -2 76.0047 59.2002 8 -13 0 -2 20.4861 94.0070 20 -13 0 -3 30285.8 858.154 8 -13 0 -3 26481.3 892.469 20 -13 0 -4 53.0711 49.8246 8 -13 0 -4-5.07076 83.2431 20 -13 0 -5 3241.99 216.295 20 13 0 5 3533.53 267.805 7 13 0 6-36.7128 107.327 7 13 0 7 2628.44 230.876 7 13 0 8 90.2646 109.008 7 -13 0 -9 1642.94 148.003 19 13 0 9 1749.10 186.114 7 13 0 10-19.1216 103.879 7 -13 0 -10 8.95779 66.0534 19 -13 0 -11 11275.5 432.369 19 13 0 11 12084.1 490.086 7 13 0 12-5.64544 89.3014 7 -13 0 -12 24.3583 61.4415 19 -13 0 -13 2073.90 146.207 19 13 0 13 1675.79 162.265 7 -13 0 -14 58.4265 57.8287 19 13 0 15 29159.9 883.442 12 -13 0 -15 29716.0 851.089 19 13 0 16 13.7934 61.0797 12 13 0 17 2237.84 136.278 12 13 0 17 2394.09 142.447 23 13 0 18 36.8193 46.9493 23 -13 1 18 3028.04 123.947 8 -13 -1 18 2720.08 119.700 20 -13 1 17 14075.6 425.315 8 13 1 -17 14277.8 468.121 11 -13 1 16 1992.95 113.756 8 13 1 -16 1983.27 143.765 11 -13 -1 16 1989.81 116.067 17 -13 1 15 150.848 50.4964 8 13 1 -15 91.6336 66.9278 11 -13 -1 15 86.5017 58.1438 17 -13 1 14 1179.41 98.3204 8 13 1 -14 1120.84 129.271 11 -13 -1 14 1089.13 104.001 17 -13 1 13 7361.11 280.498 8 13 1 -13 7581.04 336.444 11 -13 1 13 6224.49 244.363 20 -13 -1 13 6674.19 276.640 17 13 1 -12 808.631 98.8429 24 -13 1 12 649.429 76.3321 20 13 1 -12 779.388 122.111 11 -13 -1 12 762.270 102.120 17 13 1 -11 1177.78 122.363 24 -13 1 11 947.208 94.6669 20 13 1 -11 1165.23 150.112 11 -13 -1 11 1097.57 117.071 17 13 1 -10 1307.64 132.653 24 13 1 -10 1443.25 160.465 11 -13 1 10 1298.91 112.540 20 -13 -1 10 1413.27 133.843 17 -13 1 9 20435.8 676.424 8 13 1 -9 21614.2 722.482 24 13 1 -9 22967.0 780.333 11 -13 1 9 21626.7 671.384 20 -13 -1 9 21973.6 692.206 17 -13 1 8 2931.40 181.754 8 13 1 -8 2884.98 201.386 24 13 1 -8 2717.52 223.675 11 -13 1 8 2846.99 174.362 20 13 1 -7 96.7304 85.0255 24 -13 1 7 33.1378 67.7578 8 -13 1 7-16.2389 66.8843 20 13 1 -7 84.0111 106.401 11 13 1 -6 11.7866 83.4080 24 -13 1 6 143.936 77.9478 8 -13 1 6 46.6941 80.1313 20 13 1 -6 193.164 114.486 11 -13 -1 5 45762.1 1271.93 8 -13 1 5 46241.6 1305.12 8 13 1 -5 43709.2 1351.66 24 -13 1 5 45509.0 1303.87 20 -13 -1 4 2499.07 152.995 8 -13 1 4 2448.98 173.077 8 13 1 -4 2778.40 213.259 24 -13 -1 4 2421.92 185.996 20 -13 1 4 2663.23 179.464 20 -13 -1 3 8713.79 337.628 8 -13 1 3 9502.67 374.631 8 13 1 -3 8812.85 415.685 24 -13 -1 3 9954.90 395.240 20 -13 1 3 9322.14 382.701 20 -13 -1 2 680.583 80.2498 8 13 1 -2 678.425 123.699 24 -13 1 2 789.644 109.738 8 -13 -1 2 887.374 130.601 20 -13 1 2 839.331 119.369 20 -13 1 1 18801.8 619.666 8 13 1 -1 17030.4 664.576 24 -13 -1 1 19221.4 637.178 20 -13 1 1 18094.7 627.157 20 -13 1 0 1981.60 157.536 8 13 1 0 2217.41 198.977 24 -13 -1 0 2460.69 184.591 20 -13 1 0 2220.96 177.467 20 -13 1 -1 2714.82 178.323 8 13 1 1 2690.84 217.814 24 -13 -1 -1 2786.99 194.769 20 -13 1 -1 2524.03 187.068 20 -13 1 -2 3816.71 212.585 8 -13 -1 -2 3707.48 226.047 20 -13 1 -2 3622.38 226.694 20 13 1 3 28.8205 107.684 2 13 -1 3 71.6016 102.298 2 -13 1 -3 143.971 68.5467 8 -13 -1 -3 62.7267 82.5619 20 -13 1 -4 481.679 86.0872 8 -13 -1 -4 508.264 105.550 20 13 1 4 241.506 118.718 2 13 -1 4 402.718 130.459 2 13 1 4 379.531 109.075 7 13 1 5 2070.07 202.531 2 13 -1 5 2006.03 207.708 2 -13 1 -5 2238.78 155.521 8 -13 -1 -5 2538.33 178.253 20 13 -1 5 1922.58 216.647 7 13 1 5 2118.56 191.732 7 13 -1 6-53.1820 128.230 7 13 1 6 85.3902 96.1109 7 -13 1 -6 27.5040 54.5159 8 13 1 6 41.1034 99.6827 2 13 -1 6 27.2148 106.376 2 13 1 7 4307.27 276.365 2 13 -1 7 4409.36 279.438 2 -13 1 -7 3911.95 206.724 8 13 -1 7 4176.50 294.945 7 13 1 7 3653.10 243.356 7 13 -1 8 136.788 128.022 7 13 1 8 168.210 88.8552 7 -13 1 -8 265.823 66.6645 8 13 1 8 273.661 122.069 2 13 -1 8 162.586 101.821 2 -13 1 -9 40364.1 1121.43 8 13 1 9 41282.7 1224.84 2 13 -1 9 42174.9 1230.62 2 -13 -1 -9 38788.1 1137.45 19 13 -1 9 41927.1 1252.39 7 13 1 9 40861.7 1186.91 7 13 -1 10 510.113 139.657 7 13 1 10 335.953 108.932 2 13 -1 10 450.711 122.332 2 13 1 10 444.779 94.3839 7 -13 -1 -10 607.422 86.9837 19 -13 1 -10 611.534 101.849 19 13 -1 11 981.895 152.638 7 13 1 11 746.596 108.209 7 -13 -1 -11 1023.91 103.434 19 -13 1 -11 1128.78 123.323 19 13 -1 12 620.633 128.399 7 -13 -1 -12 728.618 84.3934 19 -13 1 -12 610.987 98.5515 19 -13 -1 -13 1631.11 113.954 19 -13 1 -13 1809.77 141.434 19 13 -1 13 1928.15 173.418 7 -13 1 -14 1353.87 118.395 19 13 1 15 428.756 85.6699 23 13 -1 16 6892.56 291.538 12 13 1 16 6859.23 275.702 23 13 -1 17 20639.1 606.722 12 13 1 17 19775.9 588.517 23 13 -1 18 316.654 60.2170 12 13 1 18 400.616 58.5828 23 -13 2 16 5317.70 192.427 8 -13 -2 16 6304.81 214.428 17 13 2 -15 138.676 52.1290 24 -13 2 15 192.155 41.2001 8 13 2 -14 113.418 58.2609 24 -13 2 14 98.0983 43.0489 8 -13 2 13 2317.85 127.640 8 13 2 -13 1807.69 142.972 24 -13 2 12 4930.17 209.991 8 13 2 -12 4494.08 239.926 24 -13 -2 12 4556.13 214.738 17 -13 2 11 7951.02 294.014 8 13 2 -11 7365.22 331.228 24 13 2 -11 6781.13 343.427 11 -13 -2 11 7820.89 300.632 17 -13 2 10 947.399 98.5091 8 13 2 -10 957.219 126.497 24 13 2 -10 783.797 129.562 11 -13 -2 10 914.056 107.743 17 -13 2 9 2274.06 150.987 8 13 2 -9 2491.95 186.751 24 13 2 -9 2264.53 194.202 11 -13 -2 9 2114.26 151.569 17 -13 2 8 2063.66 147.658 8 13 2 -8 1747.89 169.792 24 13 2 -8 2095.65 192.277 11 -13 -2 8 1994.73 149.497 17 -13 2 7 3986.13 208.759 8 13 2 -7 3776.82 247.953 24 -13 2 7 3651.15 179.968 20 -13 -2 7 3921.56 211.506 17 -13 2 6 2967.87 185.061 8 13 2 -6 3069.06 223.276 24 -13 2 6 2942.57 162.117 20 13 2 -5 298.890 110.642 24 -13 2 5 145.498 62.6455 20 13 2 -4 11048.9 487.428 24 -13 -2 4 11860.8 435.473 20 13 2 -3 17441.9 642.030 24 -13 -2 3 17558.6 569.161 20 -13 2 2 7070.72 311.637 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6608.01 327.992 2 -13 2 -6 6889.25 307.592 19 13 -2 6 7027.12 368.504 7 -13 2 -7 7104.27 302.423 8 13 2 7 7190.54 335.480 2 13 -2 7 7201.78 335.151 2 -13 2 -7 6765.15 307.967 19 13 -2 7 7125.88 371.787 7 13 -2 8 819.111 143.284 7 13 2 8 621.028 106.965 2 -13 2 -8 999.228 116.541 19 -13 2 -8 660.974 93.6929 8 -13 2 -9 4234.35 212.098 8 -13 2 -9 4094.80 225.715 19 13 -2 9 3961.35 263.968 7 13 2 10 2252.28 153.807 23 -13 2 -10 2174.16 145.269 8 -13 2 -10 2161.59 159.337 19 13 -2 10 2328.77 198.511 7 13 2 11 6664.23 279.513 23 -13 2 -11 6619.54 272.493 8 -13 2 -11 6346.86 284.319 19 13 -2 11 6838.27 332.314 7 13 2 12 4582.69 212.545 23 -13 2 -12 3999.69 192.772 8 -13 2 -12 4015.42 212.586 19 13 -2 12 4014.22 240.278 7 13 2 13 158.645 61.7036 23 -13 2 -13 276.029 77.7924 19 -13 2 -13 386.665 59.6982 8 13 2 14 798.335 86.3325 23 13 -2 15 8740.46 330.711 12 13 2 15 8153.66 296.913 23 13 -2 16-2.96184 56.7947 12 13 2 16 50.5272 38.9198 23 13 -2 17 269.306 53.2278 12 13 3 -12 48.4869 50.6322 24 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20 -13 3 1 4466.09 219.161 8 13 3 -1 4352.48 268.033 24 13 3 -1 3986.86 210.209 21 -13 -3 1 4206.97 194.227 20 13 3 0-6.17034 94.1648 24 13 3 0-18.9148 53.0057 21 -13 3 0 57.2085 66.0877 8 13 -3 0 32.8938 87.3852 7 13 -3 1 5.49839 84.9481 7 13 3 1-18.5282 106.334 24 13 3 1 37.2023 54.3839 21 -13 3 -1 52.7333 46.7558 19 -13 3 -2 3233.11 172.918 19 13 -3 2 3733.02 233.381 7 -13 3 -3 9196.85 369.582 8 -13 3 -3 10378.1 363.110 19 13 -3 3 10388.1 426.686 7 -13 3 -4 2005.78 145.358 8 -13 3 -4 1924.74 133.200 19 13 -3 4 1865.89 169.113 7 -13 3 -5 3948.25 210.570 8 -13 3 -5 4335.74 206.309 19 13 -3 5 4045.74 240.793 7 -13 3 -6 6254.10 270.885 8 -13 3 -6 6357.09 264.790 19 13 -3 6 6292.47 304.262 7 13 -3 7 922.625 122.671 7 -13 3 -7 885.125 100.367 8 -13 3 -7 899.866 95.6329 19 13 -3 8 18.0285 72.9268 7 -13 3 -8 44.8817 55.4526 8 -13 3 -8 38.7163 53.9069 19 -13 3 -9 1337.33 112.377 8 -13 3 -9 1335.20 108.523 19 13 -3 9 1319.70 129.544 7 13 -3 10 530.309 90.6853 7 -13 3 -10 448.262 74.5285 8 -13 3 -11 1335.83 104.855 8 13 -3 12 861.207 92.4860 12 -13 3 -12 1061.33 87.9968 8 -13 3 -12 1060.48 75.2224 10 13 -3 13 5099.56 209.108 12 -13 3 -13 5073.39 196.980 8 13 4 -9 328.997 59.5971 24 13 4 -8 578.455 73.6548 24 13 4 -8 492.255 55.8362 21 13 4 -7 1739.57 123.378 24 13 4 -7 1797.42 105.268 21 -13 4 6 1280.85 79.6941 8 13 4 -6 1611.01 123.235 24 13 4 -6 1509.45 99.4630 21 -13 4 5 5977.24 214.355 8 13 4 -5 5933.18 261.157 24 13 4 -5 5558.93 226.575 21 -13 4 4 7429.22 252.873 8 13 4 -4 6808.23 292.837 24 13 4 -4 6599.15 261.212 21 -13 4 3 6401.50 237.471 8 13 4 -3 6455.89 284.303 24 13 4 -3 6274.83 247.927 21 -13 4 2 5948.84 230.474 8 13 4 -2 5874.29 238.046 21 -13 4 1 755.564 76.4109 8 -13 4 0 79.0836 47.4443 8 -13 4 -1 185.603 56.1701 8 -13 4 -2 942.408 86.8454 8 -13 4 -3 1650.48 113.030 8 -13 4 -4 191.311 53.6073 8 -13 4 -5 6095.15 222.461 8 13 4 5 4033.81 187.707 16 -13 4 -6 20.6583 43.8892 8 13 4 6 57.8626 39.1901 16 -13 4 -7 90.7828 45.8577 10 -13 4 -8 725.428 70.1075 10 -13 4 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82.4367 104.115 7 14 0 6 1136.78 152.297 7 14 0 7 5.91165 95.6453 7 -14 0 -8 9505.22 377.905 19 14 0 8 10622.4 433.217 7 14 0 9 53.1583 85.3776 7 -14 0 -9 38.4548 63.5835 19 -14 0 -10 1460.31 121.653 19 14 0 10 1391.65 144.980 7 14 0 11 82.4529 77.3229 7 -14 0 -11 33.8979 56.6438 19 -14 0 -12 28451.1 830.582 19 14 0 12 28543.8 866.334 7 -14 0 -13 30.2207 48.0672 19 14 0 14 106.622 56.7008 12 14 0 15-9.54325 40.9425 12 -14 1 16 27.9202 24.8124 8 -14 -1 15 162.759 33.9567 8 -14 1 15 169.454 37.0107 8 -14 -1 15 168.992 39.0883 20 -14 -1 14-7.10205 30.4688 8 -14 1 14 14.1940 36.2450 8 -14 -1 14 8.55086 38.4406 20 -14 -1 13 99.9688 38.0452 8 -14 -1 13 150.114 51.9729 20 -14 -1 12 1986.29 111.491 8 -14 -1 12 1830.56 123.573 20 -14 -1 11 2618.58 132.002 8 -14 -1 11 2421.63 147.237 20 -14 1 11 2318.93 122.602 20 -14 -1 10 549.582 69.0362 8 -14 1 10 586.354 78.1367 8 -14 -1 10 485.782 85.7470 20 -14 1 10 476.336 65.6199 20 -14 -1 9 4985.23 210.164 8 -14 1 9 5365.49 230.575 8 -14 -1 9 5361.76 243.810 20 -14 1 9 5045.76 215.525 20 -14 -1 8 6949.29 259.302 8 -14 1 8 7115.47 280.111 8 -14 1 8 6389.39 264.619 20 14 1 -7 372.380 79.9039 24 -14 -1 7 404.051 62.2153 8 -14 1 7 340.014 76.1501 8 -14 1 7 277.093 70.1799 20 -14 -1 6 6958.54 263.421 8 -14 1 6 7334.90 290.722 8 14 1 -6 6465.45 301.250 24 -14 1 6 6741.55 282.543 20 -14 -1 5 3697.37 175.954 8 -14 1 5 4117.83 205.595 8 14 1 -5 3912.54 223.021 24 -14 -1 5 3680.36 213.617 20 -14 1 5 3849.36 203.580 20 14 1 -4 333.665 85.8550 24 -14 -1 4 365.673 59.8623 8 -14 1 4 362.155 79.1984 8 -14 -1 4 471.037 95.5614 20 -14 1 4 480.633 93.0880 20 14 1 -3 106.436 77.0440 24 -14 1 3 78.2693 61.4204 8 -14 -1 3 42.1216 73.0055 20 -14 1 3 23.6735 74.2685 20 -14 1 2 37.4530 58.7907 8 -14 -1 2 59.5122 74.8334 20 -14 1 2-8.11043 68.6776 20 -14 1 1 2496.38 159.948 8 -14 -1 1 2703.06 181.917 20 -14 1 1 2469.37 170.529 20 -14 1 0 1666.48 131.059 8 -14 -1 0 1690.72 148.597 20 -14 1 0 1484.89 140.031 20 14 -1 0 1911.55 183.284 2 -14 1 -1 2190.88 147.911 8 -14 -1 -1 2066.92 159.428 20 14 1 1 2021.52 192.810 2 14 -1 1 1979.67 186.139 2 -14 1 -2 2110.36 143.474 8 -14 -1 -2 2181.48 161.794 20 14 1 2 2152.09 180.792 7 14 1 2 2027.07 197.620 2 14 -1 2 2473.38 203.050 2 14 1 3 2873.18 225.721 2 14 -1 3 3082.96 231.536 2 -14 1 -3 3298.87 178.568 8 -14 -1 -3 3489.34 198.672 20 14 1 3 2948.99 207.085 7 14 1 4 738.754 113.312 7 -14 1 -4 680.772 86.6606 8 -14 -1 -4 679.659 100.142 20 14 1 4 643.694 135.630 2 14 -1 4 676.363 125.697 2 14 -1 4 580.114 131.910 7 14 -1 5 1038.01 154.851 7 14 1 5 956.749 123.618 7 -14 1 -5 1034.15 98.7350 8 14 1 5 965.184 144.452 2 14 -1 5 859.566 134.557 2 14 1 6 13675.2 531.426 2 14 -1 6 14084.2 537.669 2 -14 1 -6 13584.0 452.219 8 14 -1 6 13716.9 548.651 7 14 1 6 13374.5 496.518 7 -14 1 -7 2450.23 141.168 8 14 1 7 2704.77 206.698 2 14 -1 7 2142.57 183.378 2 14 -1 7 2561.09 209.246 7 14 1 7 2311.36 168.317 7 14 1 8 423.223 105.127 2 14 -1 8 490.867 107.414 2 14 -1 8 355.847 110.311 7 14 1 8 407.252 82.6700 7 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4904.93 208.746 19 14 -2 11 4682.28 233.564 7 14 2 12 2366.27 116.401 23 14 -2 13 5189.96 224.018 12 14 -2 14 2585.56 135.156 12 14 3 -10-2.63729 37.5122 24 -14 3 10 76.9086 26.7580 8 -14 3 9 1005.00 70.0899 8 -14 -3 9 1155.37 73.0607 20 -14 3 8 17645.9 492.099 8 14 3 -8 17140.5 537.922 24 14 3 -7 14.3466 54.9618 24 -14 3 7 8.48612 36.0493 8 -14 -3 7 15.1900 33.1133 20 14 3 -6 26.8401 61.8145 24 -14 3 6 59.8137 41.5023 8 -14 -3 6 25.7040 36.9171 20 -14 3 5 21984.2 632.271 8 14 3 -5 22144.3 685.867 24 -14 -3 5 20679.6 612.901 20 14 -3 -5 21958.1 662.003 7 -14 3 4 953.983 87.1168 8 14 3 -4 1150.60 119.752 24 -14 -3 4 992.727 75.7172 20 14 -3 -4 983.835 102.184 7 14 3 -3 87.1756 76.0886 24 -14 3 3 167.869 51.8906 8 -14 -3 3 129.085 40.9820 20 14 -3 -3 144.726 66.8180 7 14 -3 -2 103.665 63.2631 7 -14 3 2 19.5711 48.1520 8 14 -3 -1 78.5507 67.4274 7 14 -3 0 1372.41 125.705 7 14 -3 1 534.697 91.4437 7 -14 3 -2 4654.71 207.590 8 14 -3 2 4542.56 230.167 7 -14 3 -3 11269.2 373.374 8 14 -3 3 11485.5 404.788 7 14 -3 4 15.1210 59.8041 7 -14 3 -4 31.5719 48.6147 8 -14 3 -4 51.2198 40.1751 19 -14 3 -5 2465.56 138.615 8 -14 3 -5 2346.44 123.292 19 14 -3 5 2509.18 159.515 7 -14 3 -6 5149.88 205.118 8 14 -3 6 4740.24 219.751 7 -14 3 -7 3161.09 155.106 8 14 -3 7 3232.29 173.053 7 14 -3 8 23.8379 44.9114 7 -14 3 -8 31.1340 41.7701 8 -14 3 -9-2.20245 36.1540 8 -14 3 -10 7874.04 262.607 8 -15 0 13 963.230 62.1216 8 -15 0 12 29.7346 27.3150 8 -15 0 12 12.4954 27.9241 20 -15 0 11 42.6855 35.3260 8 -15 0 11 58.6422 36.3870 20 -15 0 10 16.2404 34.7236 8 -15 0 10 2.18036 39.4409 20 -15 0 9 31647.8 866.708 8 -15 0 9 30725.9 873.124 20 -15 0 8 29.8972 39.4684 8 -15 0 8 2.66496 52.0268 20 -15 0 7 4893.65 198.727 8 -15 0 7 4628.03 209.614 20 -15 0 6 61.4238 45.7455 8 -15 0 6 21.2058 54.1614 20 -15 0 5 32153.7 901.891 8 -15 0 5 32343.1 927.471 20 -15 0 4 87.9012 47.6885 8 -15 0 4 62.6237 68.1605 20 -15 0 3 11340.7 383.384 8 -15 0 3 12859.9 423.534 20 -15 0 2 29.6100 40.5095 8 -15 0 2 10.4059 66.6828 20 -15 0 1 6116.15 232.292 8 -15 0 0 13.8484 34.6377 8 15 0 1 1830.67 165.802 7 15 0 2-25.4780 84.2436 7 15 0 3 11287.1 442.830 7 15 0 4 14.5607 78.5269 7 15 0 5 9803.97 394.823 7 15 0 6 8.87978 73.1424 7 -15 0 -6 9.80316 57.5237 19 -15 0 -7 2587.52 150.574 19 15 0 7 2696.99 176.539 7 15 0 8 11.6683 66.3071 7 -15 0 -8-8.86612 48.1656 19 -15 0 -9 8006.82 295.076 19 15 0 9 8193.66 319.698 7 15 0 10-15.9069 51.8493 7 -15 0 -10-2.50556 44.5161 19 -15 0 -11 1918.52 109.364 19 -15 0 -12 11.0056 28.1092 19 15 0 13 563.392 60.2317 23 -15 1 12 141.256 35.6074 8 -15 -1 12 89.0553 34.7133 20 -15 1 11 10634.6 336.320 8 -15 -1 11 10916.6 343.325 20 -15 -1 10 195.683 31.7323 8 -15 1 10 206.071 43.3169 8 -15 -1 10 211.532 51.1681 20 -15 -1 9 432.394 44.9435 8 -15 1 9 454.737 56.7392 8 -15 1 8 787.263 74.5013 8 -15 1 8 805.971 70.4905 20 -15 1 7 1911.02 116.493 8 -15 1 7 1634.38 104.673 20 -15 1 6 6493.15 244.387 8 -15 1 6 5950.93 235.445 20 -15 1 5 417.536 63.9634 8 -15 -1 5 394.259 77.9250 20 -15 1 5 291.909 62.7234 20 -15 1 4 330.335 62.7942 8 -15 -1 4 385.809 76.3759 20 -15 1 3 9982.50 342.798 8 -15 -1 3 9831.38 354.600 20 15 1 -3 9499.68 391.040 2 15 -1 -3 9562.03 390.614 2 -15 1 2 1898.38 123.297 8 -15 -1 2 2082.31 140.114 20 15 1 -2 2018.30 165.898 2 15 -1 -2 2052.49 169.643 2 15 1 -1 184.914 84.8835 2 -15 1 1 169.786 53.8550 8 15 -1 -1 123.448 85.2565 2 -15 -1 1 229.680 71.1182 20 15 1 -1 231.937 71.8906 7 15 1 0 133.157 67.2792 7 -15 1 0 118.101 50.5025 8 -15 -1 0 98.0760 65.1711 20 15 1 0 104.746 82.5604 2 15 -1 0 199.989 90.1481 2 15 1 1 12607.8 479.002 2 15 -1 1 13391.2 484.453 2 -15 1 -1 12432.1 416.406 8 -15 -1 -1 13029.2 436.957 20 15 -1 1 13241.5 499.880 7 15 1 1 12923.2 455.186 7 15 -1 2 440.330 110.090 7 15 1 2 419.288 81.1657 7 -15 1 -2 398.169 63.2332 8 15 1 2 647.416 104.886 2 15 -1 2 313.846 92.9785 2 15 1 3 4268.53 237.630 2 15 -1 3 4776.15 247.054 2 -15 1 -3 4311.27 186.546 8 15 -1 3 4638.55 255.077 7 15 1 3 4140.22 210.168 7 15 -1 4 10.0443 87.5828 7 15 1 4 3.41133 48.5012 7 -15 1 -4 44.7467 39.7555 8 -15 1 -4 19.8979 57.2853 19 15 1 4 45.1000 76.8901 2 15 -1 4 49.5552 71.8111 2 15 -1 5 373.555 93.3976 7 -15 1 -5 330.370 49.7546 8 -15 1 -5 273.059 68.7636 19 15 1 5 341.948 90.1940 2 15 -1 5 428.729 93.0260 2 15 -1 6 889.597 120.562 7 15 1 6 999.340 115.762 2 15 -1 6 1189.53 121.086 2 -15 -1 -6 767.731 81.2123 19 -15 1 -6 646.840 86.4891 19 -15 -1 -7 1900.35 116.617 19 15 -1 7 2074.17 160.407 7 -15 -1 -8 2565.89 131.635 19 15 -1 8 2524.05 169.856 7 -15 1 -9 2858.88 154.604 19 15 -1 9 3356.96 187.065 7 15 1 10 1314.48 91.4308 23 -15 1 -10 1396.26 99.2640 19 15 -1 10 1271.85 113.788 7 15 1 11 6705.88 239.075 23 -15 1 -11 6931.03 248.543 19 -15 2 10 1069.91 67.4673 8 -15 2 9 1172.39 77.0444 8 -15 -2 9 1248.64 81.3550 20 -15 -2 8 3196.46 143.365 20 -15 -2 7 984.889 78.6083 20 15 2 -7 597.572 64.0301 2 15 -2 -6 5700.78 228.289 2 15 2 -6 5701.70 227.160 2 15 2 -5 8548.74 313.885 2 15 -2 -5 8941.99 317.405 2 -15 2 5 9721.68 315.362 8 -15 -2 5 9232.17 311.225 20 -15 2 4 2.43928 41.8609 8 -15 -2 4 35.9559 45.4777 20 15 2 -4 36.9121 47.5991 2 15 -2 -4-14.1977 46.2792 2 15 2 -3 4404.10 202.268 2 15 -2 -3 4540.23 204.630 2 -15 2 3 4926.84 198.260 8 -15 -2 3 5026.15 198.102 20 -15 2 3 4254.91 174.749 19 15 -2 -2 745.500 85.8438 2 -15 2 2 765.026 78.0240 8 -15 -2 2 874.091 80.3094 20 -15 2 2 853.107 71.9859 19 15 2 -2 638.884 82.6838 2 15 -2 -2 745.669 107.634 7 -15 2 1 561.167 71.2056 8 -15 -2 1 418.218 64.2047 20 -15 2 1 380.411 55.3308 19 15 2 -1 510.041 76.5217 2 15 -2 -1 558.623 76.3645 2 15 -2 -1 531.171 97.3686 7 15 2 0 5594.08 238.930 2 15 -2 0 5760.83 239.299 2 -15 2 0 5851.42 226.592 8 -15 -2 0 5551.51 218.958 20 -15 2 0 5272.94 214.529 19 15 -2 0 5695.98 274.062 7 15 2 1 1203.30 104.058 2 -15 2 -1 1456.75 103.048 8 15 -2 1 1249.25 107.195 2 -15 2 -1 1386.30 97.8889 19 15 -2 1 1275.98 132.097 7 -15 2 -2 1321.25 97.6908 8 15 2 2 1260.58 104.771 2 15 -2 2 1223.06 102.972 2 -15 2 -2 1249.07 95.6902 19 15 -2 2 1280.94 133.698 7 -15 2 -3 3043.55 148.826 8 15 2 3 3006.85 160.873 2 15 -2 3 3175.71 162.607 2 -15 2 -3 2813.24 146.951 19 15 -2 3 2834.37 184.939 7 15 -2 4 90.5715 71.1194 7 -15 2 -4 66.4995 43.3563 8 -15 -2 -4 22.4979 29.5691 19 -15 2 -4 87.3400 47.4307 19 -15 2 -5 7397.61 260.292 8 -15 2 -5 7267.79 268.116 19 15 -2 5 7066.83 305.636 7 -15 2 -6 2597.40 127.063 8 -15 2 -6 2448.42 133.988 19 15 -2 6 2881.90 172.639 7 -15 2 -7 1016.07 72.9624 8 -15 2 -7 940.382 81.1258 19 15 -2 7 1135.23 110.001 7 -15 2 -8 710.879 69.4138 19 15 -2 8 810.189 94.0884 7 -15 2 -9 4467.32 181.420 19 15 -2 9 4889.32 211.314 7 -15 3 5 148.567 32.5448 8 -15 3 3 2390.71 111.341 8 -15 3 0 337.952 48.4712 8 -15 3 -1 284.094 45.2322 8 -15 3 -2 1760.50 96.4102 8 -15 3 -3 3348.75 141.433 8 -15 3 -4 2460.63 114.411 8 -16 0 7 64.2893 35.1356 20 -16 0 6 9231.01 300.179 20 16 0 -3 32.3377 57.9823 7 16 0 -2 27745.4 816.428 7 16 0 -1 49.8588 56.3035 7 16 0 0 835.487 92.1886 7 16 0 1 29.3577 55.4304 7 16 0 2 6023.67 252.350 7 16 0 3-9.15188 49.7181 7 -16 0 -3 14.3610 42.6541 19 -16 0 -4 1190.01 85.9805 19 16 0 4 781.782 83.4120 7 16 0 5 32.3435 45.9633 7 -16 0 -5 55.4859 40.9807 19 -16 0 -6 9729.66 319.123 19 16 0 6 9982.52 333.904 7 -16 0 -7 30.6223 33.6999 19 16 1 -6 547.038 65.1800 2 -16 1 6 372.629 42.9262 8 16 -1 -6 487.857 62.7572 2 16 1 -5 5979.74 237.470 2 16 -1 -5 6220.90 240.312 2 -16 1 5 6176.85 210.056 8 -16 -1 5 6446.40 224.242 20 16 1 -4 3733.17 174.568 2 16 -1 -4 3787.32 175.713 2 -16 1 4 3379.05 141.757 8 -16 -1 4 3683.29 156.515 20 16 -1 -4 3611.08 183.697 7 -16 1 3 134.121 34.2139 8 -16 -1 3 125.731 43.8151 20 16 1 -3 80.2914 49.1457 2 16 -1 -3 124.702 55.8358 2 16 -1 -3 157.961 65.1850 7 16 1 -2 2142.11 130.561 2 16 -1 -2 2193.78 133.069 2 -16 1 2 1755.29 94.0867 8 16 -1 -2 1854.02 133.747 7 16 -1 -1 616.006 88.6947 7 -16 1 1 589.699 52.6240 8 -16 1 1 674.600 65.2365 19 16 1 -1 608.313 78.5604 2 16 -1 -1 647.169 80.4663 2 16 1 0 9229.03 320.278 2 16 -1 0 8923.68 317.828 2 16 -1 0 8660.42 328.618 7 16 1 1 1053.65 96.0816 2 16 -1 1 1067.29 96.3638 2 -16 1 -1 773.860 72.2161 19 16 -1 1 1057.65 103.565 7 16 1 2 967.556 92.6630 2 16 -1 2 994.719 94.1204 2 16 -1 2 1187.35 109.667 7 16 1 3 157.631 56.9068 2 16 -1 3 121.102 53.7913 2 16 -1 3 274.368 70.7317 7 -16 -1 -3 132.068 39.3226 19 -16 1 -3 118.816 44.4895 19 16 1 4 3433.42 162.279 2 16 -1 4 3542.70 164.795 2 -16 1 -4 3017.26 140.694 19 16 -1 4 3488.56 173.536 7 16 -1 5 38.5250 48.2999 7 -16 1 -5 8.34634 36.2752 19 16 -1 6 82.4298 49.1477 7 -16 1 -6 67.4979 37.8081 19 16 -1 7 2040.90 120.222 7 16 -2 -2 228.153 51.9354 7 16 -2 -1 2453.59 131.744 7 16 -2 0 27.6307 38.4976 7 16 -2 1 4837.52 199.947 7 16 -2 2 3360.64 158.779 7 0 0 0 0.00 0.00 0 TITL 1 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 13.401735 5.921057 24.391702 90.0000 90.1424 90.0000 ZERR 8.00 0.000201 0.000105 0.000382 0.0000 0.0014 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O UNIT 88.00 80.00 8.00 8.00 TREF HKLF 4 END ; _shelx_hkl_checksum 10737 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.457 _oxdiff_exptl_absorpt_empirical_full_min 0.601