####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_FDC-1-as_synthesized _database_code_depnum_ccdc_archive 'CCDC 2100317' loop_ _audit_author_name _audit_author_address 'Ken-ichi Otake' ;Kyoto University Japan ; _audit_update_record ; 2022-07-16 deposited with the CCDC. 2022-07-16 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT220_FDC-1-as_synthesized ; PROBLEM: NonSolvent Resd 1 C Ueq(max)/Ueq(min) Range 10.0 Ratio RESPONSE: The presence of disordered solvent molecules, and the disorder of coordinating solvents contribute to this alert. ; _vrf_PLAT220_FDC-1-as_synthesized_2 ; PROBLEM: NonSolvent Resd 1 N Ueq(max)/Ueq(min) Range 10.0 Ratio RESPONSE: The presence of disordered solvent molecules, and the disorder of coordinating solvents contribute to this alert. ; # end Validation Reply Form _audit_creation_method SHELXL-2018/3 _shelx_SHELXL_version_number 2018/3 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C49.30 H38 Cu2 N3.33 O10.20' _chemical_formula_weight 967.33 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C -0.0001 0.0005 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0016 0.0018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0004 0.0010 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.2444 0.4639 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system trigonal _space_group_IT_number 148 _space_group_name_H-M_alt 'R -3 :H' _space_group_name_Hall '-R 3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' _cell_length_a 23.555(2) _cell_length_b 23.555(2) _cell_length_c 20.1676(10) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 9691.0(19) _cell_formula_units_Z 9 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 43565 _cell_measurement_theta_min 1.640 _cell_measurement_theta_max 30.980 _exptl_crystal_description block _exptl_crystal_colour dark-green _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.492 _exptl_crystal_F_000 4470 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.300 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 0.246 _shelx_estimated_absorpt_T_min 0.976 _shelx_estimated_absorpt_T_max 0.976 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'ABSCOR (Rigaku, 1995)' _exptl_absorpt_correction_T_min 0.7781 _exptl_absorpt_correction_T_max 1.0000 _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.410 _diffrn_radiation_type synchrotron _diffrn_measurement_device_type 'Rigaku 1/4-chi goniometer' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 49448 _diffrn_reflns_av_unetI/netI 0.0142 _diffrn_reflns_av_R_equivalents 0.0323 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 30 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 0.819 _diffrn_reflns_theta_max 15.437 _diffrn_reflns_theta_full 14.241 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 4944 _reflns_number_gt 4558 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'RAPID AUTO (Rigaku, ????)' _computing_cell_refinement 'RAPID AUTO' _computing_data_reduction 'RAPID AUTO' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0605P)^2^+29.5780P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4944 _refine_ls_number_parameters 401 _refine_ls_number_restraints 234 _refine_ls_R_factor_all 0.0340 _refine_ls_R_factor_gt 0.0314 _refine_ls_wR_factor_ref 0.1017 _refine_ls_wR_factor_gt 0.0993 _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_restrained_S_all 1.081 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.33145(9) 0.25017(9) 0.59015(8) 0.0135(3) Uani 1 1 d . . . . . C2 C 0.33367(9) 0.30729(9) 0.55576(9) 0.0133(3) Uani 1 1 d . . . . . C3 C 0.28952(9) 0.29926(9) 0.50627(9) 0.0140(3) Uani 1 1 d . . . . . H1 H 0.257628 0.257546 0.492862 0.017 Uiso 1 1 calc R U . . . C4 C 0.29367(9) 0.35442(9) 0.47708(8) 0.0133(3) Uani 1 1 d . . . . . C5 C 0.34063(9) 0.41687(9) 0.49736(9) 0.0135(3) Uani 1 1 d . . . . . H2 H 0.343016 0.453481 0.477120 0.016 Uiso 1 1 calc R U . . . C6 C 0.38419(9) 0.42470(9) 0.54804(9) 0.0130(3) Uani 1 1 d . . . . . C7 C 0.38059(9) 0.36937(9) 0.57641(9) 0.0137(3) Uani 1 1 d . . . . . H3 H 0.409979 0.374008 0.609640 0.016 Uiso 1 1 calc R U . . . C8 C 0.24568(9) 0.34713(9) 0.42459(8) 0.0130(3) Uani 1 1 d . . . . . C9 C 0.45655(9) 0.49348(9) 0.63517(9) 0.0164(4) Uani 1 1 d . . . . . C10 C 0.51920(11) 0.50575(11) 0.64701(11) 0.0249(4) Uani 1 1 d . . . . . H4 H 0.547521 0.512935 0.611805 0.030 Uiso 1 1 calc R U . . . C11 C 0.53991(13) 0.50734(14) 0.71160(12) 0.0355(6) Uani 1 1 d . . . . . H5 H 0.582480 0.516504 0.720041 0.043 Uiso 1 1 calc R U . . . C12 C 0.49708(13) 0.49528(13) 0.76330(11) 0.0338(5) Uani 1 1 d . . . . . H6 H 0.510105 0.493777 0.806486 0.041 Uiso 1 1 calc R U . . . C13 C 0.43547(12) 0.48549(11) 0.75170(11) 0.0275(5) Uani 1 1 d . . . . . H7 H 0.407345 0.478005 0.787176 0.033 Uiso 1 1 calc R U . . . C14 C 0.41444(10) 0.48661(9) 0.68715(10) 0.0198(4) Uani 1 1 d . . . . . C15 C 0.35242(10) 0.48419(10) 0.67602(10) 0.0226(4) Uani 1 1 d . . . . . H12 H 0.318151 0.458030 0.704541 0.027 Uiso 1 1 calc R U . . . C16 C 0.33998(10) 0.51609(10) 0.62851(10) 0.0208(4) Uani 1 1 d . . . . . H13 H 0.298500 0.511727 0.628492 0.025 Uiso 1 1 calc R U . . . C17 C 0.38515(9) 0.55704(9) 0.57677(10) 0.0169(4) Uani 1 1 d . . . . . C18 C 0.43038(9) 0.54305(9) 0.54775(9) 0.0146(3) Uani 1 1 d . . . . . C19 C 0.47385(9) 0.58357(9) 0.49992(9) 0.0177(4) Uani 1 1 d . . . . . H8 H 0.503425 0.573047 0.480992 0.021 Uiso 1 1 calc R U . . . C20 C 0.47359(10) 0.63947(10) 0.48014(10) 0.0218(4) Uani 1 1 d . . . . . H9 H 0.502903 0.666777 0.448063 0.026 Uiso 1 1 calc R U . . . C21 C 0.42928(11) 0.65448(10) 0.50853(11) 0.0238(4) Uani 1 1 d . . . . . H10 H 0.428995 0.692279 0.495777 0.029 Uiso 1 1 calc R U . . . C22 C 0.38554(10) 0.61367(10) 0.55563(11) 0.0215(4) Uani 1 1 d . . . . . H11 H 0.355581 0.624080 0.573762 0.026 Uiso 1 1 calc R U . . . Cu1 Cu 0.39644(2) 0.20103(2) 0.67389(2) 0.01019(9) Uani 1 1 d . . . . . N1 N 0.43350(8) 0.48688(8) 0.56818(8) 0.0140(3) Uani 1 1 d . . . . . O1 O 0.49926(8) 0.26541(10) 0.68511(10) 0.0401(4) Uani 1 1 d D . . . . O2 O 0.38506(7) 0.25801(7) 0.61151(7) 0.0171(3) Uani 1 1 d . . . . . O3 O 0.27687(7) 0.19917(7) 0.59662(7) 0.0181(3) Uani 1 1 d . . . . . O4 O 0.20129(7) 0.28975(7) 0.41157(7) 0.0168(3) Uani 1 1 d . . . . . O5 O 0.25227(7) 0.39800(7) 0.39784(7) 0.0177(3) Uani 1 1 d . . . . . C25 C 0.6654(6) 0.3370(11) 0.6376(4) 0.051(3) Uani 0.3333 1 d D U P A -1 H14 H 0.679146 0.317364 0.670947 0.077 Uiso 0.3333 1 calc R U P A -1 H15 H 0.697706 0.382498 0.633079 0.077 Uiso 0.3333 1 calc R U P A -1 H16 H 0.660338 0.315068 0.596038 0.077 Uiso 0.3333 1 calc R U P A -1 N2 N 0.6023(3) 0.3308(3) 0.6571(3) 0.0300(12) Uani 0.3333 1 d D U P A -1 C23 C 0.5488(3) 0.2722(3) 0.6624(3) 0.0238(12) Uani 0.3333 1 d D U P A -1 C24 C 0.5495(4) 0.2100(4) 0.6417(5) 0.046(2) Uani 0.3333 1 d D U P A -1 H17 H 0.591723 0.215064 0.651288 0.070 Uiso 0.3333 1 calc R U P A -1 H18 H 0.540864 0.202810 0.595083 0.070 Uiso 0.3333 1 calc R U P A -1 H19 H 0.516405 0.173248 0.665938 0.070 Uiso 0.3333 1 calc R U P A -1 C26 C 0.6010(4) 0.3912(3) 0.6710(5) 0.0394(18) Uani 0.3333 1 d D U P A -1 H20 H 0.556649 0.382572 0.668796 0.059 Uiso 0.3333 1 calc R U P A -1 H21 H 0.627202 0.423982 0.638828 0.059 Uiso 0.3333 1 calc R U P A -1 H22 H 0.618278 0.406699 0.714569 0.059 Uiso 0.3333 1 calc R U P A -1 N3 N 0.5323(10) 0.2955(7) 0.7973(6) 0.067(4) Uani 0.1667 1 d D U P A -2 C27 C 0.5211(11) 0.3049(6) 0.7333(6) 0.054(4) Uani 0.1667 1 d D U P A -2 C28 C 0.5324(14) 0.3735(7) 0.7178(11) 0.066(5) Uani 0.1667 1 d D U P A -2 H23 H 0.548930 0.400580 0.756544 0.100 Uiso 0.1667 1 calc R U P A -2 H24 H 0.563591 0.392525 0.682385 0.100 Uiso 0.1667 1 calc R U P A -2 H25 H 0.491696 0.370259 0.704710 0.100 Uiso 0.1667 1 calc R U P A -2 C29 C 0.5059(9) 0.2273(6) 0.8205(7) 0.037(3) Uani 0.1667 1 d D U P A -2 H26 H 0.517118 0.227484 0.866285 0.055 Uiso 0.1667 1 calc R U P A -2 H27 H 0.459078 0.203698 0.815705 0.055 Uiso 0.0889 1 calc R U P A -2 H28 H 0.524396 0.206352 0.794514 0.055 Uiso 0.1667 1 calc R U P A -2 C30 C 0.5448(14) 0.3470(9) 0.8456(8) 0.060(5) Uani 0.1667 1 d D U P A -2 H29 H 0.551810 0.334090 0.888549 0.091 Uiso 0.1667 1 calc R U P A -2 H30 H 0.583043 0.387048 0.832495 0.091 Uiso 0.1667 1 calc R U P A -2 H31 H 0.507738 0.353532 0.847221 0.091 Uiso 0.1667 1 calc R U P A -2 N3B N 0.5116(15) 0.2582(13) 0.8042(11) 0.146(8) Uani 0.1667 1 d D U P A -3 C27B C 0.507(2) 0.2851(13) 0.7450(7) 0.151(9) Uani 0.1667 1 d D U P A -3 C28B C 0.529(2) 0.3583(12) 0.7571(15) 0.141(12) Uani 0.1667 1 d D U P A -3 H32 H 0.533125 0.366996 0.803876 0.211 Uiso 0.1667 1 calc R U P A -3 H33 H 0.570835 0.385333 0.736149 0.211 Uiso 0.1667 1 calc R U P A -3 H34 H 0.497374 0.368018 0.738704 0.211 Uiso 0.1667 1 calc R U P A -3 C29B C 0.5096(14) 0.1946(11) 0.7964(16) 0.092(8) Uani 0.1667 1 d D U P A -3 H35 H 0.513000 0.178675 0.839138 0.137 Uiso 0.1667 1 calc R U P A -3 H36 H 0.468925 0.163495 0.775967 0.137 Uiso 0.1667 1 calc R U P A -3 H37 H 0.545450 0.200561 0.768987 0.137 Uiso 0.1667 1 calc R U P A -3 C30B C 0.569(2) 0.3074(16) 0.8434(18) 0.147(11) Uani 0.1667 1 d D U P A -3 H38 H 0.571363 0.287954 0.884328 0.221 Uiso 0.1667 1 calc R U P A -3 H39 H 0.608304 0.321352 0.818433 0.221 Uiso 0.1667 1 calc R U P A -3 H40 H 0.563605 0.344498 0.852703 0.221 Uiso 0.1667 1 calc R U P A -3 O6 O 0.666667 0.333333 0.833333 0.52(5) Uiso 0.5328 6 d S . P B 4 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0204(9) 0.0157(8) 0.0070(7) -0.0011(6) -0.0005(6) 0.0109(7) C2 0.0171(8) 0.0147(8) 0.0100(8) 0.0013(6) 0.0013(6) 0.0094(7) C3 0.0168(8) 0.0143(8) 0.0107(8) -0.0017(6) -0.0016(6) 0.0076(7) C4 0.0156(8) 0.0175(8) 0.0084(7) 0.0000(6) -0.0008(6) 0.0095(7) C5 0.0156(8) 0.0151(8) 0.0115(8) 0.0013(6) -0.0006(6) 0.0089(7) C6 0.0137(8) 0.0152(8) 0.0109(8) -0.0008(6) 0.0008(6) 0.0077(7) C7 0.0159(8) 0.0175(8) 0.0094(8) -0.0006(6) -0.0019(6) 0.0096(7) C8 0.0142(8) 0.0187(8) 0.0081(7) -0.0005(6) 0.0005(6) 0.0098(7) C9 0.0195(9) 0.0147(8) 0.0137(8) -0.0028(6) -0.0037(7) 0.0075(7) C10 0.0217(10) 0.0315(11) 0.0209(10) -0.0076(8) -0.0073(8) 0.0130(9) C11 0.0301(12) 0.0482(15) 0.0275(12) -0.0112(10) -0.0165(9) 0.0190(11) C12 0.0436(14) 0.0376(13) 0.0174(10) -0.0078(9) -0.0136(9) 0.0181(11) C13 0.0375(12) 0.0248(10) 0.0152(9) -0.0019(8) -0.0006(8) 0.0117(9) C14 0.0244(10) 0.0164(9) 0.0155(9) -0.0011(7) -0.0006(7) 0.0080(8) C15 0.0217(10) 0.0217(9) 0.0200(9) 0.0005(7) 0.0075(7) 0.0075(8) C16 0.0156(9) 0.0218(9) 0.0239(10) -0.0016(8) 0.0053(7) 0.0084(7) C17 0.0143(8) 0.0172(9) 0.0184(9) -0.0019(7) -0.0003(7) 0.0073(7) C18 0.0148(8) 0.0133(8) 0.0150(8) -0.0016(6) -0.0021(6) 0.0066(7) C19 0.0171(9) 0.0191(9) 0.0155(8) -0.0014(7) 0.0006(7) 0.0080(7) C20 0.0237(10) 0.0201(9) 0.0185(9) 0.0031(7) 0.0010(7) 0.0087(8) C21 0.0286(11) 0.0196(9) 0.0265(10) 0.0020(8) -0.0030(8) 0.0144(8) C22 0.0215(9) 0.0224(9) 0.0260(10) -0.0027(8) -0.0005(8) 0.0151(8) Cu1 0.01181(12) 0.01105(12) 0.00784(13) -0.00049(7) -0.00057(7) 0.00581(8) N1 0.0154(7) 0.0142(7) 0.0126(7) -0.0017(5) -0.0025(6) 0.0076(6) O1 0.0164(8) 0.0439(10) 0.0447(11) -0.0079(8) 0.0006(7) 0.0037(7) O2 0.0186(6) 0.0191(6) 0.0157(6) 0.0050(5) -0.0004(5) 0.0109(5) O3 0.0196(7) 0.0157(6) 0.0171(6) 0.0035(5) -0.0030(5) 0.0075(5) O4 0.0192(6) 0.0174(6) 0.0138(6) -0.0014(5) -0.0063(5) 0.0091(5) O5 0.0189(6) 0.0181(6) 0.0155(6) 0.0013(5) -0.0062(5) 0.0090(5) C25 0.020(6) 0.055(10) 0.064(4) -0.019(9) 0.007(9) 0.007(7) N2 0.019(2) 0.030(3) 0.035(3) -0.006(2) -0.001(2) 0.008(2) C23 0.020(3) 0.028(3) 0.021(3) -0.001(2) -0.003(2) 0.011(2) C24 0.024(3) 0.042(4) 0.081(6) 0.011(4) 0.017(4) 0.022(3) C26 0.028(4) 0.031(4) 0.051(5) -0.008(3) -0.002(3) 0.008(3) N3 0.080(7) 0.051(6) 0.048(6) -0.008(5) -0.010(5) 0.017(5) C27 0.056(7) 0.050(6) 0.056(6) -0.003(5) 0.001(6) 0.025(5) C28 0.082(11) 0.028(7) 0.094(12) -0.016(8) -0.017(10) 0.031(7) C29 0.042(8) 0.032(7) 0.026(7) 0.002(6) 0.002(6) 0.011(6) C30 0.084(11) 0.065(10) 0.025(7) -0.011(8) -0.006(8) 0.032(9) N3B 0.141(10) 0.142(10) 0.141(10) 0.009(7) -0.020(7) 0.060(7) C27B 0.147(11) 0.146(11) 0.150(11) 0.009(8) -0.011(8) 0.065(8) C28B 0.140(16) 0.126(15) 0.165(17) 0.001(13) 0.016(14) 0.074(12) C29B 0.067(11) 0.083(12) 0.105(13) 0.015(10) -0.063(10) 0.021(9) C30B 0.138(15) 0.161(16) 0.139(16) 0.017(13) -0.029(13) 0.073(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 O3 1.252(2) . ? C1 O2 1.257(2) . ? C1 C2 1.491(2) . ? C2 C3 1.385(2) . ? C2 C7 1.385(3) . ? C3 C4 1.384(2) . ? C4 C5 1.388(3) . ? C4 C8 1.495(2) . ? C5 C6 1.394(2) . ? C6 C7 1.386(2) . ? C6 N1 1.399(2) . ? C8 O5 1.251(2) . ? C8 O4 1.255(2) . ? C9 C10 1.376(3) . ? C9 C14 1.396(3) . ? C9 N1 1.435(2) . ? C10 C11 1.385(3) . ? C11 C12 1.378(4) . ? C12 C13 1.371(4) . ? C13 C14 1.398(3) . ? C14 C15 1.451(3) . ? C15 C16 1.337(3) . ? C16 C17 1.458(3) . ? C17 C18 1.392(3) . ? C17 C22 1.396(3) . ? C18 C19 1.383(3) . ? C18 N1 1.422(2) . ? C19 C20 1.379(3) . ? C20 C21 1.383(3) . ? C21 C22 1.377(3) . ? Cu1 O4 1.9504(13) 5 ? Cu1 O2 1.9535(13) . ? Cu1 O5 1.9594(13) 11_556 ? Cu1 O3 1.9657(13) 13_556 ? Cu1 O1 2.1316(17) . ? Cu1 Cu1 2.5945(5) 13_556 ? O1 C23 1.189(5) . ? O1 C27 1.263(8) . ? O1 C27B 1.275(10) . ? C25 N2 1.473(9) . ? N2 C23 1.329(6) . ? N2 C26 1.465(7) . ? C23 C24 1.530(7) . ? N3 C27 1.356(9) . ? N3 C30 1.465(9) . ? N3 C29 1.479(9) . ? C27 C28 1.534(9) . ? N3B C27B 1.381(10) . ? N3B C29B 1.483(10) . ? N3B C30B 1.491(10) . ? C27B C28B 1.550(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 C1 O2 125.40(17) . . ? O3 C1 C2 118.03(16) . . ? O2 C1 C2 116.56(16) . . ? C3 C2 C7 120.63(16) . . ? C3 C2 C1 121.80(16) . . ? C7 C2 C1 117.55(16) . . ? C2 C3 C4 118.85(16) . . ? C3 C4 C5 120.94(16) . . ? C3 C4 C8 119.92(16) . . ? C5 C4 C8 119.10(16) . . ? C4 C5 C6 119.99(16) . . ? C7 C6 C5 118.90(16) . . ? C7 C6 N1 119.53(16) . . ? C5 C6 N1 121.48(16) . . ? C2 C7 C6 120.67(16) . . ? O5 C8 O4 125.35(17) . . ? O5 C8 C4 118.09(16) . . ? O4 C8 C4 116.55(16) . . ? C10 C9 C14 121.30(18) . . ? C10 C9 N1 119.61(18) . . ? C14 C9 N1 119.08(17) . . ? C9 C10 C11 119.7(2) . . ? C12 C11 C10 119.6(2) . . ? C13 C12 C11 120.7(2) . . ? C12 C13 C14 120.7(2) . . ? C9 C14 C13 117.6(2) . . ? C9 C14 C15 122.11(18) . . ? C13 C14 C15 120.19(19) . . ? C16 C15 C14 126.02(19) . . ? C15 C16 C17 126.31(19) . . ? C18 C17 C22 117.24(18) . . ? C18 C17 C16 122.42(18) . . ? C22 C17 C16 120.32(18) . . ? C19 C18 C17 121.35(17) . . ? C19 C18 N1 118.63(17) . . ? C17 C18 N1 120.02(17) . . ? C20 C19 C18 120.36(18) . . ? C19 C20 C21 119.27(19) . . ? C22 C21 C20 120.26(19) . . ? C21 C22 C17 121.51(18) . . ? O4 Cu1 O2 87.67(6) 5 . ? O4 Cu1 O5 169.10(6) 5 11_556 ? O2 Cu1 O5 92.06(6) . 11_556 ? O4 Cu1 O3 90.32(6) 5 13_556 ? O2 Cu1 O3 169.22(6) . 13_556 ? O5 Cu1 O3 87.92(6) 11_556 13_556 ? O4 Cu1 O1 91.73(7) 5 . ? O2 Cu1 O1 94.41(7) . . ? O5 Cu1 O1 99.15(7) 11_556 . ? O3 Cu1 O1 96.23(7) 13_556 . ? O4 Cu1 Cu1 84.99(4) 5 13_556 ? O2 Cu1 Cu1 81.27(4) . 13_556 ? O5 Cu1 Cu1 84.20(4) 11_556 13_556 ? O3 Cu1 Cu1 88.00(4) 13_556 13_556 ? O1 Cu1 Cu1 174.67(6) . 13_556 ? C6 N1 C18 119.19(15) . . ? C6 N1 C9 117.24(15) . . ? C18 N1 C9 111.39(15) . . ? C23 O1 Cu1 138.2(3) . . ? C27 O1 Cu1 120.4(10) . . ? C27B O1 Cu1 105(2) . . ? C1 O2 Cu1 126.32(12) . . ? C1 O3 Cu1 117.90(12) . 13_556 ? C8 O4 Cu1 122.34(12) . 9_554 ? C8 O5 Cu1 122.97(12) . 12_556 ? C23 N2 C26 121.7(5) . . ? C23 N2 C25 120.6(10) . . ? C26 N2 C25 117.8(9) . . ? O1 C23 N2 121.8(5) . . ? O1 C23 C24 117.1(5) . . ? N2 C23 C24 121.0(5) . . ? C27 N3 C30 118.2(11) . . ? C27 N3 C29 117.8(11) . . ? C30 N3 C29 119.4(12) . . ? O1 C27 N3 130.8(10) . . ? O1 C27 C28 114.2(10) . . ? N3 C27 C28 114.9(10) . . ? C27B N3B C29B 113.7(15) . . ? C27B N3B C30B 110.5(15) . . ? C29B N3B C30B 113.6(15) . . ? O1 C27B N3B 132.9(17) . . ? O1 C27B C28B 117.5(15) . . ? N3B C27B C28B 108.3(13) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3 C1 C2 C3 -30.8(3) . . . . ? O2 C1 C2 C3 150.55(17) . . . . ? O3 C1 C2 C7 147.33(17) . . . . ? O2 C1 C2 C7 -31.3(2) . . . . ? C7 C2 C3 C4 0.9(3) . . . . ? C1 C2 C3 C4 178.99(16) . . . . ? C2 C3 C4 C5 -0.8(3) . . . . ? C2 C3 C4 C8 -178.66(16) . . . . ? C3 C4 C5 C6 -0.4(3) . . . . ? C8 C4 C5 C6 177.50(16) . . . . ? C4 C5 C6 C7 1.4(3) . . . . ? C4 C5 C6 N1 177.84(16) . . . . ? C3 C2 C7 C6 0.1(3) . . . . ? C1 C2 C7 C6 -178.03(16) . . . . ? C5 C6 C7 C2 -1.3(3) . . . . ? N1 C6 C7 C2 -177.79(16) . . . . ? C3 C4 C8 O5 -177.72(16) . . . . ? C5 C4 C8 O5 4.4(3) . . . . ? C3 C4 C8 O4 3.0(2) . . . . ? C5 C4 C8 O4 -174.86(16) . . . . ? C14 C9 C10 C11 4.1(3) . . . . ? N1 C9 C10 C11 -175.3(2) . . . . ? C9 C10 C11 C12 1.3(4) . . . . ? C10 C11 C12 C13 -3.8(4) . . . . ? C11 C12 C13 C14 0.9(4) . . . . ? C10 C9 C14 C13 -6.8(3) . . . . ? N1 C9 C14 C13 172.52(18) . . . . ? C10 C9 C14 C15 169.9(2) . . . . ? N1 C9 C14 C15 -10.7(3) . . . . ? C12 C13 C14 C9 4.3(3) . . . . ? C12 C13 C14 C15 -172.5(2) . . . . ? C9 C14 C15 C16 -33.2(3) . . . . ? C13 C14 C15 C16 143.4(2) . . . . ? C14 C15 C16 C17 3.1(3) . . . . ? C15 C16 C17 C18 34.9(3) . . . . ? C15 C16 C17 C22 -143.4(2) . . . . ? C22 C17 C18 C19 -0.1(3) . . . . ? C16 C17 C18 C19 -178.34(18) . . . . ? C22 C17 C18 N1 178.58(17) . . . . ? C16 C17 C18 N1 0.3(3) . . . . ? C17 C18 C19 C20 0.5(3) . . . . ? N1 C18 C19 C20 -178.18(18) . . . . ? C18 C19 C20 C21 -0.2(3) . . . . ? C19 C20 C21 C22 -0.6(3) . . . . ? C20 C21 C22 C17 1.0(3) . . . . ? C18 C17 C22 C21 -0.7(3) . . . . ? C16 C17 C22 C21 177.6(2) . . . . ? C7 C6 N1 C18 -169.21(16) . . . . ? C5 C6 N1 C18 14.4(3) . . . . ? C7 C6 N1 C9 -30.0(2) . . . . ? C5 C6 N1 C9 153.62(17) . . . . ? C19 C18 N1 C6 -107.2(2) . . . . ? C17 C18 N1 C6 74.1(2) . . . . ? C19 C18 N1 C9 111.36(19) . . . . ? C17 C18 N1 C9 -67.3(2) . . . . ? C10 C9 N1 C6 111.7(2) . . . . ? C14 C9 N1 C6 -67.6(2) . . . . ? C10 C9 N1 C18 -106.1(2) . . . . ? C14 C9 N1 C18 74.6(2) . . . . ? O3 C1 O2 Cu1 -12.4(3) . . . . ? C2 C1 O2 Cu1 166.15(12) . . . . ? O2 C1 O3 Cu1 12.9(2) . . . 13_556 ? C2 C1 O3 Cu1 -165.62(12) . . . 13_556 ? O5 C8 O4 Cu1 5.1(3) . . . 9_554 ? C4 C8 O4 Cu1 -175.77(11) . . . 9_554 ? O4 C8 O5 Cu1 -3.2(3) . . . 12_556 ? C4 C8 O5 Cu1 177.69(11) . . . 12_556 ? Cu1 O1 C23 N2 149.3(5) . . . . ? Cu1 O1 C23 C24 -33.1(9) . . . . ? C26 N2 C23 O1 -7.9(11) . . . . ? C25 N2 C23 O1 171.3(7) . . . . ? C26 N2 C23 C24 174.5(8) . . . . ? C25 N2 C23 C24 -6.2(11) . . . . ? Cu1 O1 C27 N3 81(3) . . . . ? Cu1 O1 C27 C28 -94.2(18) . . . . ? C30 N3 C27 O1 -167(2) . . . . ? C29 N3 C27 O1 -11(4) . . . . ? C30 N3 C27 C28 8(3) . . . . ? C29 N3 C27 C28 164(2) . . . . ? Cu1 O1 C27B N3B 83(5) . . . . ? Cu1 O1 C27B C28B -112(4) . . . . ? C29B N3B C27B O1 2(6) . . . . ? C30B N3B C27B O1 132(5) . . . . ? C29B N3B C27B C28B -164(3) . . . . ? C30B N3B C27B C28B -35(4) . . . . ? _refine_diff_density_max 1.045 _refine_diff_density_min -0.409 _refine_diff_density_rms 0.082 _shelx_res_file ; TITL shelxt_a.res in R-3 shelxt_a.res created by SHELXL-2018/3 at 16:47:19 on 05-Jun-2022 REM Yadorkari-X generated CELL 0.41000 23.5555 23.5555 20.1676 90.0000 90.0000 120.0000 ZERR 9.0 0.0022 0.0022 0.0010 0.0000 0.0000 0.0000 LATT 3 SYMM -Y, +X-Y, +Z SYMM -X+Y, -X, +Z REM SPGR R-3 trigonal SFAC C H O N Cu DISP C -0.0001 0.0005 5.13 DISP H 0.0000 0.0000 0.64 DISP O 0.0016 0.0018 10.11 DISP N 0.0004 0.0010 7.17 DISP Cu 0.2444 0.4639 1120.67 UNIT 443.7 342 91.8 29.97 18 L.S. 125 FMAP 2 PLAN -20 ACTA CONF LIST 4 DFIX 1.25 0.01 O1 C23 O1 C27 O1 C27B DFIX 1.52 0.01 C23 C24 C27 C28 C27B C28B DANG 2.43 0.02 N2 C24 N3 C28 N3B C28B DANG 2.43 0.02 O1 C24 O1 C28 O1 C28B DFIX 1.33 0.01 C23 N2 C27 N3 C27B N3B DANG 2.43 0.02 C23 C25 C23 C26 C27 C29 C27 C30 C27B C29B C27B C30B DFIX 1.47 0.01 N2 C25 N2 C26 N3 C29 N3 C30 N3B C29B N3B C30B DANG 2.53 0.02 C25 C26 C29 C30 C29B C30B RIGU 0.01 0.02 C23 C24 C25 C26 N2 RIGU 0.01 0.02 C27 C28 C29 C30 N3 RIGU 0.01 0.02 C27B C28B C29B C30B N3B SIMU 0.01 0.02 C23 C24 C25 C26 N2 SIMU 0.01 0.02 C27 C28 C29 C30 N3 SIMU 0.01 0.02 C27B C28B C29B C30B N3B ISOR 0.01 0.02 N3 C27 C28 C29 C30 N3B C27B C28B C29B C30B WGHT 0.060500 29.577999 FVAR 0.12942 C1 1 0.331446 0.250165 0.590155 11.00000 0.02041 0.01570 = 0.00703 -0.00110 -0.00054 0.01091 C2 1 0.333671 0.307292 0.555759 11.00000 0.01708 0.01468 = 0.01000 0.00125 0.00134 0.00942 C3 1 0.289521 0.299264 0.506268 11.00000 0.01684 0.01426 = 0.01070 -0.00169 -0.00159 0.00760 AFIX 43 H1 2 0.257628 0.257546 0.492862 11.00000 -1.20000 AFIX 0 C4 1 0.293671 0.354415 0.477083 11.00000 0.01556 0.01754 = 0.00836 0.00005 -0.00077 0.00950 C5 1 0.340631 0.416872 0.497357 11.00000 0.01561 0.01511 = 0.01145 0.00125 -0.00057 0.00893 AFIX 43 H2 2 0.343016 0.453481 0.477120 11.00000 -1.20000 AFIX 0 C6 1 0.384193 0.424699 0.548037 11.00000 0.01372 0.01516 = 0.01088 -0.00081 0.00081 0.00772 C7 1 0.380587 0.369374 0.576406 11.00000 0.01588 0.01750 = 0.00938 -0.00061 -0.00185 0.00962 AFIX 43 H3 2 0.409979 0.374008 0.609640 11.00000 -1.20000 AFIX 0 C8 1 0.245684 0.347125 0.424592 11.00000 0.01421 0.01875 = 0.00813 -0.00047 0.00046 0.00983 C9 1 0.456546 0.493482 0.635172 11.00000 0.01948 0.01469 = 0.01370 -0.00283 -0.00367 0.00748 C10 1 0.519200 0.505748 0.647011 11.00000 0.02174 0.03150 = 0.02090 -0.00758 -0.00729 0.01297 AFIX 43 H4 2 0.547521 0.512935 0.611805 11.00000 -1.20000 AFIX 0 C11 1 0.539905 0.507343 0.711602 11.00000 0.03010 0.04822 = 0.02746 -0.01120 -0.01651 0.01897 AFIX 43 H5 2 0.582480 0.516504 0.720041 11.00000 -1.20000 AFIX 0 C12 1 0.497081 0.495284 0.763298 11.00000 0.04356 0.03761 = 0.01744 -0.00777 -0.01364 0.01809 AFIX 43 H6 2 0.510105 0.493777 0.806486 11.00000 -1.20000 AFIX 0 C13 1 0.435465 0.485486 0.751702 11.00000 0.03747 0.02475 = 0.01521 -0.00186 -0.00061 0.01172 AFIX 43 H7 2 0.407345 0.478005 0.787176 11.00000 -1.20000 AFIX 0 C14 1 0.414437 0.486615 0.687153 11.00000 0.02442 0.01643 = 0.01549 -0.00114 -0.00061 0.00796 C15 1 0.352423 0.484187 0.676016 11.00000 0.02174 0.02173 = 0.01999 0.00046 0.00748 0.00755 AFIX 43 H12 2 0.318151 0.458030 0.704541 11.00000 -1.20000 AFIX 0 C16 1 0.339981 0.516088 0.628515 11.00000 0.01556 0.02176 = 0.02393 -0.00163 0.00533 0.00843 AFIX 43 H13 2 0.298500 0.511727 0.628492 11.00000 -1.20000 AFIX 0 C17 1 0.385148 0.557038 0.576767 11.00000 0.01431 0.01720 = 0.01842 -0.00194 -0.00028 0.00726 C18 1 0.430376 0.543048 0.547754 11.00000 0.01482 0.01331 = 0.01497 -0.00159 -0.00208 0.00661 C19 1 0.473853 0.583566 0.499920 11.00000 0.01708 0.01913 = 0.01551 -0.00143 0.00057 0.00801 AFIX 43 H8 2 0.503425 0.573047 0.480992 11.00000 -1.20000 AFIX 0 C20 1 0.473593 0.639469 0.480143 11.00000 0.02370 0.02014 = 0.01847 0.00312 0.00102 0.00869 AFIX 43 H9 2 0.502903 0.666777 0.448063 11.00000 -1.20000 AFIX 0 C21 1 0.429276 0.654479 0.508531 11.00000 0.02864 0.01960 = 0.02646 0.00200 -0.00296 0.01444 AFIX 43 H10 2 0.428995 0.692279 0.495777 11.00000 -1.20000 AFIX 0 C22 1 0.385538 0.613669 0.555629 11.00000 0.02154 0.02244 = 0.02597 -0.00265 -0.00054 0.01508 AFIX 43 H11 2 0.355581 0.624080 0.573762 11.00000 -1.20000 AFIX 0 CU1 5 0.396437 0.201027 0.673892 11.00000 0.01181 0.01105 = 0.00784 -0.00049 -0.00057 0.00581 N1 4 0.433501 0.486884 0.568182 11.00000 0.01539 0.01425 = 0.01258 -0.00172 -0.00254 0.00763 O1 3 0.499255 0.265407 0.685114 11.00000 0.01640 0.04389 = 0.04473 -0.00786 0.00065 0.00369 O2 3 0.385061 0.258011 0.611509 11.00000 0.01856 0.01905 = 0.01574 0.00496 -0.00040 0.01087 O3 3 0.276867 0.199173 0.596623 11.00000 0.01963 0.01573 = 0.01710 0.00348 -0.00297 0.00751 O4 3 0.201288 0.289752 0.411568 11.00000 0.01919 0.01738 = 0.01382 -0.00143 -0.00632 0.00913 O5 3 0.252273 0.397999 0.397844 11.00000 0.01894 0.01810 = 0.01552 0.00132 -0.00624 0.00895 PART -1 C25 1 0.665356 0.336978 0.637590 10.33333 0.01955 0.05493 = 0.06358 -0.01942 0.00700 0.00737 AFIX 137 H14 2 0.679146 0.317364 0.670947 10.33333 -1.50000 H15 2 0.697706 0.382498 0.633079 10.33333 -1.50000 H16 2 0.660338 0.315068 0.596038 10.33333 -1.50000 AFIX 0 N2 4 0.602278 0.330847 0.657083 10.33333 0.01916 0.02953 = 0.03547 -0.00577 -0.00094 0.00777 C23 1 0.548842 0.272209 0.662366 10.33333 0.02024 0.02850 = 0.02134 -0.00119 -0.00252 0.01116 C24 1 0.549522 0.210043 0.641748 10.33333 0.02370 0.04173 = 0.08141 0.01091 0.01677 0.02214 AFIX 137 H17 2 0.591723 0.215064 0.651288 10.33333 -1.50000 H18 2 0.540864 0.202810 0.595083 10.33333 -1.50000 H19 2 0.516405 0.173248 0.665938 10.33333 -1.50000 AFIX 0 C26 1 0.600991 0.391228 0.671020 10.33333 0.02775 0.03069 = 0.05074 -0.00844 -0.00245 0.00786 AFIX 137 H20 2 0.556649 0.382572 0.668796 10.33333 -1.50000 H21 2 0.627202 0.423982 0.638828 10.33333 -1.50000 H22 2 0.618278 0.406699 0.714569 10.33333 -1.50000 PART -2 AFIX 0 N3 4 0.532260 0.295487 0.797308 10.16667 0.07962 0.05149 = 0.04806 -0.00817 -0.00951 0.01725 C27 1 0.521127 0.304864 0.733337 10.16667 0.05586 0.04989 = 0.05563 -0.00297 0.00077 0.02533 C28 1 0.532389 0.373472 0.717790 10.16667 0.08184 0.02766 = 0.09403 -0.01552 -0.01698 0.03062 AFIX 33 H23 2 0.548930 0.400580 0.756544 10.16667 -1.50000 H24 2 0.563591 0.392525 0.682385 10.16667 -1.50000 H25 2 0.491696 0.370259 0.704710 10.16667 -1.50000 AFIX 0 C29 1 0.505899 0.227268 0.820488 10.16667 0.04230 0.03249 = 0.02584 0.00231 0.00218 0.01141 AFIX 33 H26 2 0.517118 0.227484 0.866285 10.16667 -1.50000 H27 2 0.459078 0.203698 0.815705 10.08889 -1.50000 H28 2 0.524396 0.206352 0.794514 10.16667 -1.50000 AFIX 0 C30 1 0.544793 0.346978 0.845552 10.16667 0.08414 0.06527 = 0.02465 -0.01099 -0.00593 0.03192 AFIX 33 H29 2 0.551810 0.334090 0.888549 10.16667 -1.50000 H30 2 0.583043 0.387048 0.832495 10.16667 -1.50000 H31 2 0.507738 0.353532 0.847221 10.16667 -1.50000 PART -3 AFIX 0 N3B 4 0.511560 0.258213 0.804227 10.16667 0.14065 0.14244 = 0.14090 0.00920 -0.01981 0.05963 C27B 1 0.506894 0.285121 0.745043 10.16667 0.14741 0.14616 = 0.14997 0.00935 -0.01084 0.06539 C28B 1 0.529179 0.358337 0.757090 10.16667 0.14049 0.12647 = 0.16517 0.00137 0.01631 0.07410 AFIX 33 H32 2 0.533125 0.366996 0.803876 10.16667 -1.50000 H33 2 0.570835 0.385333 0.736149 10.16667 -1.50000 H34 2 0.497374 0.368018 0.738704 10.16667 -1.50000 AFIX 0 C29B 1 0.509557 0.194629 0.796389 10.16667 0.06655 0.08254 = 0.10470 0.01472 -0.06250 0.02149 AFIX 33 H35 2 0.513000 0.178675 0.839138 10.16667 -1.50000 H36 2 0.468925 0.163495 0.775967 10.16667 -1.50000 H37 2 0.545450 0.200561 0.768987 10.16667 -1.50000 AFIX 0 C30B 1 0.568803 0.307380 0.843410 10.16667 0.13829 0.16114 = 0.13897 0.01725 -0.02916 0.07257 AFIX 33 H38 2 0.571363 0.287954 0.884328 10.16667 -1.50000 H39 2 0.608304 0.321352 0.818433 10.16667 -1.50000 H40 2 0.563605 0.344498 0.852703 10.16667 -1.50000 PART 4 AFIX 0 O6 3 0.666667 0.333333 0.833333 10.08880 0.51612 PART 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM shelxt_a.res in R-3 REM wR2 = 0.1017, GooF = S = 1.073, Restrained GooF = 1.081 for all data REM R1 = 0.0314 for 4558 Fo > 4sig(Fo) and 0.0340 for all 4944 data REM 401 parameters refined using 234 restraints END WGHT 0.0587 30.6231 REM Highest difference peak 1.045, deepest hole -0.409, 1-sigma level 0.082 Q1 1 0.5315 0.1760 0.6227 11.00000 0.05 0.77 Q2 1 0.5752 0.2945 0.7930 11.00000 0.05 0.68 Q3 1 0.4937 0.2653 0.8232 11.00000 0.05 0.54 Q4 1 0.5887 0.3541 0.8035 11.00000 0.05 0.43 Q5 1 0.5135 0.2559 0.6615 11.00000 0.05 0.43 Q6 1 0.5067 0.2678 0.8745 11.00000 0.05 0.41 Q7 1 0.5279 0.2187 0.7071 11.00000 0.05 0.40 Q8 1 0.3291 0.2777 0.5713 11.00000 0.05 0.39 Q9 1 0.3590 0.3380 0.5602 11.00000 0.05 0.36 Q10 1 0.3648 0.5358 0.6024 11.00000 0.05 0.35 Q11 1 0.2724 0.3520 0.4513 11.00000 0.05 0.35 Q12 1 0.3623 0.4210 0.5246 11.00000 0.05 0.35 Q13 1 0.4495 0.5626 0.5210 11.00000 0.05 0.35 Q14 1 0.4359 0.4933 0.6605 11.00000 0.05 0.34 Q15 1 0.5959 0.2712 0.8300 11.00000 0.05 0.34 Q16 1 0.3116 0.3837 0.4890 11.00000 0.05 0.33 Q17 1 0.2924 0.3291 0.4939 11.00000 0.05 0.33 Q18 1 0.4974 0.2422 0.7122 11.00000 0.05 0.33 Q19 1 0.3109 0.3086 0.5340 11.00000 0.05 0.33 Q20 1 0.4427 0.4890 0.6014 11.00000 0.05 0.32 ; _shelx_res_checksum 69279 _shelx_hkl_file ; 0 0 3 3011.10 48.55 0 0 -3 3066.15 48.52 0 0 -3 3170.97 50.70 0 0 6 1704.26 33.64 0 0 6 1794.39 35.21 0 0 -6 1776.76 34.25 0 0 -6 1686.89 33.72 0 0 9 919.11 22.60 0 0 9 968.67 24.05 0 0 -9 987.89 23.88 0 0 -9 977.63 24.24 0 0 12 5950.18 117.71 0 0 12 5852.04 118.47 0 0 -12 5996.51 118.50 0 0 -12 5943.02 119.87 0 0 15 132.08 7.68 0 0 15 128.42 7.99 0 0 -15 133.54 8.42 0 0 -15 135.60 8.29 0 0 18 560.34 20.54 0 0 18 547.53 20.51 0 0 -18 534.61 19.40 0 0 -18 535.33 20.67 0 0 21 26.16 5.83 0 0 21 36.71 4.98 0 0 -21 32.73 4.62 0 0 -21 25.14 4.59 0 0 24 156.83 11.32 0 0 24 175.64 11.66 0 0 -24 152.06 9.95 0 0 -24 146.36 11.63 0 -1 -26 15.86 3.99 0 -1 -26 19.51 5.73 0 1 26 16.51 5.87 0 1 26 17.96 4.80 -1 0 -25 17.50 6.19 -1 0 -25 24.61 5.65 1 0 25 21.99 5.82 1 0 25 24.27 4.59 1 1 -24 79.16 9.17 1 1 -24 80.88 7.20 -1 -1 24 76.64 8.65 -1 -1 24 78.66 8.54 0 -1 -23 2.75 4.76 0 -1 -23 7.12 3.40 0 1 23 15.32 5.09 0 1 23 10.01 4.80 -1 0 -22 74.37 7.47 1 0 22 79.07 7.08 1 1 -21 -1.72 3.54 1 1 -21 0.60 2.81 0 -1 -20 1.46 3.23 0 1 20 -1.43 4.43 -1 0 -19 76.18 6.86 -1 0 -19 79.39 6.50 1 0 19 73.00 6.65 1 0 19 74.59 6.49 1 1 -18 33.11 4.52 1 1 -18 31.56 4.85 -1 -1 18 28.72 5.52 -1 -1 18 32.30 4.87 0 -1 -17 4.66 4.90 0 -1 -17 7.08 4.09 0 1 17 6.10 3.15 0 1 17 2.36 2.82 -1 0 -16 776.27 24.26 -1 0 -16 792.40 25.97 1 0 16 815.85 25.53 1 0 16 770.88 24.86 1 1 -15 366.87 14.73 1 1 -15 362.46 13.80 -1 -1 15 397.13 15.82 -1 -1 15 369.10 14.01 0 -1 -14 619.86 21.12 0 -1 -14 612.90 19.46 0 1 14 607.41 19.53 0 1 14 596.65 19.93 -1 0 -13 1228.32 31.86 -1 0 -13 1194.52 32.47 1 0 13 1238.95 32.08 1 0 13 1217.88 32.30 1 1 -12 101.55 6.05 1 1 -12 108.08 6.59 -1 -1 12 102.48 6.80 -1 -1 12 107.18 6.50 0 -1 -11 0.97 2.38 0 -1 -11 0.80 3.84 0 1 11 2.04 2.08 0 1 11 0.85 2.46 -1 0 -10 12.08 3.65 -1 0 -10 7.87 3.78 1 0 10 17.16 3.75 1 0 10 14.90 3.15 1 1 -9 31.00 3.81 1 1 -9 34.11 3.76 -1 -1 9 37.85 3.26 -1 -1 9 34.20 3.77 0 -1 -8 0.28 3.17 0 1 8 2.87 1.97 0 1 8 6.27 2.28 -1 0 -7 82.09 5.50 1 1 -6 394.53 11.85 1 1 -6 393.44 10.45 -1 -1 6 374.20 10.68 -1 -1 6 408.07 11.56 0 -1 -5 756.23 17.30 0 -1 -5 704.16 15.78 0 1 5 722.51 17.34 -1 0 -4 1881.57 34.01 -1 0 -4 2010.17 35.08 1 0 4 1928.75 34.28 1 1 -3 417.41 10.02 1 1 -3 419.36 9.05 -1 -1 3 412.79 8.60 -1 -1 3 435.71 9.99 0 -1 -2 359.30 7.86 0 1 2 361.81 7.38 -1 0 -1 203.60 4.57 1 0 1 196.09 4.08 1 1 0 1294.99 17.49 -1 -1 0 1230.46 20.87 -1 -1 0 1283.51 17.37 0 -1 1 201.35 3.39 0 1 -1 206.03 3.51 0 1 -1 202.02 3.98 -1 0 2 337.03 6.73 1 0 -2 357.78 7.25 1 0 -2 357.99 7.86 1 1 3 1140.35 21.61 1 1 3 1201.19 21.69 -1 -1 -3 1254.32 23.71 0 -1 4 1897.11 33.98 0 -1 4 1965.26 33.72 0 1 -4 1940.49 34.48 0 1 -4 1884.28 32.88 -1 0 5 724.79 17.09 -1 0 5 711.51 15.53 1 0 -5 727.07 16.25 1 0 -5 744.49 16.85 1 1 6 1198.11 25.67 1 1 6 1209.39 26.17 -1 -1 -6 1145.62 25.40 0 1 -7 85.35 5.12 -1 0 8 8.72 3.02 1 0 -8 -2.02 2.72 1 1 9 59.15 5.07 -1 -1 -9 58.00 5.06 -1 -1 -9 61.90 5.18 0 -1 10 12.52 3.42 0 -1 10 15.04 3.46 0 1 -10 15.79 3.63 0 1 -10 13.54 3.69 -1 0 11 -1.17 2.17 -1 0 11 2.52 2.34 1 0 -11 1.30 3.64 1 0 -11 1.63 3.21 1 1 12 295.33 12.42 1 1 12 307.32 12.04 -1 -1 -12 298.06 11.96 -1 -1 -12 297.49 12.47 0 -1 13 1270.20 32.14 0 -1 13 1209.50 31.94 0 1 -13 1258.64 31.68 0 1 -13 1190.29 31.98 -1 0 14 604.53 20.03 -1 0 14 616.46 19.50 1 0 -14 604.60 20.46 1 0 -14 612.45 19.72 1 1 15 50.72 5.68 1 1 15 51.67 6.14 -1 -1 -15 49.56 4.98 -1 -1 -15 49.53 6.16 0 -1 16 828.94 25.05 0 -1 16 775.87 25.49 0 1 -16 812.71 24.60 0 1 -16 786.90 25.61 -1 0 17 0.58 3.07 -1 0 17 3.64 2.89 1 0 -17 4.27 3.29 1 0 -17 7.76 3.98 1 1 18 2.02 2.53 1 1 18 -1.74 3.43 -1 -1 -18 4.13 3.44 -1 -1 -18 3.92 3.99 0 -1 19 77.04 7.14 0 -1 19 66.80 6.51 0 1 -19 74.07 6.24 0 1 -19 71.23 6.71 -1 0 20 -0.29 3.49 1 0 -20 3.49 4.35 1 1 21 3.39 4.36 -1 -1 -21 5.29 3.26 -1 -1 -21 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19.28 2.95 6 9 0 665.74 14.99 3 -6 0 109.36 3.73 -9 -3 0 26.44 4.10 6 9 0 699.08 23.60 -3 6 3 184.52 7.18 9 3 3 54.00 3.90 -3 6 3 160.68 6.08 -6 -9 3 3.70 2.96 -6 -9 3 0.66 1.16 9 3 3 56.18 5.18 -9 -3 -3 58.76 4.46 3 -6 -3 162.78 7.56 3 -6 -3 176.85 5.76 6 9 -3 -0.42 0.92 -9 -3 -3 56.77 5.63 6 9 -3 -2.90 2.86 -6 -9 6 8.10 3.63 -6 -9 6 8.58 1.41 9 3 6 249.15 9.56 -3 6 6 1724.46 38.24 9 3 6 247.04 11.87 -6 -9 6 10.41 1.44 -9 -3 -6 244.13 9.74 6 9 -6 9.53 4.17 3 -6 -6 1747.18 38.93 -9 -3 -6 249.25 12.47 3 -6 -6 1672.76 34.40 -6 -9 9 22.20 4.33 -3 6 9 1362.64 31.92 9 3 9 145.25 7.57 9 3 9 137.21 10.04 -9 -3 -9 144.27 8.12 3 -6 -9 1444.13 35.97 6 9 -9 25.42 4.95 -9 -3 -9 138.71 10.52 -3 6 12 114.51 6.71 9 3 12 1.98 2.63 -3 6 12 123.57 7.78 -6 -9 12 50.61 6.45 9 3 12 4.41 4.46 -6 -9 12 44.68 3.78 6 9 -12 42.74 5.44 3 -6 -12 128.60 8.67 -9 -3 -12 1.58 3.23 -9 -3 -12 2.62 5.81 3 -6 -12 117.17 6.78 6 9 -12 47.21 3.50 -6 -9 15 98.20 6.56 9 3 15 265.87 13.25 -3 6 15 0.14 4.61 9 3 15 252.36 14.85 9 3 15 240.72 13.13 -3 6 15 1.39 3.02 -6 -9 15 97.09 8.65 -9 -3 -15 270.32 12.88 6 9 -15 101.63 8.45 3 -6 -15 2.87 3.36 6 9 -15 92.37 5.87 -3 6 18 158.19 10.31 -6 -9 18 31.16 6.12 9 3 18 97.92 10.57 9 3 18 101.89 7.66 9 3 18 102.43 8.30 -6 -9 18 30.40 4.64 6 9 -18 33.09 4.26 -9 -3 -18 96.61 7.92 3 -6 -18 155.08 10.46 -3 6 21 14.57 3.86 -3 6 21 8.17 3.74 9 3 21 72.54 6.89 -6 -9 21 76.71 7.90 -6 -9 21 75.04 6.69 9 3 21 75.18 7.38 -9 -3 -21 79.16 7.19 3 -6 -21 9.73 4.77 3 -6 -21 17.11 5.43 6 9 -21 70.69 6.62 6 9 -21 73.19 8.45 -3 6 24 12.38 4.12 -3 6 24 15.44 5.47 3 -6 -24 12.42 4.40 3 -6 -24 15.16 5.23 -4 5 -24 89.72 7.92 4 -5 24 99.53 8.22 -5 -9 -23 29.84 5.79 5 9 23 19.85 7.30 5 9 23 26.22 4.83 5 9 23 30.20 8.27 9 4 -22 171.09 13.01 9 4 -22 198.42 11.51 -9 -4 22 185.15 11.56 -9 -4 22 184.80 13.54 -4 5 -21 133.46 9.48 4 -5 21 121.99 8.36 -5 -9 -20 97.77 8.04 5 9 20 111.00 11.50 5 9 20 91.55 10.11 5 9 20 102.29 9.03 9 4 -19 -1.20 3.02 9 4 -19 -1.74 2.26 -9 -4 19 0.60 3.45 -9 -4 19 0.54 3.64 -4 5 -18 91.96 6.70 -4 5 -18 84.84 6.31 4 -5 18 86.93 7.09 4 -5 18 92.42 7.28 -5 -9 -17 99.90 8.23 5 9 17 96.43 9.55 9 4 -16 99.89 7.96 9 4 -16 98.55 6.94 -9 -4 16 96.67 7.33 -4 5 -15 213.34 10.11 -4 5 -15 216.33 10.31 4 -5 15 225.41 10.74 4 -5 15 233.31 10.69 -5 -9 -14 11.89 4.66 5 9 14 16.61 4.56 5 9 14 16.82 5.67 5 9 14 12.91 4.22 9 4 -13 50.07 6.49 9 4 -13 49.51 4.44 -9 -4 13 49.74 4.32 -9 -4 13 49.25 6.80 -4 5 -12 564.71 16.78 -4 5 -12 551.19 17.27 4 -5 12 569.66 17.64 4 -5 12 561.38 16.75 -5 -9 -11 793.34 30.85 -5 -9 -11 821.99 24.50 5 9 11 782.51 30.28 5 9 11 792.48 23.79 9 4 -10 369.28 15.91 9 4 -10 336.12 11.25 -9 -4 10 346.19 15.32 -9 -4 10 351.59 11.91 -4 5 -9 163.22 6.85 -4 5 -9 162.98 6.78 4 -5 9 159.39 7.43 4 -5 9 160.89 6.54 -5 -9 -8 919.47 24.72 -5 -9 -8 884.89 31.60 5 9 8 925.55 32.85 5 9 8 953.66 25.09 9 4 -7 464.84 16.83 -9 -4 7 426.44 16.40 -9 -4 7 408.48 12.02 -9 -4 7 407.58 12.24 -4 5 -6 256.80 7.02 4 -5 6 263.18 8.27 4 -5 6 237.60 6.69 -5 -9 -5 388.55 12.39 -5 -9 -5 366.23 17.25 5 9 5 404.49 12.29 -9 -4 4 99.67 4.60 -9 -4 4 104.94 8.15 -4 5 -3 1087.14 16.03 -4 5 -3 1128.23 21.45 4 -5 3 1155.88 22.14 5 9 2 11.86 2.10 5 9 2 12.31 4.42 9 4 -1 0.95 2.77 -9 -4 1 2.26 3.24 -9 -4 1 2.35 2.08 -4 5 0 3978.72 64.00 -4 5 0 4158.20 65.43 4 -5 0 3941.74 62.44 4 -5 0 4098.19 65.26 -5 -9 1 1408.79 39.51 -5 -9 1 1479.89 26.95 5 9 -1 1400.63 38.27 5 9 -1 1392.88 24.95 9 4 2 2.14 1.68 9 4 2 2.36 4.03 -9 -4 -2 -0.08 4.89 -9 -4 -2 1.23 2.44 -4 5 3 16.57 3.92 -4 5 3 19.71 3.26 4 -5 -3 20.34 2.18 4 -5 -3 18.40 4.15 -5 -9 4 267.78 6.65 -5 -9 4 267.25 6.60 -5 -9 4 263.37 13.36 9 4 5 224.11 9.13 9 4 5 205.16 11.73 -9 -4 -5 203.36 12.11 -9 -4 -5 200.74 8.91 -4 5 6 174.31 7.84 4 -5 -6 168.84 7.16 -5 -9 7 688.44 14.85 -5 -9 7 685.03 15.23 -5 -9 7 708.59 23.74 5 9 -7 686.67 22.53 9 4 8 6.60 3.83 9 4 8 11.05 2.53 -9 -4 -8 12.22 3.42 -9 -4 -8 11.75 5.74 -4 5 9 2018.67 43.76 4 -5 -9 2012.04 46.34 -5 -9 10 524.41 19.80 5 9 -10 482.25 13.12 5 9 -10 500.38 19.03 9 4 11 39.06 4.40 9 4 11 38.35 6.82 -9 -4 -11 38.15 7.81 -9 -4 -11 37.45 5.17 -4 5 12 274.04 12.13 4 -5 -12 296.85 12.75 4 -5 -12 311.86 11.81 -5 -9 13 122.59 8.45 -5 -9 13 116.13 6.39 5 9 -13 122.36 8.35 5 9 -13 119.31 5.96 9 4 14 -1.37 3.92 9 4 14 -0.63 3.17 9 4 14 -0.82 5.45 -9 -4 -14 1.05 3.46 -4 5 15 1203.09 35.17 -4 5 15 1130.35 32.01 4 -5 -15 1171.75 32.82 4 -5 -15 1162.68 34.63 -5 -9 16 236.00 13.71 -5 -9 16 217.47 10.34 5 9 -16 244.63 12.82 5 9 -16 240.75 10.43 9 4 17 8.58 4.79 9 4 17 6.60 4.80 -9 -4 -17 0.86 2.99 -4 5 18 195.79 11.28 -4 5 18 201.94 11.84 4 -5 -18 197.65 12.77 4 -5 -18 204.87 11.58 -5 -9 19 118.29 9.32 -5 -9 19 123.51 7.67 5 9 -19 115.06 7.13 9 4 20 5.24 4.81 9 4 20 8.34 3.44 -9 -4 -20 6.83 3.09 -4 5 21 1.35 4.66 -4 5 21 1.40 3.01 4 -5 -21 6.59 4.40 4 -5 -21 -2.10 3.81 -5 -9 22 39.70 5.55 -5 -9 22 27.56 5.34 5 9 -22 32.73 5.29 9 4 23 1.21 3.13 9 4 23 3.59 5.39 9 4 23 1.66 5.20 -9 -4 -23 2.29 3.35 -4 5 24 11.50 5.67 -4 5 24 9.12 4.25 4 -5 -24 14.65 5.16 4 -5 -24 16.43 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3050.78 53.36 11 4 -2 118.91 5.40 -4 7 -2 103.49 4.25 -7 -11 -2 1.60 1.70 -4 7 -2 109.00 4.10 11 4 -2 123.41 8.84 -11 -4 2 111.15 8.65 4 -7 2 110.14 4.75 -11 -4 2 119.51 5.59 7 11 2 4.39 4.13 4 -7 2 111.77 4.04 -4 7 1 59.49 5.37 -4 7 1 53.71 3.09 -7 -11 1 39.86 5.77 -4 7 1 59.27 3.44 11 4 1 212.08 10.82 -7 -11 1 43.36 2.86 -4 7 1 57.97 2.76 11 4 1 198.69 8.00 7 11 -1 42.57 7.23 7 11 -1 41.96 2.64 -11 -4 -1 215.33 8.84 -11 -4 -1 232.12 12.09 11 4 4 665.51 23.30 11 4 4 645.51 18.67 -4 7 4 11.30 1.94 -7 -11 4 101.36 8.60 -7 -11 4 107.25 4.23 7 11 -4 92.14 8.73 -11 -4 -4 639.31 18.89 -11 -4 -4 649.42 24.26 -4 7 7 2456.27 54.01 -7 -11 7 21.69 1.99 -4 7 7 2561.33 51.35 11 4 7 924.27 30.55 -7 -11 7 19.01 6.11 -7 -11 7 23.38 2.15 11 4 7 871.89 24.37 7 11 -7 23.99 5.99 4 -7 -7 2401.94 52.98 4 -7 -7 2500.20 51.04 -11 -4 -7 919.16 31.84 -11 -4 -7 908.95 25.95 11 4 10 164.10 9.23 -4 7 10 7.28 4.49 11 4 10 160.10 11.71 -4 7 10 11.71 2.64 -7 -11 10 22.71 2.47 -7 -11 10 29.19 5.14 -11 -4 -10 163.37 11.52 4 -7 -10 9.58 3.35 4 -7 -10 10.24 3.71 7 11 -10 19.33 4.46 -11 -4 -10 155.79 9.15 -4 7 13 42.46 5.29 -4 7 13 35.95 5.57 11 4 13 333.02 14.26 11 4 13 308.27 16.77 -7 -11 13 27.32 3.40 4 -7 -13 43.33 5.10 7 11 -13 27.90 2.99 -11 -4 -13 334.26 14.58 -11 -4 -13 326.98 18.19 7 11 -13 20.11 5.97 4 -7 -13 39.11 4.85 11 4 16 99.27 10.79 11 4 16 95.15 8.38 -7 -11 16 1.03 3.30 -4 7 16 283.36 13.97 -4 7 16 292.40 13.64 -7 -11 16 4.28 2.63 -11 -4 -16 97.16 8.46 7 11 -16 -0.71 1.32 7 11 -16 0.59 2.79 4 -7 -16 268.25 13.53 -7 -11 19 43.52 6.09 11 4 19 135.97 9.44 -7 -11 19 38.01 4.45 11 4 19 114.84 9.90 7 11 -19 49.71 5.19 4 -7 -19 9.64 4.57 7 11 -19 37.49 6.12 -11 -4 -19 130.24 9.38 11 4 22 50.07 8.34 -4 7 22 18.13 4.60 11 4 22 49.18 6.74 11 4 22 52.02 6.77 -4 7 22 20.03 4.66 4 -7 -22 18.09 4.82 -11 -4 -22 50.04 6.37 4 -7 -22 24.08 4.54 -4 7 25 19.84 4.62 -4 7 25 13.57 5.93 4 -7 -25 15.69 4.90 4 -7 -25 12.64 4.87 -5 6 -23 35.50 5.90 -5 6 -23 30.51 4.78 5 -6 23 36.11 5.96 5 -6 23 28.89 5.48 11 5 -21 23.25 4.51 11 5 -21 21.51 6.14 -11 -5 21 25.17 5.14 -5 6 -20 25.18 5.00 5 -6 20 24.14 4.61 -6 -11 -19 17.76 4.08 6 11 19 15.86 6.09 6 11 19 15.58 5.10 6 11 19 18.38 8.19 11 5 -18 36.20 4.23 11 5 -18 34.19 5.87 -11 -5 18 39.88 4.71 -11 -5 18 39.06 5.53 -5 6 -17 6.52 2.96 -5 6 -17 6.69 2.53 5 -6 17 7.51 3.16 5 -6 17 6.22 3.40 6 11 16 8.06 8.09 6 11 16 9.12 5.02 11 5 -15 3.75 2.73 -11 -5 15 5.37 3.51 -11 -5 15 0.35 3.81 -5 6 -14 2.47 2.90 -5 6 -14 2.67 2.61 5 -6 14 2.13 2.19 5 -6 14 0.78 2.03 -6 -11 -13 19.81 4.66 6 11 13 27.19 4.86 11 5 -12 94.24 8.85 -11 -5 12 80.86 5.58 -11 -5 12 96.40 8.78 -11 -5 12 91.63 6.16 -5 6 -11 50.71 4.27 5 -6 11 52.29 4.90 -6 -11 -10 68.94 5.19 -6 -11 -10 51.48 9.40 6 11 10 54.46 9.11 6 11 10 58.65 5.85 11 5 -9 86.91 8.33 -11 -5 9 82.28 5.19 -11 -5 9 85.36 5.15 -11 -5 9 85.91 7.19 -5 6 -8 1.45 1.83 -5 6 -8 -0.78 1.84 5 -6 8 1.28 1.78 5 -6 8 -1.69 2.33 -6 -11 -7 3.10 4.06 -6 -11 -7 6.41 2.96 6 11 7 5.55 3.05 6 11 7 0.49 6.62 11 5 -6 4.96 4.58 -11 -5 6 1.02 1.37 -11 -5 6 0.26 1.84 -11 -5 6 3.14 4.89 -5 6 -5 1968.18 30.73 5 -6 5 1897.29 29.96 5 -6 5 2105.09 39.34 -6 -11 -4 21.47 2.88 -6 -11 -4 17.49 7.13 6 11 4 15.18 5.63 6 11 4 13.39 2.51 11 5 -3 261.04 9.04 11 5 -3 242.14 12.71 -11 -5 3 267.91 13.78 -11 -5 3 247.96 8.83 -5 6 -2 1.83 1.36 -5 6 -2 2.21 2.44 -5 6 -2 2.31 1.13 5 -6 2 2.20 1.49 -6 -11 -1 364.76 17.08 6 11 1 364.20 16.53 6 11 1 349.06 9.86 11 5 0 32.27 3.36 11 5 0 34.15 5.03 -11 -5 0 33.77 5.02 -11 -5 0 29.69 3.22 -5 6 1 161.56 5.72 -5 6 1 149.54 5.07 5 -6 -1 165.22 5.95 5 -6 -1 155.15 5.65 -6 -11 2 142.75 9.86 -6 -11 2 136.16 4.73 6 11 -2 139.69 4.68 6 11 -2 131.35 9.64 11 5 3 58.59 4.76 11 5 3 55.04 5.77 -11 -5 -3 52.55 7.85 -11 -5 -3 66.30 5.04 5 -6 -4 1704.04 35.68 -6 -11 5 17.97 6.15 -6 -11 5 23.69 1.79 -6 -11 5 27.67 1.81 6 11 -5 18.97 5.65 11 5 6 47.44 6.62 11 5 6 43.43 4.56 -11 -5 -6 52.47 6.55 -11 -5 -6 45.55 5.10 -5 6 7 2570.32 51.26 -5 6 7 2610.75 55.17 5 -6 -7 2410.52 48.62 5 -6 -7 2442.96 53.00 -6 -11 8 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6 181.49 8.38 -12 -6 6 -0.19 1.72 -12 -6 6 2.12 3.30 -12 -6 6 0.12 1.84 -6 6 -3 12.32 3.05 -6 -12 -3 229.10 8.54 12 6 -3 232.81 13.08 12 6 -3 233.63 8.52 6 -6 3 16.30 3.01 6 12 3 239.48 13.59 -12 -6 3 219.53 8.84 -12 -6 3 229.50 12.88 6 12 3 225.09 8.30 12 6 0 113.72 8.63 12 6 0 107.39 5.48 -6 -12 0 144.25 5.49 -6 6 0 180.06 6.58 -6 -12 0 151.58 10.70 -6 6 0 177.24 5.39 6 -6 0 186.33 5.74 6 12 0 149.85 10.92 6 -6 0 173.35 5.77 -12 -6 0 121.28 10.18 -12 -6 0 114.85 6.41 6 12 0 145.62 5.24 12 6 3 41.70 5.66 -6 -12 3 590.07 12.70 12 6 3 39.85 4.08 -6 6 3 512.26 13.93 -6 6 3 524.47 12.81 -6 -12 3 582.00 24.06 6 12 -3 563.26 22.03 6 12 -3 570.68 11.96 -12 -6 -3 35.09 6.74 -12 -6 -3 38.45 4.26 6 -6 -3 533.61 14.38 -6 -12 6 640.31 13.72 -6 -12 6 694.13 25.92 12 6 6 22.24 5.28 -6 -12 6 638.85 13.45 12 6 6 24.73 4.05 -6 6 6 342.74 12.26 -6 6 6 346.49 11.35 -12 -6 -6 23.49 4.17 -12 -6 -6 26.93 5.61 6 -6 -6 319.38 11.47 6 12 -6 676.90 23.92 6 -6 -6 313.79 10.15 12 6 9 233.94 13.82 -6 6 9 553.59 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7.20 5 12 8 10.01 2.71 12 7 -7 33.10 6.06 -12 -7 7 30.83 2.89 -12 -7 7 34.21 5.60 -12 -7 7 37.01 3.46 -7 5 -6 737.54 18.72 7 -5 6 755.41 18.79 7 -5 6 763.35 16.72 7 -5 6 720.13 14.44 -5 -12 -5 3.99 2.39 5 12 5 6.23 1.85 5 12 5 7.46 4.02 12 7 -4 130.19 6.25 -12 -7 4 147.17 6.78 -12 -7 4 138.66 9.69 -7 5 -3 146.31 4.08 7 -5 3 148.28 3.81 -5 -12 -2 28.82 7.23 5 12 2 33.89 5.62 12 7 -1 1.01 4.80 12 7 -1 2.15 2.06 -12 -7 1 2.60 3.78 -12 -7 1 0.57 2.40 -7 5 0 759.12 15.37 7 -5 0 779.81 17.20 7 -5 0 778.00 15.87 -5 -12 1 194.08 5.84 -5 -12 1 197.27 12.81 5 12 -1 197.51 11.62 5 12 -1 190.16 5.45 12 7 2 22.57 3.36 12 7 2 28.24 6.32 -12 -7 -2 22.40 2.76 -12 -7 -2 15.53 7.14 -7 5 3 42.90 3.55 7 -5 -3 42.32 4.58 -5 -12 4 72.32 7.17 -5 -12 4 75.36 2.77 5 12 -4 73.60 6.46 12 7 5 337.93 12.74 12 7 5 305.33 15.68 -12 -7 -5 298.49 12.21 -12 -7 -5 319.81 17.02 -7 5 6 4141.44 81.97 7 -5 -6 4307.95 83.93 7 -5 -6 4270.49 79.23 -5 -12 7 818.48 28.25 5 12 -7 827.73 27.07 12 7 8 181.20 9.60 12 7 8 190.55 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297.76 13.90 -12 -13 1 2.17 1.56 12 13 -1 2.85 1.79 12 13 -1 0.35 4.30 -1 12 2 184.86 10.15 -1 12 2 177.64 5.92 1 -12 -2 204.74 10.95 1 -12 -2 177.74 5.85 13 1 3 39.38 4.90 13 1 3 34.54 4.19 -13 -1 -3 31.13 5.84 -13 -1 -3 34.88 4.12 -12 -13 4 94.22 10.97 -12 -13 4 94.26 5.24 12 13 -4 96.42 4.98 12 13 -4 91.07 8.41 -1 12 5 216.73 8.24 -1 12 5 234.34 12.55 1 -12 -5 225.45 12.52 1 -12 -5 221.42 7.90 13 1 6 9.01 4.56 13 1 6 16.50 3.11 -13 -1 -6 12.20 5.10 -13 -1 -6 15.38 3.04 -12 -13 7 285.69 9.83 -12 -13 7 329.84 19.16 12 13 -7 336.06 18.24 -1 12 8 29.73 4.42 -1 12 8 26.57 5.34 -1 12 8 25.64 2.95 1 -12 -8 22.03 3.06 13 1 9 7.95 4.35 -13 -1 -9 11.68 3.12 -13 -1 -9 12.63 6.01 -12 -13 10 146.24 6.95 -12 -13 10 152.47 6.93 -12 -13 10 149.76 11.99 12 13 -10 155.54 12.15 -1 12 11 216.46 9.95 -1 12 11 225.18 12.70 -1 12 11 214.41 14.66 1 -12 -11 216.98 9.85 13 1 12 52.13 6.15 13 1 12 48.85 5.14 -13 -1 -12 48.13 5.20 -13 -1 -12 53.42 6.65 -12 -13 13 121.50 6.70 -12 -13 13 129.08 6.94 -12 -13 13 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8.09 2.62 -14 -7 8 8.90 2.70 -7 7 -5 37.45 3.10 14 7 -5 16.00 2.93 -7 -14 -5 106.39 6.31 7 14 5 102.04 5.85 7 14 5 106.04 9.51 -14 -7 5 13.06 2.60 -7 -14 -2 22.15 2.68 -7 -14 -2 28.96 6.14 -7 7 -2 7.98 1.14 14 7 -2 5.69 3.95 14 7 -2 2.29 2.10 -14 -7 2 -0.05 5.07 7 14 2 25.32 2.74 7 -7 2 8.14 1.90 -14 -7 2 -0.36 1.67 7 -7 2 9.01 1.28 7 14 2 27.35 6.75 14 7 1 2.21 2.43 -7 7 1 188.33 6.41 14 7 1 -3.41 3.39 -7 -14 1 120.95 5.08 -7 -14 1 121.28 10.19 7 -7 -1 195.56 6.50 -14 -7 -1 0.29 4.09 7 -7 -1 198.40 6.51 7 14 -1 126.41 9.76 -14 -7 -1 -2.07 1.85 7 14 -1 106.48 4.27 14 7 4 28.63 3.32 14 7 4 26.24 5.62 -7 -14 4 98.30 9.22 -7 -14 4 106.89 3.93 -7 -14 4 104.04 3.86 7 -7 -4 337.01 10.18 7 14 -4 107.76 9.66 -14 -7 -4 30.23 4.43 -14 -7 -4 26.90 5.59 -7 -14 7 248.82 6.91 14 7 7 6.80 6.06 -7 -14 7 240.20 6.83 14 7 7 -0.01 2.94 -7 7 7 2903.41 61.42 -7 7 7 2765.34 56.61 7 -7 -7 2830.19 56.94 7 -7 -7 2808.49 60.68 -14 -7 -7 3.10 4.65 7 14 -7 249.35 14.39 -14 -7 -7 1.46 2.55 -7 7 10 645.13 19.55 -7 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1151.86 29.05 -8 -15 7 12.36 4.80 -8 -15 7 10.11 1.34 8 15 -7 10.74 4.14 15 7 8 194.99 9.98 -15 -7 -8 197.38 10.46 -7 8 9 242.45 9.80 -7 8 9 249.49 10.92 7 -8 -9 241.23 10.14 7 -8 -9 257.79 11.24 -8 -15 10 354.72 10.33 -8 -15 10 406.66 20.44 8 15 -10 409.34 19.80 15 7 11 2.17 2.75 15 7 11 5.13 5.27 -15 -7 -11 -3.56 3.88 -7 8 12 451.26 15.78 -7 8 12 438.59 16.82 7 -8 -12 410.59 15.27 -8 -15 13 139.99 6.44 -8 -15 13 136.92 6.06 -8 -15 13 150.38 12.76 8 15 -13 149.25 10.87 15 7 14 52.12 6.76 15 7 14 58.12 7.89 -15 -7 -14 64.06 6.74 -15 -7 -14 58.22 8.71 -7 8 15 148.37 8.63 7 -8 -15 147.25 9.97 -8 -15 16 138.70 6.89 -8 -15 16 157.38 11.96 -8 -15 16 143.64 7.59 8 15 -16 141.37 11.10 15 7 17 100.00 11.29 15 7 17 92.02 7.81 -15 -7 -17 91.96 12.30 -15 -7 -17 112.95 8.89 -7 8 21 250.77 14.30 -7 8 21 238.28 14.64 7 -8 -21 263.49 15.00 7 -8 -21 249.13 13.42 -7 8 24 3.85 4.91 -7 8 24 -1.91 5.09 7 -8 -24 1.35 5.16 7 -8 -24 1.95 4.85 -8 7 -24 99.08 8.24 -8 7 -24 84.79 8.19 8 -7 24 93.24 7.85 8 -7 24 97.45 7.69 -8 7 -21 17.61 4.86 -8 7 -21 8.30 2.88 8 -7 21 9.57 2.85 8 -7 21 7.41 4.84 -8 7 -18 53.42 5.33 -8 7 -18 60.37 5.51 8 -7 18 63.43 5.62 8 -7 18 59.96 5.62 -7 -15 -16 214.44 12.74 7 15 16 207.49 12.40 7 15 16 203.25 13.73 7 15 16 208.44 16.25 -8 7 -15 57.51 5.50 -8 7 -15 57.77 4.78 8 -7 15 56.20 4.63 8 -7 15 51.40 4.88 15 8 -14 67.90 8.34 -15 -8 14 75.31 6.30 -15 -8 14 66.40 7.86 -15 -8 14 76.70 5.69 -7 -15 -13 409.29 24.50 -7 -15 -13 406.79 17.30 7 15 13 379.37 21.45 7 15 13 387.30 16.85 -8 7 -12 156.00 8.39 8 -7 12 158.14 8.53 15 8 -11 77.89 7.80 -15 -8 11 66.23 5.15 -15 -8 11 70.42 5.65 -15 -8 11 62.93 7.59 -7 -15 -10 299.04 13.00 -7 -15 -10 297.70 18.74 7 15 10 271.49 18.52 7 15 10 293.14 13.00 -8 7 -9 34.63 2.66 -8 7 -9 30.47 4.29 8 -7 9 37.28 4.30 8 -7 9 31.86 2.45 15 8 -8 8.15 4.17 -15 -8 8 8.97 2.54 -15 -8 8 5.58 2.02 -7 -15 -7 391.39 22.41 -7 -15 -7 366.67 13.54 7 15 7 385.70 13.71 -8 7 -6 804.19 20.62 8 -7 6 829.95 20.77 8 -7 6 791.41 13.21 8 -7 6 806.57 14.78 15 8 -5 9.33 3.73 15 8 -5 6.85 2.37 -15 -8 5 12.18 6.59 -15 -8 5 6.49 2.73 -7 -15 -4 335.84 11.77 7 15 4 337.92 11.62 -8 7 -3 40.48 3.34 -8 7 -3 40.57 1.47 15 8 -2 54.53 4.38 -15 -8 2 59.13 8.35 -15 -8 2 59.18 4.45 7 15 1 228.77 14.47 -8 7 0 487.94 11.38 8 -7 0 506.99 11.88 15 8 1 27.85 3.68 -15 -8 -1 25.86 3.78 -7 -15 2 0.95 1.35 7 15 -2 -2.10 4.95 7 15 -2 -0.38 1.11 -8 7 3 411.40 11.58 8 -7 -3 398.13 11.82 15 8 4 199.83 9.72 -15 -8 -4 211.65 10.59 -7 -15 5 65.38 2.75 -7 -15 5 67.63 2.79 -8 7 6 623.82 18.63 -8 7 6 620.42 16.87 8 -7 -6 623.57 16.69 8 -7 -6 592.86 18.10 15 8 7 112.24 7.27 -15 -8 -7 110.04 12.26 -15 -8 -7 102.39 7.77 -7 -15 8 24.04 1.74 -7 -15 8 21.49 1.72 -8 7 9 104.73 6.09 -8 7 9 106.02 7.43 8 -7 -9 102.36 7.47 15 8 10 4.60 6.61 15 8 10 4.46 2.88 -15 -8 -10 1.91 2.67 -15 -8 -10 11.61 7.36 -7 -15 11 6.92 5.65 7 15 -11 5.92 3.80 -8 7 12 154.84 9.00 8 -7 -12 146.66 7.72 15 8 13 17.62 3.98 15 8 13 22.07 7.34 -15 -8 -13 17.61 7.97 -15 -8 -13 23.13 5.29 -7 -15 14 47.29 7.62 -7 -15 14 40.57 3.66 -7 -15 14 42.33 3.35 7 15 -14 42.70 6.79 -8 7 15 429.01 16.49 8 -7 -15 453.11 18.58 8 -7 -15 425.27 16.21 15 8 16 97.80 8.00 15 8 16 100.92 11.22 -15 -8 -16 87.61 12.23 -15 -8 -16 110.34 9.05 -7 -15 17 17.46 3.09 -7 -15 17 12.34 4.86 7 15 -17 13.44 2.19 7 15 -17 15.51 4.85 -8 7 21 0.04 2.78 -8 7 21 -0.10 4.17 8 -7 -21 -0.57 5.00 8 -7 -21 -2.00 2.69 -8 7 24 25.98 6.45 -8 7 24 40.03 7.28 8 -7 -24 44.62 8.49 8 -7 -24 39.24 6.46 -9 6 -24 27.19 4.75 -9 6 -24 26.51 4.34 9 -6 24 33.11 5.06 9 -6 24 25.23 5.08 -9 6 -21 59.31 6.25 -9 6 -21 56.43 6.40 9 -6 21 61.32 6.44 9 -6 21 55.17 6.22 -6 -15 -18 71.44 6.94 -9 6 -18 40.43 4.53 6 15 18 72.18 7.97 6 15 18 71.26 8.08 9 -6 18 44.22 5.37 6 15 18 71.38 10.10 9 -6 18 46.39 5.00 15 9 -15 247.54 15.20 -6 -15 -15 3.47 3.39 -9 6 -15 58.97 5.42 -9 6 -15 54.29 4.52 -15 -9 15 267.40 17.61 6 15 15 0.79 5.06 -15 -9 15 256.72 12.37 9 -6 15 54.43 4.76 9 -6 15 57.72 5.29 6 15 15 9.21 5.73 -15 -9 15 261.28 11.47 -6 -15 -12 10.18 8.23 15 9 -12 76.62 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14.35 4.47 15 9 3 27.99 5.63 15 9 3 25.07 3.56 -9 6 3 1157.48 25.60 -6 -15 3 1.58 6.24 -6 -15 3 0.96 0.91 -15 -9 -3 17.71 3.11 -15 -9 -3 21.21 7.60 6 15 -3 0.33 5.58 15 9 6 -3.09 3.70 15 9 6 2.22 2.10 -9 6 6 3143.40 65.73 -6 -15 6 33.99 6.01 6 15 -6 32.85 5.88 -15 -9 -6 2.37 4.43 9 -6 -6 3106.49 61.60 9 -6 -6 3086.64 64.88 -15 -9 -6 0.92 2.29 -9 6 9 137.36 7.77 -9 6 9 127.72 6.62 -6 -15 9 12.47 1.64 15 9 9 5.24 4.43 -15 -9 -9 1.66 3.01 9 -6 -9 137.76 7.76 6 15 -9 23.30 5.31 -15 -9 -9 1.09 5.12 9 -6 -9 134.53 6.87 -9 6 12 0.61 2.33 -9 6 12 -0.87 2.29 15 9 12 32.12 8.65 -6 -15 12 28.43 5.82 9 -6 -12 -1.10 2.19 -15 -9 -12 28.95 9.12 -15 -9 -12 41.37 5.00 -9 6 15 17.13 3.35 15 9 15 43.39 6.69 -6 -15 15 77.76 4.93 15 9 15 49.75 8.04 -6 -15 15 83.07 8.31 6 15 -15 82.95 9.02 9 -6 -15 6.67 5.09 -15 -9 -15 50.17 8.20 -15 -9 -15 52.98 6.06 6 15 -15 73.36 4.59 9 -6 -15 19.48 3.57 -6 -15 18 81.67 8.35 -6 -15 18 71.32 5.68 6 15 -18 74.44 5.16 6 15 -18 86.25 8.27 -9 6 21 9.13 5.45 -9 6 21 9.12 5.29 9 -6 -21 15.69 4.41 9 -6 -21 15.74 4.66 -9 6 24 0.87 5.08 -9 6 24 1.10 4.31 9 -6 -24 2.44 3.05 9 -6 -24 6.80 5.87 -10 5 -24 95.05 9.02 -10 5 -24 95.61 8.78 10 -5 24 100.57 9.37 10 -5 24 93.45 7.77 -10 5 -21 261.33 13.04 -10 5 -21 255.02 13.45 10 -5 21 247.31 13.10 10 -5 21 233.97 11.88 10 -5 18 351.01 14.45 10 -5 18 358.63 17.00 -5 -15 -17 306.94 15.48 5 15 17 314.22 15.38 5 15 17 310.48 17.44 5 15 17 311.82 20.05 -10 5 -15 952.68 29.10 10 -5 15 964.52 26.59 10 -5 15 947.46 30.02 10 -5 15 954.12 29.47 5 15 14 322.93 17.40 5 15 14 317.97 20.21 5 15 14 305.02 14.16 15 10 -13 42.33 6.42 -15 -10 13 42.11 3.85 -15 -10 13 42.33 4.68 -15 -10 13 41.56 7.13 -10 5 -12 1009.31 28.53 10 -5 12 1000.06 25.40 10 -5 12 1023.05 28.98 10 -5 12 956.33 27.83 -5 -15 -11 303.24 18.46 -5 -15 -11 296.94 12.86 5 15 11 290.86 12.61 5 15 11 320.90 19.98 15 10 -10 40.30 7.80 -15 -10 10 41.10 4.12 -15 -10 10 53.82 8.57 -15 -10 10 47.28 4.54 -10 5 -9 3230.12 69.44 10 -5 9 3332.29 70.29 10 -5 9 3358.34 68.02 -5 -15 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49.51 -10 5 6 2417.61 50.27 -10 5 6 2292.79 51.42 10 -5 -6 2436.91 54.11 -5 -15 7 538.67 23.62 -5 -15 7 466.45 8.76 5 15 -7 485.89 19.95 15 10 8 116.50 12.42 15 10 8 127.26 7.81 -15 -10 -8 133.16 12.68 -15 -10 -8 120.33 8.73 -10 5 9 3747.71 81.75 -10 5 9 3824.97 78.29 10 -5 -9 3605.45 80.28 10 -5 -9 3612.53 74.28 -5 -15 10 47.66 2.66 -5 -15 10 46.81 7.52 -5 -15 10 54.44 3.00 5 15 -10 49.45 5.99 15 10 11 182.42 13.77 -15 -10 -11 173.89 14.70 -10 5 12 926.93 26.30 -10 5 12 931.55 28.66 10 -5 -12 875.67 24.83 -5 -15 13 -0.47 1.67 5 15 -13 0.66 1.31 15 10 14 184.35 11.07 15 10 14 187.41 14.36 -15 -10 -14 191.95 12.55 -15 -10 -14 176.75 16.74 -10 5 15 508.96 18.61 10 -5 -15 532.71 21.53 10 -5 -15 511.79 18.56 -5 -15 16 -1.60 2.10 -5 -15 16 -0.14 3.45 5 15 -16 2.09 1.94 5 15 -16 2.57 3.44 -10 5 18 92.05 7.72 -5 -15 19 59.20 5.27 -5 -15 19 54.98 6.85 5 15 -19 57.87 5.00 -10 5 21 530.92 21.59 -10 5 21 594.51 24.84 10 -5 -21 505.80 22.69 10 -5 -21 535.94 20.86 -10 5 24 142.83 11.01 -10 5 24 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1191.01 23.77 -6 10 -1 1187.38 27.02 6 -10 1 1212.91 27.67 6 -10 1 1108.68 22.28 -10 -16 0 52.24 3.79 -10 -16 0 51.30 9.08 10 16 0 54.35 3.70 10 16 0 58.71 7.21 16 6 1 59.58 4.66 16 6 1 67.07 7.21 -16 -6 -1 65.69 5.50 -10 -16 3 18.10 5.97 10 16 -3 17.24 4.95 16 6 4 23.48 7.37 16 6 4 24.59 3.31 -16 -6 -4 27.09 3.93 -6 10 5 87.32 4.73 -6 10 5 85.88 5.58 6 -10 -5 87.34 4.74 6 -10 -5 85.79 6.56 -10 -16 6 67.98 8.64 10 16 -6 76.48 8.35 16 6 7 3.82 2.47 -16 -6 -7 1.65 3.39 -6 10 8 -0.97 1.92 -6 10 8 -0.44 2.67 6 -10 -8 0.97 2.84 6 -10 -8 1.93 2.77 -10 -16 9 60.15 7.42 10 16 -9 57.35 8.83 16 6 10 1.11 2.69 -16 -6 -10 4.90 5.84 -6 10 11 18.42 3.90 -6 10 11 21.86 4.97 6 -10 -11 18.20 4.28 6 -10 -11 24.70 4.29 -10 -16 12 13.51 2.05 -10 -16 12 13.07 2.15 -10 -16 12 7.61 4.66 10 16 -12 11.87 5.42 16 6 13 54.83 6.66 16 6 13 64.29 9.90 -16 -6 -13 64.22 8.75 -16 -6 -13 71.26 6.73 -6 10 14 48.80 5.90 -6 10 14 52.03 5.10 6 -10 -14 51.74 5.82 6 -10 -14 59.81 6.45 16 6 16 14.27 7.26 16 6 16 7.08 3.21 -16 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15.82 -16 -7 9 228.37 10.23 -9 -16 -8 21.60 6.67 -9 -16 -8 30.03 4.17 9 16 8 22.28 6.63 9 16 8 27.42 4.20 -7 9 -7 84.29 5.07 -7 9 -7 79.58 3.31 7 -9 7 82.28 5.10 7 -9 7 76.22 3.22 16 7 -6 97.17 5.71 16 7 -6 124.07 10.51 -16 -7 6 98.49 6.46 -16 -7 6 93.29 8.83 -9 -16 -5 17.10 2.59 9 16 5 14.77 2.89 9 16 5 10.82 5.61 -7 9 -4 0.37 0.63 7 -9 4 0.66 1.32 16 7 -3 106.06 6.39 -16 -7 3 119.76 10.18 -16 -7 3 97.68 6.25 -9 -16 -2 15.48 8.01 -9 -16 -2 16.19 2.69 9 16 2 16.88 2.45 9 16 2 17.86 5.38 -7 9 -1 40.70 3.36 -7 9 -1 41.47 2.89 7 -9 1 41.44 2.86 16 7 0 396.31 14.26 -16 -7 0 405.48 15.22 -9 -16 1 124.02 12.87 9 16 -1 129.85 10.88 -7 9 2 292.53 9.41 7 -9 -2 294.25 10.03 16 7 3 159.87 8.82 -16 -7 -3 155.25 8.37 -9 -16 4 15.08 5.10 -9 -16 4 10.14 1.52 9 16 -4 9.21 6.50 -7 9 5 1953.75 43.44 -7 9 5 1926.29 40.32 7 -9 -5 2132.27 46.74 7 -9 -5 2008.96 41.17 16 7 6 132.39 8.16 -16 -7 -6 134.02 12.35 -16 -7 -6 127.36 8.44 -9 -16 7 6.52 6.07 -9 -16 7 0.05 0.92 -9 -16 7 0.24 0.97 9 16 -7 2.95 3.71 -7 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1.84 -8 -20 -3 11.43 5.07 8 20 3 -3.79 5.97 -12 8 -2 856.94 22.13 -12 8 -2 865.40 18.78 12 -8 2 848.41 22.03 12 -8 2 892.43 18.94 -8 -20 0 43.75 7.83 8 20 0 58.72 9.31 -12 8 1 626.26 17.29 12 -8 -1 580.76 16.42 -8 -20 3 74.83 9.89 8 20 -3 77.51 8.46 -12 8 4 106.39 6.65 -12 8 4 110.58 6.51 12 -8 -4 101.47 5.95 -8 -20 6 91.25 11.68 8 20 -6 77.30 8.51 -12 8 7 547.83 18.53 12 -8 -7 531.80 18.21 -12 8 10 16.11 3.69 -12 8 10 13.06 3.88 12 -8 -10 15.01 3.59 12 -8 -10 10.29 4.71 -12 8 13 13.82 3.10 -12 8 13 20.54 4.22 12 -8 -13 11.63 5.07 12 -8 -13 11.56 3.17 -12 8 16 29.97 4.46 12 -8 -16 41.32 6.11 -12 8 19 12.56 4.97 12 -8 -19 18.66 3.77 12 -8 -19 14.32 4.82 -12 8 22 205.39 13.33 -12 8 22 183.78 12.43 12 -8 -22 198.80 14.22 12 -8 -22 191.25 12.20 -13 7 -23 25.96 4.90 13 -7 23 25.90 5.13 13 -7 23 23.78 4.82 13 -7 23 26.50 3.79 -13 7 -20 80.55 7.27 13 -7 20 73.40 6.59 13 -7 20 72.27 7.54 13 -7 20 74.45 8.35 -13 7 -17 327.73 15.45 13 -7 17 315.55 12.93 13 -7 17 304.17 14.09 -13 7 -14 755.81 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180.73 10.00 14 -9 14 169.86 7.51 14 -9 14 179.42 10.41 -14 9 -11 379.81 15.46 14 -9 11 365.26 14.29 14 -9 11 344.19 11.29 14 -9 11 352.75 10.52 -14 9 -8 357.65 14.12 -14 9 -8 368.71 11.01 14 -9 8 352.84 13.47 14 -9 8 365.41 9.86 -14 9 -5 66.42 5.49 -14 9 -5 62.67 3.81 14 -9 5 67.26 4.84 14 -9 5 64.36 3.45 -14 9 -2 1044.98 26.94 -14 9 -2 1074.12 23.87 14 -9 2 1053.97 23.15 14 -9 2 1005.07 26.31 -14 9 1 1040.21 25.03 -14 9 1 1012.71 26.15 14 -9 -1 1066.58 26.80 -14 9 4 332.20 12.23 -14 9 4 307.49 11.69 14 -9 -4 311.16 12.18 -14 9 7 125.10 8.18 14 -9 -7 122.46 7.44 -14 9 10 1845.42 45.79 -14 9 10 1841.28 48.86 14 -9 -10 1921.65 49.77 14 -9 -10 1864.67 45.31 -14 9 13 9.36 2.84 -14 9 13 7.56 3.88 14 -9 -13 10.12 2.78 14 -9 -13 11.17 4.30 -14 9 16 62.35 7.71 14 -9 -16 45.37 5.72 -14 9 19 50.30 7.73 -14 9 19 39.60 6.22 14 -9 -19 44.36 5.68 -14 9 22 64.26 7.95 14 -9 -22 66.12 7.07 14 -9 -22 67.25 9.07 -15 8 -20 104.19 8.42 15 -8 20 94.39 9.04 15 -8 20 89.93 6.90 15 -8 20 87.27 8.63 -15 8 -17 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106.39 6.47 16 -10 2 108.47 6.24 -16 10 1 354.17 13.12 -16 10 1 366.39 12.76 16 -10 -1 384.40 13.04 16 -10 -1 376.76 13.40 -16 10 4 24.02 3.36 -16 10 4 21.79 3.28 16 -10 -4 23.03 4.20 -16 10 7 5.71 2.91 16 -10 -7 6.26 3.03 -16 10 10 85.00 6.89 -16 10 10 82.74 6.69 -16 10 10 90.50 6.54 16 -10 -10 89.53 8.17 -16 10 13 370.89 16.79 -16 10 13 358.22 15.02 16 -10 -13 392.52 17.24 -16 10 16 16.97 4.23 -16 10 16 13.82 3.91 16 -10 -16 17.07 4.63 16 -10 -16 14.46 3.70 -16 10 19 54.16 7.27 -16 10 19 49.21 6.72 16 -10 -19 43.62 6.88 16 -10 -19 57.88 6.61 -16 10 22 11.04 5.81 -16 10 22 14.03 4.47 16 -10 -22 20.21 5.12 -17 9 -20 84.16 7.74 17 -9 20 91.71 6.89 17 -9 20 94.19 8.35 17 -9 20 92.30 9.07 -17 9 -17 135.79 9.49 17 -9 17 148.93 9.09 17 -9 17 137.88 7.62 17 -9 17 150.28 10.76 -17 9 -14 59.50 5.94 17 -9 14 58.22 4.59 17 -9 14 60.30 5.30 -17 9 -11 79.03 7.35 17 -9 11 75.82 6.08 -17 9 -8 0.48 2.47 17 -9 8 2.19 2.11 17 -9 8 2.43 2.33 -17 9 -5 62.10 5.43 17 -9 5 63.49 5.39 -17 9 -2 308.80 12.32 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197.66 10.41 19 -7 5 186.08 9.06 19 -7 5 195.57 10.45 -19 7 -2 326.97 13.81 -19 7 -2 321.98 13.33 19 -7 2 312.68 12.86 19 -7 2 321.86 12.66 -19 7 1 129.23 8.47 -19 7 1 135.60 8.80 19 -7 -1 135.13 8.64 19 -7 -1 141.33 7.83 -19 7 4 185.02 10.85 -19 7 4 188.38 9.37 19 -7 -4 183.80 9.50 19 -7 -4 192.40 11.01 -19 7 7 59.17 5.17 -19 7 7 71.10 7.12 -19 7 7 63.54 5.29 19 -7 -7 64.87 6.50 -19 7 10 68.66 5.69 -19 7 10 71.54 6.30 -19 7 10 73.52 7.56 19 -7 -10 56.06 7.32 -19 7 13 5.99 2.39 -19 7 13 4.52 3.63 19 -7 -13 3.71 3.66 -19 7 16 2.60 2.40 -19 7 16 -0.33 3.50 -19 7 16 -0.62 2.80 19 -7 -16 -2.14 5.33 -19 7 19 18.89 6.09 -19 7 19 18.27 5.17 19 -7 -19 16.06 4.55 19 -7 -19 11.45 4.42 20 -6 17 -0.05 3.53 20 -6 17 2.69 2.76 20 -6 17 3.00 2.83 -20 6 -14 25.76 5.68 -20 6 -14 28.56 5.87 20 -6 14 26.06 5.51 20 -6 14 15.90 3.87 -20 6 -11 168.68 10.73 -20 6 -11 153.10 9.90 20 -6 11 179.08 9.76 20 -6 11 179.18 10.24 -20 6 -8 693.90 24.84 20 -6 8 721.02 23.97 20 -6 8 716.51 23.73 -20 6 -5 12.31 3.59 -20 6 -5 10.02 4.23 20 -6 5 12.67 3.95 20 -6 5 11.93 3.41 -20 6 -2 686.58 23.11 -20 6 -2 627.11 22.23 20 -6 2 646.09 21.89 20 -6 2 677.27 21.78 -20 6 1 254.90 11.62 -20 6 1 263.52 12.58 20 -6 -1 254.90 11.84 20 -6 -1 289.09 13.61 -20 6 4 760.92 26.73 -20 6 4 724.98 23.72 20 -6 -4 727.49 22.68 20 -6 -4 781.24 26.61 -20 6 7 136.63 10.01 -20 6 7 141.93 8.33 20 -6 -7 128.63 9.07 -20 6 10 183.24 9.86 -20 6 13 48.92 5.20 -20 6 13 46.17 5.89 -20 6 13 51.19 6.30 20 -6 -13 59.76 7.82 -20 6 16 155.44 9.41 -20 6 16 164.15 10.30 -20 6 16 169.26 11.82 20 -6 -16 173.28 11.78 -20 6 19 14.18 3.26 -20 6 19 14.35 4.57 -20 6 19 12.51 5.69 20 -6 -19 12.49 4.85 -21 5 -17 0.39 3.36 21 -5 17 4.53 3.20 21 -5 17 4.60 3.91 21 -5 17 6.63 4.47 -21 5 -14 8.17 4.96 -21 5 -14 2.67 3.62 21 -5 14 2.79 4.15 21 -5 14 1.64 3.51 -21 5 -11 -0.78 5.04 -21 5 -11 -1.13 2.94 21 -5 11 6.48 2.69 21 -5 11 0.95 4.12 -21 5 -8 37.22 6.39 -21 5 -8 34.28 5.45 -21 5 -5 2.69 4.79 21 -5 5 5.86 4.14 21 -5 5 4.82 3.78 -21 5 -2 2.76 4.01 -21 5 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55.17 5.69 -14 13 12 57.26 5.28 14 -13 -12 50.73 5.08 14 -13 -12 56.00 6.06 14 -13 -15 43.34 4.76 -14 13 18 10.53 3.81 -14 13 18 9.04 4.23 14 -13 -18 11.13 6.13 -14 13 21 -0.48 2.86 14 -13 -21 7.90 4.27 14 -13 -21 9.76 4.72 -15 12 -21 71.29 7.22 15 -12 21 79.75 5.77 15 -12 21 78.80 8.22 15 -12 21 77.76 7.47 -15 12 -18 20.09 4.27 15 -12 18 18.91 5.31 15 -12 18 20.60 2.90 15 -12 15 1.97 2.96 15 -12 15 7.77 3.98 -15 12 -12 3.59 2.67 15 -12 12 5.20 2.68 15 -12 12 4.83 1.33 15 -12 12 4.62 1.29 -15 12 -9 667.88 21.56 15 -12 9 635.31 20.52 -15 12 -6 490.82 16.63 15 -12 6 471.11 16.44 -15 12 -3 3.72 1.30 -15 12 -3 4.08 3.13 15 -12 3 2.94 1.46 15 -12 3 5.53 2.23 -15 12 0 194.65 9.40 15 -12 0 212.57 9.08 -15 12 3 87.65 6.22 -15 12 3 92.15 5.90 15 -12 -3 86.02 5.96 15 -12 -3 91.05 6.15 -15 12 6 303.28 12.39 -15 12 6 288.92 11.96 -15 12 6 293.69 11.69 15 -12 -6 304.73 12.96 -15 12 9 29.08 4.44 -15 12 9 28.26 3.58 -15 12 9 24.86 3.69 15 -12 -9 30.78 5.55 -15 12 12 1242.79 35.63 -15 12 12 1281.44 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205.66 10.68 -20 7 12 203.59 13.11 -20 7 15 252.26 12.60 -20 7 15 253.26 15.32 -20 7 15 243.95 13.58 20 -7 -15 256.23 14.73 -20 7 18 82.57 8.63 -20 7 18 87.96 8.44 -20 7 18 94.45 7.24 20 -7 -18 96.46 9.36 21 -6 18 65.64 7.16 21 -6 18 66.01 7.58 21 -6 18 68.22 6.74 -21 6 -15 68.66 7.85 -21 6 -15 82.36 7.69 21 -6 15 69.07 7.69 21 -6 15 74.86 7.34 -21 6 -12 25.40 5.92 -21 6 -12 25.58 5.33 21 -6 12 28.34 5.53 21 -6 12 20.80 4.54 -21 6 -9 13.05 3.45 -21 6 -9 12.52 3.69 21 -6 9 12.01 3.43 21 -6 9 7.70 4.08 -21 6 -6 31.64 4.71 21 -6 6 39.83 5.15 -21 6 -3 0.44 2.46 -21 6 -3 -1.98 3.28 21 -6 3 -3.20 3.54 21 -6 3 3.77 2.46 -21 6 0 19.30 3.66 -21 6 0 14.72 4.75 21 -6 0 18.25 4.56 21 -6 0 19.30 4.24 -21 6 3 0.71 2.46 -21 6 3 0.79 2.54 21 -6 -3 -2.31 3.63 21 -6 -3 -3.30 2.94 -21 6 6 101.81 7.62 -21 6 6 107.84 9.07 21 -6 -6 104.31 6.84 21 -6 -6 106.29 8.17 -21 6 12 5.70 2.61 -21 6 12 9.50 3.47 -21 6 12 4.20 3.63 21 -6 -12 10.78 4.03 -21 6 15 1.73 2.68 -21 6 15 0.54 3.95 -21 6 15 4.35 3.56 21 -6 -15 2.25 3.96 -21 6 18 68.70 8.65 -21 6 18 67.95 7.17 -21 6 18 69.75 6.94 21 -6 -18 72.61 8.16 -22 5 -15 143.43 10.92 -22 5 -15 149.84 10.46 22 -5 15 139.30 9.74 22 -5 15 142.67 10.83 -22 5 -12 9.37 3.91 -22 5 -12 1.45 3.23 22 -5 12 6.31 4.26 22 -5 12 12.88 3.54 -22 5 -9 -2.00 4.43 -22 5 -9 -2.86 2.48 22 -5 9 -4.24 2.85 22 -5 9 -2.65 2.81 -22 5 -6 31.56 4.69 -22 5 -6 30.17 6.31 22 -5 6 31.82 5.03 -22 5 -3 107.77 9.49 22 -5 3 125.38 8.37 -22 5 0 198.41 11.76 22 -5 0 205.72 11.55 22 -5 0 202.63 10.81 -22 5 3 127.32 9.35 22 -5 -3 118.23 7.57 22 -5 -3 138.04 9.94 22 -5 -6 824.13 28.94 22 -5 -6 770.85 24.82 -22 5 9 606.26 21.74 -22 5 9 564.08 23.34 22 -5 -9 632.69 24.99 -22 5 12 296.00 16.38 -22 5 12 282.01 14.24 -22 5 12 292.03 13.89 22 -5 -12 299.75 16.12 -22 5 15 179.03 11.63 -22 5 15 171.28 12.53 -22 5 15 181.47 10.63 22 -5 -15 178.43 12.26 -23 4 -15 39.86 6.88 -23 4 -15 23.62 7.24 23 -4 15 47.64 7.13 23 -4 15 36.74 5.42 -23 4 -12 62.01 7.52 -23 4 -12 57.47 7.62 23 -4 12 65.59 7.67 23 -4 12 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45.09 4.82 -4 24 8 43.90 7.37 4 -24 -8 55.81 9.93 4 -24 -8 43.53 4.03 -4 24 11 11.82 5.61 -4 24 11 17.90 3.08 -4 24 11 18.57 6.25 4 -24 -11 7.99 2.51 -4 24 14 89.79 12.29 -4 24 14 77.47 8.63 4 -24 -14 84.73 6.90 -5 23 -16 35.66 3.37 -5 23 -16 37.64 5.94 5 -23 16 35.08 5.35 5 -23 16 40.65 3.62 -5 23 -13 96.00 7.41 -5 23 -13 88.10 4.58 5 -23 13 90.74 8.88 -5 23 -10 143.63 9.31 5 -23 10 144.43 11.14 -5 23 -7 379.85 16.96 5 -23 7 369.78 19.49 -5 23 -4 317.30 16.19 5 -23 4 295.10 16.74 -5 23 -1 49.98 3.00 -5 23 -1 54.92 8.03 -5 23 -1 51.38 3.03 5 -23 1 57.06 7.52 -5 23 2 90.30 4.87 -5 23 2 91.70 9.51 -5 23 2 84.63 4.41 5 -23 -2 90.68 9.46 -5 23 5 421.75 14.22 5 -23 -5 421.80 13.74 -5 23 8 199.20 14.60 -5 23 8 211.01 13.70 -5 23 8 200.75 9.62 5 -23 -8 205.97 9.76 -5 23 11 123.62 7.74 -5 23 11 120.77 11.08 -5 23 11 132.24 14.07 5 -23 -11 130.60 7.78 -5 23 14 185.64 15.30 -5 23 14 182.07 13.45 -6 22 -16 19.07 4.04 -6 22 -16 14.71 2.89 6 -22 16 14.00 3.69 6 -22 16 12.05 2.49 -6 22 -13 64.84 6.34 -6 22 -13 62.11 4.10 6 -22 13 62.66 6.34 6 -22 13 57.89 4.03 -6 22 -10 5.29 3.74 6 -22 10 6.89 3.78 -6 22 -7 3.15 1.04 -6 22 -7 -0.57 3.67 6 -22 7 -0.54 2.95 6 -22 7 1.79 0.92 -6 22 -4 30.81 2.23 -6 22 -4 25.78 2.04 -6 22 -4 28.62 4.61 6 -22 4 32.74 6.91 -6 22 -1 65.84 3.61 -6 22 -1 71.93 8.39 6 -22 1 79.06 7.65 -6 22 2 23.20 2.47 -6 22 2 16.43 5.05 -6 22 2 22.20 2.62 6 -22 -2 21.74 7.36 -6 22 5 73.30 9.73 -6 22 5 54.96 4.10 6 -22 -5 65.64 9.44 6 -22 -5 60.85 4.59 -6 22 8 103.04 6.40 6 -22 -8 99.04 6.62 -6 22 11 3.80 3.39 -6 22 11 -0.40 7.87 -6 22 11 4.46 5.10 6 -22 -11 6.02 3.44 -6 22 14 269.44 15.68 -6 22 14 302.67 19.81 -6 22 17 72.39 11.78 -6 22 17 77.92 7.12 -6 22 17 86.07 9.84 6 -22 -17 62.54 6.65 -7 21 -16 113.80 8.11 -7 21 -16 122.91 7.17 7 -21 16 124.92 7.21 7 -21 16 124.05 9.05 -7 21 -13 1.87 2.75 -7 21 -13 -0.77 1.88 7 -21 13 1.93 1.87 7 -21 13 2.66 3.96 -7 21 -10 15.99 2.32 -7 21 -10 11.44 3.42 7 -21 10 14.12 2.26 7 -21 10 19.46 4.79 -7 21 -7 4.12 3.73 7 -21 7 4.17 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310.56 15.36 -10 24 5 309.36 11.78 -10 24 5 329.33 18.04 -10 24 5 316.00 12.47 -10 24 8 107.46 7.10 10 -24 -8 105.24 6.60 -10 24 11 14.32 6.16 -10 24 11 26.88 6.33 -10 24 11 19.73 4.43 10 -24 -11 19.57 4.08 -10 24 14 161.96 14.64 -10 24 14 165.35 12.78 -10 24 14 167.70 11.04 10 -24 -14 181.38 10.83 -11 23 -16 27.43 4.12 -11 23 -16 25.77 3.74 11 -23 16 29.80 4.33 11 -23 16 27.37 3.77 -11 23 -13 42.45 4.59 -11 23 -13 52.19 4.55 11 -23 13 54.24 5.34 11 -23 13 47.63 4.62 -11 23 -10 39.18 3.47 -11 23 -10 36.48 4.15 11 -23 10 36.77 3.69 11 -23 10 39.42 5.18 -11 23 -7 156.67 7.39 -11 23 -7 159.87 8.54 11 -23 7 158.23 7.25 11 -23 7 164.69 9.86 -11 23 -4 37.80 3.59 -11 23 -4 38.76 5.10 11 -23 4 35.40 4.92 11 -23 4 39.26 3.31 -11 23 -1 22.37 2.77 -11 23 -1 15.82 3.36 -11 23 -1 16.46 2.30 11 -23 1 17.53 4.42 -11 23 2 44.11 4.10 -11 23 2 42.37 6.61 -11 23 2 43.04 5.20 -11 23 2 36.30 4.08 -11 23 5 284.77 17.13 -11 23 5 269.33 13.55 -11 23 5 293.61 11.98 -11 23 5 265.88 10.96 -11 23 8 3.33 3.33 -11 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170.00 7.88 -13 23 0 173.12 9.75 -13 23 0 186.60 10.67 -13 23 0 173.60 7.87 -13 23 3 132.40 7.14 -13 23 3 116.25 10.02 -13 23 3 126.94 8.89 -13 23 3 131.44 7.28 -13 23 6 71.25 9.49 -13 23 6 71.49 5.20 -13 23 6 76.22 5.69 -13 23 6 79.86 7.05 -13 23 9 296.42 13.13 -13 23 9 315.59 19.11 13 -23 -9 318.83 13.36 -13 23 12 104.94 10.64 -13 23 12 122.08 9.41 13 -23 -12 108.51 7.96 -13 23 15 13.13 5.70 -13 23 15 14.82 4.90 -13 23 15 19.93 5.96 13 -23 -15 20.97 5.07 -14 22 -15 249.12 12.25 14 -22 15 263.42 12.28 -14 22 -12 179.37 6.88 -14 22 -12 196.68 10.46 14 -22 12 191.54 10.05 -14 22 -9 622.27 19.76 -14 22 -9 592.68 15.53 14 -22 9 651.60 19.93 -14 22 -6 228.31 10.31 14 -22 6 260.09 10.75 -14 22 -3 477.15 15.79 -14 22 -3 496.72 17.50 -14 22 -3 481.57 16.10 14 -22 3 487.32 16.03 -14 22 0 511.79 17.46 -14 22 0 474.62 19.03 -14 22 0 447.72 15.38 -14 22 0 471.27 15.67 -14 22 3 303.39 14.00 -14 22 3 326.46 12.66 -14 22 3 320.18 16.26 -14 22 3 322.90 12.60 -14 22 6 519.30 20.17 -14 22 6 473.60 17.30 -14 22 6 505.78 23.04 -14 22 6 488.63 17.32 -14 22 9 1884.04 47.36 -14 22 9 1887.37 48.54 -14 22 9 1849.49 53.52 -14 22 9 1850.60 59.80 -14 22 12 96.92 8.37 14 -22 -12 96.41 8.79 14 -22 -12 88.47 6.77 -14 22 15 39.47 6.27 -14 22 15 37.03 6.02 14 -22 -15 40.74 6.05 14 -22 -15 36.04 4.82 -15 21 -18 66.27 6.34 -15 21 -15 2.81 2.47 -15 21 -15 2.74 1.04 15 -21 15 5.88 2.62 15 -21 15 3.07 1.99 -15 21 -12 5.68 1.15 -15 21 -12 5.61 2.78 15 -21 12 5.53 1.59 15 -21 12 4.26 2.12 -15 21 -9 63.49 5.62 15 -21 9 64.79 5.01 -15 21 -6 98.88 5.05 -15 21 -6 99.50 5.01 -15 21 -6 96.37 6.72 15 -21 6 99.44 6.14 -15 21 -3 -0.82 2.47 -15 21 -3 -0.35 2.21 15 -21 3 0.93 2.71 -15 21 0 24.48 4.59 -15 21 0 18.27 3.44 -15 21 0 18.52 3.62 15 -21 0 23.07 3.60 -15 21 3 1.46 2.02 -15 21 3 -0.27 2.12 -15 21 3 1.41 2.68 -15 21 3 -2.35 2.81 -15 21 6 46.67 5.49 -15 21 6 35.70 3.92 -15 21 6 35.12 5.67 15 -21 -6 28.36 4.67 -15 21 9 14.73 4.03 -15 21 9 12.61 3.96 -15 21 9 9.76 3.87 15 -21 -9 13.48 4.21 -15 21 12 26.56 6.09 15 -21 -12 30.14 5.05 -15 21 15 85.16 8.04 -15 21 15 81.20 8.23 15 -21 -15 68.12 9.21 15 -21 -15 81.89 7.52 -15 21 18 75.02 8.26 -15 21 18 76.13 8.32 15 -21 -18 87.90 7.49 15 -21 -18 78.77 8.83 -16 20 -18 258.10 13.88 16 -20 15 7.79 3.90 -16 20 -12 55.39 5.82 16 -20 12 61.90 5.25 -16 20 -9 23.18 3.50 16 -20 9 26.13 3.65 -16 20 -6 359.42 14.51 -16 20 -6 358.18 9.43 16 -20 6 376.84 14.36 -16 20 -3 31.24 3.95 16 -20 3 29.58 4.22 -16 20 0 8.07 2.67 -16 20 0 3.08 3.46 -16 20 0 4.90 3.11 16 -20 0 2.57 3.14 -16 20 3 12.92 2.71 -16 20 3 9.55 3.59 -16 20 3 10.29 3.02 16 -20 -3 17.75 3.63 -16 20 6 472.00 18.19 -16 20 6 487.72 17.24 -16 20 6 499.54 17.51 16 -20 -6 493.34 19.33 -16 20 9 0.51 3.29 -16 20 9 0.52 2.34 -16 20 9 0.14 4.23 16 -20 -9 1.73 4.02 -16 20 12 14.37 3.74 16 -20 -12 12.57 4.24 -16 20 15 35.83 5.72 -16 20 15 35.90 5.04 16 -20 -15 35.42 5.99 16 -20 -15 28.70 4.33 -16 20 18 7.37 4.01 -16 20 18 1.98 3.13 16 -20 -18 6.28 4.15 16 -20 -18 5.89 2.94 -17 19 -18 108.91 8.64 17 -19 18 121.58 8.84 -17 19 -12 506.34 19.18 17 -19 12 518.19 19.15 -17 19 -9 304.75 13.21 17 -19 9 296.26 13.30 -17 19 -6 497.11 18.18 17 -19 6 487.89 17.39 -17 19 -3 232.17 10.57 -17 19 -3 229.31 7.85 -17 19 -3 220.28 9.00 17 -19 3 232.43 10.21 -17 19 0 1701.32 38.96 -17 19 0 1637.16 41.46 17 -19 0 1653.90 41.48 -17 19 3 85.15 5.87 -17 19 3 82.29 6.68 -17 19 3 85.83 5.81 -17 19 6 66.73 5.58 -17 19 6 68.12 6.23 -17 19 6 57.21 6.12 17 -19 -6 60.57 6.55 -17 19 9 100.20 7.01 -17 19 9 87.90 7.44 17 -19 -9 108.96 8.18 -17 19 12 390.83 16.74 -17 19 15 143.72 10.49 -17 19 15 135.57 10.73 17 -19 -15 148.91 11.71 17 -19 -15 144.98 9.38 -17 19 18 176.46 11.15 -17 19 18 147.60 11.46 17 -19 -18 152.28 10.58 -18 18 -18 12.90 5.33 18 -18 18 14.86 1.82 18 -18 18 17.98 4.16 18 -18 18 13.29 1.31 -18 18 -15 27.00 4.32 18 -18 15 30.34 5.10 18 -18 12 3.33 3.83 -18 18 -9 178.08 10.38 18 -18 9 182.70 9.89 -18 18 -6 72.02 5.78 18 -18 6 71.52 5.69 -18 18 -3 137.26 5.66 -18 18 -3 130.13 8.49 18 -18 3 140.76 5.93 18 -18 3 140.66 8.45 -18 18 0 21.69 2.48 -18 18 0 21.53 3.98 18 -18 0 24.18 4.03 18 -18 0 21.25 3.22 -18 18 3 58.60 5.78 -18 18 3 56.17 5.11 18 -18 -3 62.49 5.88 18 -18 -3 57.67 5.04 -18 18 6 191.89 9.67 -18 18 6 198.64 10.57 -18 18 6 205.20 11.05 18 -18 -6 212.57 10.92 -18 18 9 82.28 6.98 18 -18 -9 84.90 7.40 -18 18 12 437.36 17.72 -18 18 12 433.46 18.15 -18 18 15 474.77 21.25 -18 18 15 455.48 19.49 18 -18 -15 475.83 22.67 18 -18 -15 462.74 18.91 -18 18 18 234.10 15.67 -18 18 18 218.60 12.76 18 -18 -18 233.40 13.36 18 -18 -18 207.13 14.12 -19 17 -18 107.74 8.41 19 -17 18 110.41 8.93 -19 17 -15 326.74 15.63 19 -17 15 322.30 16.00 -19 17 -9 404.60 16.37 19 -17 9 398.39 15.77 -19 17 -6 171.86 10.08 19 -17 6 174.94 9.07 -19 17 -3 994.02 22.27 -19 17 -3 974.01 28.84 19 -17 3 955.37 22.37 19 -17 3 1017.09 28.97 -19 17 0 2190.60 53.19 -19 17 0 2182.33 47.75 19 -17 0 2175.49 52.73 -19 17 3 997.36 28.25 -19 17 3 1042.78 29.99 19 -17 -3 956.73 28.10 19 -17 -3 996.74 29.03 -19 17 6 4.58 2.52 -19 17 6 0.71 3.20 -19 17 6 -2.18 3.23 19 -17 -6 0.07 2.77 -19 17 9 130.80 8.57 19 -17 -9 135.84 9.23 -19 17 12 378.37 16.34 -19 17 12 375.33 15.98 -19 17 15 576.13 24.76 -19 17 15 571.96 22.38 19 -17 -15 565.31 21.56 19 -17 -15 587.57 25.09 -19 17 18 66.18 7.44 -19 17 18 69.57 7.03 19 -17 -18 66.99 8.00 19 -17 -18 74.11 6.80 -20 16 -18 25.66 4.56 20 -16 18 27.44 4.69 20 -16 18 19.71 2.04 -20 16 -15 25.25 5.74 20 -16 15 26.14 5.93 -20 16 -12 -4.03 3.82 20 -16 12 -2.53 2.62 20 -16 9 68.93 6.94 -20 16 -6 3.48 1.09 -20 16 -6 6.32 3.65 20 -16 6 2.34 1.06 20 -16 6 6.27 2.68 -20 16 -3 884.07 27.33 20 -16 3 867.95 21.30 20 -16 3 867.91 26.66 -20 16 0 92.11 6.60 20 -16 0 101.07 6.67 -20 16 3 94.08 6.69 -20 16 3 103.77 6.96 20 -16 -3 103.49 7.28 20 -16 -3 97.72 6.75 -20 16 6 -0.03 3.29 -20 16 6 2.37 4.05 20 -16 -6 1.38 3.86 -20 16 9 134.99 8.79 -20 16 9 141.84 9.36 20 -16 -9 146.78 10.38 -20 16 12 45.11 5.32 -20 16 12 37.94 5.31 -20 16 15 243.88 12.87 -20 16 15 239.95 12.50 -20 16 15 232.84 13.80 -20 16 18 9.36 4.03 -20 16 18 11.04 4.55 20 -16 -18 14.51 4.88 -21 15 -18 30.65 6.21 21 -15 18 34.00 5.85 21 -15 18 29.28 3.05 -21 15 -15 351.02 17.33 21 -15 15 359.34 17.50 -21 15 -12 42.56 6.30 21 -15 12 44.32 5.15 -21 15 -9 123.71 8.17 -21 15 -6 255.97 8.91 21 -15 6 258.89 12.51 21 -15 6 250.65 7.83 -21 15 -3 235.18 11.55 -21 15 -3 227.95 8.68 21 -15 3 217.80 11.12 -21 15 0 2.47 2.38 -21 15 0 3.43 3.39 21 -15 0 1.50 2.61 21 -15 0 2.35 3.82 -21 15 3 96.58 6.49 -21 15 3 109.27 8.25 21 -15 -3 116.15 8.31 21 -15 -3 105.06 7.55 -21 15 6 10.58 3.72 21 -15 -6 7.54 3.08 -21 15 9 4.66 3.75 -21 15 9 0.09 2.88 -21 15 9 1.15 4.07 21 -15 -9 -0.25 2.91 -21 15 12 1.55 3.36 -21 15 12 2.07 3.37 -21 15 12 3.34 4.29 -21 15 15 0.37 5.00 21 -15 -15 3.05 5.10 -21 15 18 4.13 3.21 -21 15 18 5.24 4.18 21 -15 -18 -4.60 6.03 21 -15 -18 3.20 2.77 -22 14 -15 44.58 6.38 22 -14 15 31.00 5.19 22 -14 15 31.00 3.13 -22 14 -12 251.04 13.23 22 -14 12 241.14 8.05 22 -14 12 232.84 7.81 22 -14 12 245.96 13.07 -22 14 -9 111.87 8.16 -22 14 -9 107.82 5.82 22 -14 9 107.10 4.75 22 -14 9 118.03 8.03 -22 14 -3 374.89 13.36 22 -14 3 389.48 15.65 22 -14 3 399.80 13.35 -22 14 0 246.85 10.72 22 -14 0 269.18 11.54 22 -14 0 257.37 12.74 22 -14 -3 117.22 8.15 -22 14 6 45.35 5.43 -22 14 6 38.89 5.85 22 -14 -6 37.83 4.90 -22 14 9 399.23 17.45 22 -14 -9 437.64 18.74 -22 14 12 116.26 9.52 -22 14 12 114.68 9.85 -22 14 12 117.01 8.20 22 -14 -12 118.22 9.29 -22 14 15 0.58 4.19 -22 14 15 1.54 3.57 -22 14 15 1.78 2.72 22 -14 -15 5.86 5.42 -23 13 -15 3.18 3.44 23 -13 15 -2.97 4.53 23 -13 15 0.85 2.33 23 -13 15 0.83 2.55 -23 13 -12 106.59 8.42 23 -13 12 100.89 8.22 -23 13 -9 6.41 4.31 -23 13 -9 1.26 2.48 23 -13 9 2.69 3.23 -23 13 -6 202.15 11.81 -23 13 -6 193.93 9.41 23 -13 6 206.70 8.86 23 -13 6 209.87 11.08 -23 13 -3 24.73 4.10 -23 13 -3 23.70 3.86 23 -13 3 26.66 3.79 -23 13 0 166.16 8.94 23 -13 0 175.66 9.27 -23 13 3 150.65 9.03 23 -13 -3 154.57 9.66 -23 13 6 227.27 11.72 -23 13 6 217.79 11.58 23 -13 -6 234.90 12.29 23 -13 -6 223.23 11.94 -23 13 9 108.53 7.71 -23 13 9 94.67 8.05 23 -13 -9 112.65 9.29 -23 13 12 262.09 14.62 -23 13 12 262.47 13.56 -23 13 12 266.46 13.25 23 -13 -12 258.37 14.44 -23 13 15 267.80 14.18 -23 13 15 286.68 15.87 -23 13 15 302.52 15.37 23 -13 -15 293.63 16.64 -24 12 -15 45.38 6.11 24 -12 15 45.19 4.47 24 -12 15 40.06 4.40 24 -12 15 45.05 6.14 -24 12 -12 105.61 7.33 -24 12 -12 133.48 10.29 24 -12 12 104.61 6.50 24 -12 12 112.90 8.90 -24 12 -9 418.24 18.59 -24 12 -9 385.13 15.76 24 -12 9 407.76 14.47 24 -12 9 456.73 18.86 -24 12 -6 307.72 15.14 -24 12 -6 285.00 12.98 24 -12 6 300.85 11.87 -24 12 -3 394.60 15.99 24 -12 3 416.83 15.62 24 -12 3 422.99 17.14 -24 12 0 349.79 15.28 -24 12 0 315.89 13.93 24 -12 0 358.74 15.35 24 -12 0 351.37 14.41 -24 12 3 246.25 12.20 -24 12 3 258.42 13.40 24 -12 -3 256.91 12.17 24 -12 -3 259.04 13.27 -24 12 6 462.33 18.43 -24 12 6 451.48 19.11 24 -12 -6 462.76 18.18 24 -12 -6 485.85 19.57 -24 12 9 237.20 12.77 -24 12 9 243.37 12.47 -24 12 12 237.12 12.84 -24 12 12 236.79 12.77 -24 12 12 230.72 13.60 24 -12 -12 266.23 14.70 -24 12 15 153.99 10.48 -24 12 15 161.06 12.72 -24 12 15 179.32 10.72 24 -12 -15 171.83 13.14 -25 11 -15 9.90 4.19 25 -11 15 9.59 2.48 25 -11 15 0.78 5.34 25 -11 15 6.17 2.96 -25 11 -12 196.83 11.42 -25 11 -12 201.39 13.59 25 -11 12 209.20 10.51 -25 11 -9 6.96 3.96 25 -11 9 9.17 4.62 25 -11 9 9.18 2.76 -25 11 -6 7.54 3.60 -25 11 -6 1.35 4.72 25 -11 6 4.72 3.39 25 -11 6 4.82 3.34 -25 11 -3 4.03 2.66 -25 11 -3 4.15 4.03 25 -11 3 5.21 3.28 25 -11 3 4.90 2.90 -25 11 0 25.46 4.46 -25 11 0 23.09 4.00 25 -11 0 26.07 4.91 25 -11 0 26.62 4.46 -25 11 3 21.93 3.94 -25 11 3 18.04 3.82 25 -11 -3 22.01 5.14 25 -11 -3 21.94 5.34 -25 11 6 199.75 11.21 -25 11 6 209.34 12.41 25 -11 -6 195.77 11.23 25 -11 -6 199.62 12.36 -25 11 9 245.64 13.46 -25 11 9 229.03 13.34 -25 11 9 233.84 12.95 25 -11 -9 220.96 14.38 -25 11 12 402.85 17.85 -25 11 12 442.30 18.76 -25 11 12 407.06 19.68 25 -11 -12 436.07 21.62 -25 11 15 170.59 11.83 -25 11 15 191.78 11.48 -25 11 15 197.11 14.11 25 -11 -15 184.60 12.65 -26 10 -12 14.07 4.18 -26 10 -12 12.37 3.69 26 -10 12 18.86 4.13 26 -10 12 17.40 4.12 -26 10 -9 55.04 6.94 -26 10 -9 45.77 6.96 26 -10 9 54.10 5.95 26 -10 9 54.65 5.53 -26 10 -6 76.17 7.33 -26 10 -6 69.98 6.79 26 -10 6 76.62 6.96 26 -10 6 82.48 7.29 -26 10 -3 16.97 5.34 -26 10 -3 17.49 4.18 26 -10 3 18.18 3.56 26 -10 3 16.85 3.88 -26 10 0 49.14 6.51 -26 10 0 65.71 7.18 26 -10 0 63.45 6.93 26 -10 0 56.08 6.62 -26 10 3 73.90 6.58 -26 10 3 73.33 6.94 26 -10 -3 78.18 7.93 26 -10 -3 79.87 6.74 -26 10 6 24.12 4.22 26 -10 -6 20.71 3.95 -26 10 9 86.46 8.32 -26 10 9 85.61 8.20 -26 10 9 91.38 7.74 26 -10 -9 87.40 9.41 -26 10 12 18.13 5.14 -26 10 12 12.03 3.79 -26 10 12 13.35 4.89 26 -10 -12 10.25 6.27 -27 9 -9 2.65 2.87 -27 9 -9 0.67 3.00 27 -9 9 -0.25 3.67 27 -9 9 1.21 3.24 -27 9 -6 54.45 6.32 -27 9 -6 45.63 6.88 27 -9 6 58.76 7.06 27 -9 6 53.46 6.42 -27 9 -3 58.29 7.40 -27 9 -3 58.44 7.04 27 -9 3 52.09 6.82 27 -9 3 63.11 6.20 -27 9 0 86.41 7.67 -27 9 0 77.65 7.60 27 -9 0 67.80 7.12 27 -9 0 89.81 7.74 -27 9 3 110.01 8.28 27 -9 -3 95.84 7.72 -27 9 6 102.52 8.54 -27 9 6 97.67 8.73 27 -9 -6 104.50 8.58 27 -9 -6 105.19 9.27 -27 9 9 19.53 4.01 -27 9 9 13.23 3.54 -27 9 9 9.90 4.14 27 -9 -9 19.20 6.54 -28 8 -6 62.82 8.61 -28 8 -6 69.57 7.68 28 -8 6 81.44 7.34 28 -8 6 70.05 7.07 -28 8 -3 70.90 7.17 -28 8 -3 63.12 8.52 28 -8 3 67.51 7.46 28 -8 3 64.26 7.26 -28 8 0 45.13 5.73 28 -8 0 43.23 5.92 -28 8 3 -0.78 3.38 -28 8 3 4.88 2.94 28 -8 -3 1.10 2.60 28 -8 -3 1.26 3.31 -28 8 6 247.11 13.91 -28 8 6 250.07 15.96 28 -8 -6 286.55 14.05 28 -8 -6 254.34 15.98 -29 7 -3 175.71 14.52 -29 7 -3 212.75 13.00 29 -7 3 211.15 12.28 -29 7 0 84.18 9.01 -29 7 0 96.98 8.73 29 -7 0 87.69 8.00 29 -7 0 97.64 9.48 -29 7 3 95.34 9.18 -29 7 3 85.50 7.80 29 -7 -3 96.00 7.79 -8 29 -4 4.13 1.30 -8 29 -1 1.52 1.19 8 -29 1 5.48 5.96 -8 29 2 26.26 2.99 -8 29 2 21.98 6.07 -8 29 2 22.37 2.68 8 -29 -2 32.97 6.67 -8 29 5 3.35 5.98 -8 29 5 -0.11 3.13 -8 29 5 1.75 1.27 -8 29 5 0.60 1.99 -9 28 -7 0.82 3.54 9 -28 7 10.12 5.40 -9 28 -4 119.60 9.74 -9 28 -4 107.40 5.16 9 -28 4 126.31 11.45 -9 28 -1 5.42 1.66 -9 28 -1 7.22 1.80 -9 28 -1 6.69 5.81 -9 28 2 0.05 1.32 -9 28 2 0.15 1.81 9 -28 -2 -5.21 5.72 -9 28 5 39.72 5.84 -9 28 5 35.76 3.87 -9 28 5 43.33 8.92 -9 28 5 44.12 4.44 -9 28 8 6.10 2.88 -9 28 8 12.36 5.33 -9 28 8 8.05 4.26 9 -28 -8 8.24 2.96 -10 27 -10 7.13 1.78 -10 27 -10 9.51 3.69 10 -27 10 10.93 3.79 10 -27 10 6.91 1.68 -10 27 -7 207.45 8.01 -10 27 -7 206.11 7.56 -10 27 -7 228.35 12.12 10 -27 7 239.25 14.56 -10 27 -4 64.50 6.74 -10 27 -4 65.62 4.05 -10 27 -4 67.04 4.24 10 -27 4 70.51 8.28 -10 27 -1 309.95 16.95 -10 27 -1 309.20 10.81 -10 27 -1 334.72 11.45 10 -27 1 349.15 19.16 -10 27 2 89.41 5.34 -10 27 2 83.51 5.58 -10 27 2 85.01 8.79 10 -27 -2 82.22 9.07 -10 27 5 42.59 3.88 -10 27 5 43.37 6.18 -10 27 5 41.05 4.62 -10 27 8 53.68 8.29 -10 27 8 52.48 5.27 -10 27 8 54.26 8.58 10 -27 -8 59.00 5.31 -10 27 11 26.58 5.86 -10 27 11 15.14 6.45 -10 27 11 20.88 4.27 -11 26 -13 4.10 2.82 -11 26 -13 5.01 1.74 11 -26 13 3.19 3.43 11 -26 13 0.13 2.09 -11 26 -10 9.59 2.34 -11 26 -10 7.67 2.44 11 -26 10 12.26 2.39 11 -26 10 9.31 4.52 -11 26 -7 102.31 5.61 -11 26 -7 121.96 8.56 11 -26 7 109.68 5.48 11 -26 7 117.47 9.53 -11 26 -4 6.86 2.14 -11 26 -4 8.09 2.11 -11 26 -4 7.33 3.30 11 -26 4 7.60 3.53 -11 26 -1 8.98 2.34 -11 26 -1 8.47 4.47 -11 26 -1 9.27 2.01 11 -26 1 3.09 3.88 -11 26 2 40.89 7.44 -11 26 2 38.56 5.31 -11 26 2 42.02 4.15 -11 26 2 37.39 3.84 -11 26 5 4.87 4.71 -11 26 5 5.45 2.42 -11 26 5 7.16 2.64 -11 26 8 3.93 3.44 -11 26 8 0.67 4.73 -11 26 8 4.62 5.33 11 -26 -8 9.70 3.12 -11 26 11 13.75 4.59 -11 26 11 18.31 5.68 -12 25 -13 105.80 6.72 -12 25 -13 112.58 7.13 12 -25 13 106.72 8.20 12 -25 13 99.38 6.11 -12 25 -10 160.45 8.00 -12 25 -10 168.25 8.71 12 -25 10 158.08 7.57 12 -25 10 177.07 10.67 -12 25 -7 219.06 10.79 -12 25 -7 235.19 9.55 12 -25 7 251.65 13.32 12 -25 7 231.90 9.30 -12 25 -4 377.99 13.19 -12 25 -4 406.12 16.64 12 -25 4 412.78 18.59 -12 25 -1 194.41 11.89 -12 25 -1 201.59 8.74 -12 25 -1 184.90 8.38 -12 25 -1 179.23 9.81 -12 25 2 118.28 6.55 -12 25 2 110.64 8.60 -12 25 2 116.51 10.77 -12 25 2 106.86 6.09 -12 25 5 90.52 10.33 -12 25 5 67.62 5.28 -12 25 5 86.43 8.10 -12 25 5 72.93 5.36 -12 25 8 10.74 3.52 -12 25 8 8.42 2.45 -12 25 11 5.72 3.84 -12 25 11 2.96 5.01 -12 25 14 71.89 8.83 -12 25 14 73.07 9.70 -12 25 14 67.67 7.47 12 -25 -14 74.46 6.60 -13 24 -16 3.54 2.31 -13 24 -16 8.97 2.97 13 -24 16 6.49 3.05 13 -24 16 8.01 2.96 -13 24 -13 84.44 5.26 -13 24 -13 94.02 6.69 13 -24 13 89.87 6.31 13 -24 13 84.52 6.55 -13 24 -10 10.78 2.60 -13 24 -10 14.25 3.05 13 -24 10 12.63 3.70 13 -24 10 13.80 2.97 -13 24 -7 13.05 2.38 -13 24 -7 17.47 3.00 13 -24 7 12.03 2.82 13 -24 7 14.76 3.53 -13 24 -4 -1.32 2.20 -13 24 -4 0.24 2.68 13 -24 4 1.73 2.09 13 -24 4 7.07 3.47 -13 24 -1 92.88 6.45 -13 24 -1 106.54 8.36 -13 24 -1 94.91 6.05 -13 24 -1 103.46 5.72 -13 24 2 96.99 7.50 -13 24 2 88.68 9.03 -13 24 2 88.34 6.17 -13 24 2 78.36 5.53 -13 24 5 4.90 2.64 -13 24 5 5.09 2.16 -13 24 5 3.96 4.52 -13 24 5 5.22 3.26 -13 24 8 17.00 2.94 -13 24 8 21.15 3.59 -13 24 8 13.54 6.80 -13 24 11 72.84 8.40 -13 24 11 75.05 10.43 -13 24 14 18.87 5.13 -13 24 14 12.34 3.76 -13 24 14 10.67 7.67 13 -24 -14 18.22 3.56 -14 23 -16 9.32 1.93 -14 23 -16 7.52 2.52 14 -23 16 7.06 2.64 14 -23 16 4.95 2.45 -14 23 -13 33.76 3.97 14 -23 13 35.07 4.58 -14 23 -10 13.30 3.11 14 -23 10 16.09 3.32 -14 23 -7 306.52 12.00 14 -23 7 297.79 11.45 14 -23 7 311.32 13.11 -14 23 -4 23.34 3.32 -14 23 -4 24.11 3.67 -14 23 -4 20.62 3.92 14 -23 4 27.95 3.63 -14 23 -1 138.56 7.35 -14 23 -1 124.81 7.01 -14 23 -1 120.01 7.58 -14 23 2 28.37 3.75 -14 23 2 23.55 5.30 -14 23 2 27.89 3.61 -14 23 5 218.00 9.95 -14 23 5 216.39 10.46 -14 23 5 231.84 12.31 -14 23 5 238.10 15.06 -14 23 8 3.60 2.64 -14 23 8 -0.87 5.40 -14 23 8 3.60 3.30 -14 23 8 -2.45 4.46 -14 23 11 110.49 8.91 -14 23 14 19.11 6.06 -14 23 14 24.78 4.19 14 -23 -14 14.63 4.46 14 -23 -14 14.91 4.60 -14 23 17 18.18 6.07 -14 23 17 21.25 4.91 14 -23 -17 26.90 6.80 14 -23 -17 16.15 3.98 -15 22 -16 187.35 10.77 15 -22 16 202.76 10.80 -15 22 -13 393.87 16.13 15 -22 13 365.28 14.93 -15 22 -10 259.61 7.74 -15 22 -10 288.21 12.37 15 -22 10 283.93 11.95 15 -22 10 269.54 9.58 -15 22 -7 355.91 14.10 -15 22 -7 342.20 10.73 -15 22 -7 339.59 10.61 15 -22 7 379.39 14.13 -15 22 -4 335.81 11.75 15 -22 4 351.77 12.78 -15 22 -1 217.09 11.21 -15 22 -1 198.93 9.56 -15 22 -1 194.82 8.97 15 -22 1 205.51 9.12 -15 22 2 1.78 2.73 -15 22 2 -1.73 2.66 -15 22 2 -0.51 1.43 -15 22 2 -0.78 3.48 -15 22 5 65.93 5.68 -15 22 5 81.17 7.25 -15 22 5 73.46 6.02 -15 22 5 73.40 8.54 -15 22 8 25.94 3.69 -15 22 8 27.37 5.78 -15 22 8 26.32 3.62 -15 22 14 56.63 7.73 -15 22 14 46.48 5.24 15 -22 -14 45.16 5.25 15 -22 -14 46.02 8.00 -15 22 17 15.14 4.84 -15 22 17 21.25 4.18 15 -22 -17 13.00 6.53 15 -22 -17 16.03 4.97 -16 21 -13 206.31 11.34 16 -21 13 196.78 10.60 -16 21 -10 16.36 4.10 16 -21 10 8.54 2.81 -16 21 -7 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53.86 6.01 -28 9 8 51.84 6.73 28 -9 -8 43.33 7.98 -29 8 -4 4.17 3.98 29 -8 4 5.54 3.23 29 -8 4 3.75 3.30 -29 8 -1 49.01 5.78 -29 8 -1 61.46 7.44 29 -8 1 46.59 6.82 -29 8 2 6.33 4.14 -29 8 2 11.16 5.86 29 -8 -2 11.07 5.67 29 -8 -2 4.56 4.66 -29 8 5 4.02 4.10 -29 8 5 7.90 3.06 29 -8 -5 10.56 5.59 29 -8 -5 1.77 3.31 -9 29 -5 445.88 21.03 9 -29 5 493.58 25.16 -9 29 -2 128.90 5.92 -9 29 -2 129.48 5.99 -9 29 1 187.19 8.33 -9 29 1 185.29 7.84 -9 29 1 196.65 13.99 9 -29 -1 217.10 16.41 -9 29 4 234.84 9.80 -9 29 4 224.39 10.07 -9 29 4 240.73 16.28 -9 29 4 258.54 15.99 -10 28 -8 3.22 1.84 -10 28 -8 -1.21 2.72 -10 28 -8 1.80 1.23 10 -28 8 -0.86 3.98 -10 28 -5 43.32 3.33 -10 28 -5 47.44 6.65 -10 28 -5 43.91 3.21 10 -28 5 57.75 8.32 -10 28 -2 18.24 4.42 -10 28 -2 11.31 2.06 -10 28 -2 13.64 2.32 10 -28 2 14.82 5.03 -10 28 1 61.68 7.19 -10 28 1 51.67 4.08 -10 28 1 52.88 4.24 -10 28 4 1.94 2.53 -10 28 4 0.22 3.52 -10 28 4 2.96 1.97 -10 28 4 6.83 6.17 -10 28 7 162.93 8.73 -10 28 7 166.72 15.16 -10 28 7 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315.49 13.04 -13 25 10 175.10 13.69 -13 25 10 165.83 12.23 -13 25 10 161.14 9.90 -13 25 13 148.77 14.92 -13 25 13 151.81 10.52 -13 25 13 141.70 11.20 13 -25 -13 150.99 9.38 -14 24 -14 33.38 3.94 14 -24 14 29.07 3.98 14 -24 14 28.48 3.75 -14 24 -11 141.47 8.33 14 -24 11 132.55 7.59 14 -24 11 134.11 7.75 -14 24 -8 195.68 8.58 -14 24 -8 203.05 9.66 14 -24 8 213.37 10.61 14 -24 8 206.86 9.46 -14 24 -5 294.51 12.47 -14 24 -5 288.59 11.60 -14 24 -5 300.10 12.04 14 -24 5 316.14 11.95 -14 24 -2 329.38 12.48 -14 24 -2 348.07 14.02 -14 24 -2 332.31 14.95 14 -24 2 342.54 12.37 -14 24 1 151.67 10.86 -14 24 1 144.23 9.09 -14 24 1 150.99 7.63 -14 24 1 147.44 7.91 -14 24 4 506.10 20.05 -14 24 4 499.91 22.95 -14 24 4 513.77 17.70 -14 24 4 532.15 18.22 -14 24 7 351.19 20.17 -14 24 7 374.83 17.31 -14 24 10 410.13 19.66 -14 24 10 444.26 18.22 -14 24 13 225.02 14.74 -14 24 13 232.64 18.45 -14 24 13 222.72 11.84 14 -24 -13 227.36 12.03 -14 24 16 71.96 12.13 -14 24 16 73.14 6.90 -14 24 16 66.38 8.00 14 -24 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3.11 17 -21 -1 3.76 2.41 -17 21 4 17.65 3.93 -17 21 4 19.96 4.20 -17 21 4 16.51 3.88 17 -21 -4 16.04 3.54 -17 21 7 172.95 10.22 -17 21 7 173.33 9.42 -17 21 7 172.83 9.32 17 -21 -7 156.91 9.81 -17 21 10 2.38 3.30 -17 21 10 2.91 3.35 -17 21 13 7.55 4.89 -17 21 13 3.22 3.27 17 -21 -13 8.13 4.29 17 -21 -13 3.54 2.79 -17 21 16 47.21 7.09 -17 21 16 37.75 5.21 17 -21 -16 46.88 5.31 17 -21 -16 38.91 7.05 -18 20 -17 27.42 5.34 18 -20 17 23.81 5.12 -18 20 -11 2.96 3.40 18 -20 11 8.66 3.92 -18 20 -8 194.80 10.08 18 -20 8 179.39 9.99 -18 20 -5 16.14 1.50 -18 20 -5 17.13 2.00 -18 20 -5 18.90 4.18 18 -20 5 20.43 3.98 -18 20 -2 26.44 4.51 18 -20 2 26.46 3.48 -18 20 1 43.15 4.32 -18 20 1 49.49 5.33 18 -20 -1 52.53 4.92 18 -20 -1 45.56 4.59 -18 20 4 -0.19 2.32 -18 20 4 6.07 2.72 -18 20 4 1.36 3.56 18 -20 -4 1.95 2.58 -18 20 7 65.60 5.67 -18 20 7 64.39 5.65 -18 20 7 63.37 5.87 18 -20 -7 68.39 7.20 -18 20 10 102.12 8.50 -18 20 10 100.29 6.93 18 -20 -10 95.82 8.44 -18 20 13 171.56 9.81 -18 20 13 191.49 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20 -18 8 7.83 3.05 -20 18 -5 65.32 3.12 -20 18 -5 72.26 6.40 20 -18 5 60.43 3.00 20 -18 5 66.16 6.28 -20 18 -2 240.50 11.40 20 -18 2 254.17 12.18 -20 18 1 227.81 10.92 -20 18 1 215.88 9.58 20 -18 -1 222.28 11.34 20 -18 -1 220.01 9.93 -20 18 4 18.00 3.24 -20 18 4 10.73 4.07 20 -18 -4 17.01 4.10 -20 18 7 314.99 14.13 20 -18 -7 324.03 14.63 -20 18 10 713.02 26.56 -20 18 10 715.06 24.18 -20 18 10 735.97 25.21 20 -18 -10 743.74 27.96 -20 18 13 442.60 18.61 -20 18 13 455.73 20.04 -20 18 13 433.55 18.11 20 -18 -13 448.25 20.77 -20 18 16 151.46 11.22 -20 18 16 158.27 10.42 20 -18 -16 157.98 12.06 20 -18 -16 143.11 9.39 -21 17 -17 8.01 3.58 21 -17 17 15.24 5.05 -21 17 -14 201.08 11.88 21 -17 14 203.77 11.51 -21 17 -11 78.94 6.81 21 -17 11 77.04 6.56 -21 17 -5 71.01 3.87 21 -17 5 71.96 3.64 21 -17 5 70.40 6.60 -21 17 -2 487.19 18.15 -21 17 -2 473.28 14.36 21 -17 2 455.12 17.27 -21 17 1 429.99 17.25 -21 17 1 433.52 14.99 21 -17 -1 460.86 17.66 21 -17 -1 464.57 16.24 -21 17 4 45.56 4.49 21 -17 -4 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15 -14 70.56 6.99 23 -15 14 67.76 7.49 23 -15 14 63.17 3.49 23 -15 14 64.71 3.44 -23 15 -11 66.86 6.51 23 -15 11 56.82 3.32 23 -15 11 57.72 3.25 23 -15 11 69.33 7.15 -23 15 -8 8.51 3.45 -23 15 -8 4.60 2.09 23 -15 8 5.94 1.53 23 -15 8 7.54 3.54 -23 15 -5 8.24 2.60 -23 15 -5 6.15 4.51 -23 15 -2 58.14 5.77 -23 15 -2 53.16 4.95 23 -15 2 49.83 4.08 -23 15 1 29.64 3.81 -23 15 1 22.21 4.64 23 -15 -1 25.90 4.33 -23 15 4 209.48 11.31 -23 15 4 214.85 11.64 23 -15 -4 194.66 11.18 23 -15 -4 211.25 10.96 -23 15 7 118.00 8.04 -23 15 7 125.59 8.83 -23 15 7 125.49 8.69 23 -15 -7 127.99 9.42 -23 15 10 4.90 4.11 -23 15 10 5.82 3.12 -23 15 13 18.77 4.76 -23 15 13 25.14 5.11 23 -15 -13 25.38 5.23 -23 15 16 95.59 8.35 -23 15 16 100.68 8.15 -23 15 16 93.71 9.00 23 -15 -16 102.15 10.44 -24 14 -14 149.87 10.88 24 -14 14 171.32 10.97 24 -14 14 144.25 6.58 -24 14 -11 17.25 3.94 24 -14 11 21.91 4.40 -24 14 -8 101.37 8.39 -24 14 -8 85.18 5.73 24 -14 8 103.43 7.86 -24 14 -5 353.51 15.92 -24 14 -5 306.16 12.70 24 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28.00 5.53 -27 11 -11 10.17 4.26 27 -11 11 9.75 3.99 27 -11 11 4.76 2.09 -27 11 -8 -0.48 3.53 -27 11 -8 4.91 4.58 27 -11 8 0.71 2.34 27 -11 8 -0.13 4.48 -27 11 -5 1.37 2.53 -27 11 -5 1.35 4.03 27 -11 5 -0.43 4.08 27 -11 5 1.47 2.75 -27 11 -2 28.09 4.55 -27 11 -2 23.30 4.44 27 -11 2 25.31 5.05 27 -11 2 21.66 5.37 -27 11 1 0.19 2.58 -27 11 1 3.06 3.74 27 -11 -1 1.46 2.83 27 -11 -1 1.81 4.40 -27 11 4 36.00 5.10 27 -11 -4 42.66 6.85 27 -11 -4 30.76 4.58 -27 11 7 8.30 3.91 -27 11 7 9.08 4.08 27 -11 -7 9.56 3.65 27 -11 -7 8.93 4.65 -27 11 10 73.10 7.01 -27 11 10 70.64 6.67 -27 11 10 85.04 9.36 27 -11 -10 81.76 8.15 -28 10 -8 14.51 5.09 -28 10 -8 16.02 4.59 28 -10 8 11.23 3.02 28 -10 8 11.78 3.83 -28 10 -5 3.24 4.42 -28 10 -5 5.77 4.21 28 -10 5 4.58 3.05 28 -10 5 4.45 3.05 -28 10 -2 56.32 7.79 -28 10 -2 74.81 7.04 28 -10 2 75.29 7.86 28 -10 2 68.56 7.51 -28 10 1 10.68 5.35 -28 10 1 8.34 3.28 28 -10 -1 8.93 3.37 28 -10 -1 3.49 4.50 -28 10 4 8.30 3.81 -28 10 4 1.66 2.94 28 -10 -4 9.13 3.21 -28 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12.16 2.91 -11 28 6 2.52 2.30 -11 28 6 -5.02 6.32 -11 28 6 -3.69 4.22 -11 28 6 1.60 2.16 -11 28 9 4.35 2.48 -11 28 9 10.54 5.21 -11 28 9 0.85 7.34 11 -28 -9 1.58 2.87 -12 27 -12 245.18 11.45 -12 27 -12 239.58 10.27 12 -27 12 260.87 13.97 12 -27 12 244.64 10.05 -12 27 -9 207.23 9.19 -12 27 -9 219.99 11.16 12 -27 9 218.19 9.10 12 -27 9 205.07 12.76 -12 27 -6 72.98 7.00 -12 27 -6 73.94 4.75 12 -27 6 74.62 7.88 12 -27 6 73.18 4.70 -12 27 -3 254.92 14.21 -12 27 -3 221.55 9.38 -12 27 -3 226.05 9.37 12 -27 3 261.27 15.46 -12 27 0 125.72 9.19 -12 27 0 115.34 9.51 -12 27 0 97.04 5.99 -12 27 0 103.51 5.86 -12 27 3 73.77 7.63 -12 27 3 64.48 5.37 -12 27 3 63.25 5.08 -12 27 3 70.37 9.54 -12 27 6 8.19 2.33 -12 27 6 12.12 2.43 -12 27 9 8.76 6.66 -12 27 9 25.70 6.53 -12 27 9 13.85 4.18 12 -27 -9 19.07 3.65 -12 27 12 1.14 4.90 -12 27 12 3.08 2.63 -12 27 12 5.32 5.43 12 -27 -12 3.85 2.49 -13 26 -12 63.13 5.31 -13 26 -12 59.93 5.10 13 -26 12 65.47 4.83 13 -26 12 56.52 6.24 -13 26 -9 250.50 10.68 -13 26 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3.67 14 -25 3 21.49 2.64 -14 25 0 23.05 2.94 -14 25 0 23.04 3.56 -14 25 0 31.10 4.67 -14 25 0 25.13 4.22 -14 25 3 3.51 2.91 -14 25 3 -1.36 2.59 -14 25 3 4.35 5.04 -14 25 3 2.19 2.62 -14 25 6 7.51 4.30 -14 25 6 4.31 2.09 -14 25 6 1.24 4.55 -14 25 6 0.54 3.05 -14 25 9 11.50 3.19 -14 25 9 6.45 3.62 -14 25 9 14.85 3.90 -14 25 12 263.20 15.01 -14 25 12 243.90 13.31 -14 25 12 226.86 18.48 14 -25 -12 249.90 13.06 -14 25 15 9.04 4.58 -14 25 15 12.60 6.63 -14 25 15 10.51 4.79 14 -25 -15 8.28 3.10 -15 24 -15 45.51 5.51 15 -24 15 47.12 4.82 -15 24 -12 -0.07 1.37 -15 24 -12 -0.59 2.92 15 -24 12 -0.35 2.47 -15 24 -9 44.09 5.05 15 -24 9 46.91 4.86 -15 24 -6 10.15 2.67 -15 24 -6 7.68 2.35 -15 24 -6 11.79 2.53 15 -24 6 12.00 2.92 -15 24 -3 313.53 12.30 -15 24 -3 320.17 13.55 -15 24 -3 316.58 12.57 15 -24 3 322.81 12.48 -15 24 0 11.86 2.31 -15 24 0 13.63 3.81 -15 24 0 11.98 3.41 -15 24 0 16.22 3.09 -15 24 3 14.79 3.94 -15 24 3 11.71 4.65 -15 24 3 8.53 2.33 -15 24 3 8.86 3.31 -15 24 6 5.37 3.44 -15 24 6 13.15 2.97 -15 24 6 20.21 5.28 -15 24 9 16.11 3.52 -15 24 12 184.92 12.08 -15 24 12 159.26 9.87 -15 24 12 179.68 14.18 15 -24 -12 169.38 10.43 -15 24 15 -1.31 3.94 -15 24 15 1.90 5.23 15 -24 -15 4.50 3.76 15 -24 -15 -6.59 5.59 -16 23 -15 2.67 1.09 -16 23 -15 1.46 2.76 16 -23 15 2.19 1.69 16 -23 15 3.01 3.08 -16 23 -12 -0.10 0.73 -16 23 -12 -2.19 1.75 16 -23 12 -0.35 2.85 16 -23 12 0.35 1.41 -16 23 -9 63.30 5.89 16 -23 9 65.28 5.27 -16 23 -6 16.22 2.93 16 -23 6 11.21 2.57 -16 23 -3 97.29 6.85 -16 23 -3 94.06 6.01 -16 23 -3 86.85 6.60 16 -23 3 94.86 6.64 -16 23 0 39.94 5.58 -16 23 0 44.65 4.46 -16 23 0 37.26 4.12 -16 23 0 42.06 4.64 -16 23 3 61.28 5.55 -16 23 3 69.67 7.52 -16 23 3 76.49 5.62 -16 23 3 70.08 6.16 -16 23 6 57.56 5.85 -16 23 6 59.46 8.28 -16 23 6 55.90 6.73 -16 23 6 60.01 5.63 -16 23 9 88.95 8.68 16 -23 -9 89.07 9.11 -16 23 12 20.01 4.57 -16 23 12 16.94 4.03 16 -23 -12 20.65 4.85 16 -23 -12 20.74 3.91 -16 23 15 16.09 5.24 -16 23 15 21.45 6.45 16 -23 -15 20.04 3.92 16 -23 -15 18.51 6.34 -17 22 -12 291.14 13.83 17 -22 12 306.19 13.63 -17 22 -9 609.69 20.88 17 -22 9 632.25 20.93 -17 22 -6 734.23 17.10 -17 22 -6 725.14 17.61 -17 22 -6 812.40 24.99 17 -22 6 780.49 23.92 -17 22 -3 119.96 6.16 -17 22 -3 109.36 7.46 17 -22 3 125.66 7.57 -17 22 0 211.06 9.71 -17 22 0 201.99 11.13 -17 22 0 216.18 9.94 17 -22 0 215.95 10.17 -17 22 3 117.72 8.62 -17 22 3 115.74 7.89 -17 22 3 118.83 7.20 -17 22 3 118.05 7.36 -17 22 6 29.18 3.91 -17 22 6 36.17 4.01 -17 22 6 31.40 4.28 17 -22 -6 31.21 5.37 -17 22 9 -1.28 3.75 17 -22 -9 3.87 3.36 -17 22 12 7.48 3.04 -17 22 12 3.50 4.29 -17 22 12 8.47 3.30 17 -22 -12 7.23 4.17 -17 22 15 155.03 11.37 -17 22 15 165.86 10.39 17 -22 -15 154.11 11.44 17 -22 -15 162.27 10.67 -18 21 -15 32.80 5.48 18 -21 12 150.47 8.95 -18 21 -9 25.49 4.82 18 -21 9 31.97 4.71 -18 21 -6 109.86 7.05 -18 21 -6 103.82 3.63 18 -21 6 108.12 6.84 -18 21 -3 0.43 2.00 18 -21 3 -2.65 2.79 -18 21 0 426.28 14.45 -18 21 0 407.25 16.43 -18 21 0 419.93 15.55 18 -21 0 439.84 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192.72 11.21 20 -19 15 185.08 11.69 -20 19 -12 9.01 3.26 20 -19 9 40.51 4.86 -20 19 -6 -2.54 3.22 20 -19 6 0.49 2.25 -20 19 -3 16.93 3.74 20 -19 3 14.29 4.21 20 -19 3 21.87 2.59 -20 19 0 -0.90 2.13 -20 19 0 0.43 2.52 20 -19 0 5.38 3.15 20 -19 0 0.41 2.20 -20 19 3 -2.52 2.83 -20 19 3 0.55 2.55 20 -19 -3 1.44 2.27 20 -19 -3 3.47 2.62 -20 19 6 306.84 14.33 20 -19 -6 330.73 14.71 -20 19 9 51.23 5.71 -20 19 9 50.86 5.37 -20 19 9 48.67 5.16 20 -19 -9 53.81 7.32 -20 19 12 3.03 3.66 -20 19 12 4.20 4.26 -20 19 12 2.58 2.75 -20 19 15 11.96 4.28 -20 19 15 8.74 3.36 -20 19 15 11.35 3.94 20 -19 -15 9.79 3.79 -21 18 -15 22.54 4.37 21 -18 15 26.25 5.38 -21 18 -12 63.24 6.94 21 -18 12 65.69 6.14 21 -18 6 96.05 7.03 -21 18 -3 637.26 22.73 21 -18 3 683.15 18.14 21 -18 3 715.75 23.48 -21 18 0 1.71 2.67 -21 18 0 5.32 2.38 21 -18 0 6.61 2.76 21 -18 0 3.79 2.47 -21 18 3 60.10 5.34 21 -18 -3 52.45 5.34 21 -18 -3 59.02 5.27 -21 18 6 184.49 10.80 -21 18 6 197.42 10.62 21 -18 -6 203.68 11.47 -21 18 9 302.03 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19.66 4.80 -24 15 6 2.77 2.87 -24 15 6 1.06 3.54 24 -15 -6 1.77 2.74 24 -15 -9 1.92 2.88 -24 15 12 41.48 5.12 -24 15 12 39.37 5.76 -24 15 12 40.06 5.26 24 -15 -12 37.38 7.38 -24 15 15 53.00 6.03 -24 15 15 54.98 6.67 -24 15 15 52.82 7.95 24 -15 -15 54.01 7.08 -25 14 -15 17.26 4.29 25 -14 15 9.95 2.20 25 -14 15 9.28 2.27 25 -14 15 11.84 5.23 -25 14 -12 0.99 2.04 -25 14 -12 0.86 3.05 25 -14 12 -1.72 2.95 -25 14 -9 87.39 6.47 -25 14 -9 100.48 7.91 25 -14 9 91.43 5.31 25 -14 9 94.65 8.43 -25 14 -6 6.55 3.09 -25 14 -6 12.66 4.88 25 -14 6 9.93 2.49 25 -14 6 11.01 3.50 -25 14 -3 26.83 5.54 -25 14 -3 28.50 4.20 25 -14 3 26.39 3.96 25 -14 3 24.65 4.43 -25 14 0 175.74 9.77 -25 14 0 175.88 10.82 25 -14 0 175.90 9.46 -25 14 3 75.35 7.35 25 -14 -3 80.44 7.39 25 -14 -3 71.37 7.18 -25 14 6 28.93 4.70 -25 14 6 23.61 4.23 25 -14 -6 25.66 4.27 25 -14 -6 33.80 6.11 -25 14 9 2.80 3.79 -25 14 9 6.18 2.88 -25 14 12 -2.70 3.10 -25 14 12 0.04 2.91 25 -14 -12 -2.06 3.59 -25 14 15 133.90 11.78 -25 14 15 156.93 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4.20 -26 15 13 6.07 3.58 -26 15 13 0.18 2.96 -26 15 13 0.42 3.40 26 -15 -13 4.60 3.90 -27 14 -11 -0.95 3.55 -27 14 -11 1.20 2.72 27 -14 11 1.68 1.71 27 -14 11 -0.68 3.34 -27 14 -8 121.62 10.16 -27 14 -8 111.37 7.81 27 -14 8 103.92 6.58 27 -14 8 114.76 8.68 -27 14 -5 25.66 5.86 -27 14 -5 29.96 4.20 27 -14 5 32.27 3.67 -27 14 -2 82.45 6.58 27 -14 2 73.44 5.93 27 -14 2 84.29 7.16 -27 14 1 62.48 6.37 -27 14 1 53.99 5.70 27 -14 -1 58.15 5.67 27 -14 -1 64.67 6.02 -27 14 4 -0.55 2.69 -27 14 4 -1.54 2.45 27 -14 -4 2.39 2.71 27 -14 -4 6.74 3.73 -27 14 7 2.27 3.88 -27 14 7 3.43 2.52 -27 14 10 26.17 4.51 -27 14 10 26.82 6.32 -27 14 10 26.74 4.51 27 -14 -10 33.46 6.16 -28 13 -8 128.98 9.58 -28 13 -8 145.77 10.87 28 -13 8 160.30 11.26 28 -13 8 133.80 8.39 -28 13 -5 199.82 12.14 -28 13 -5 213.29 13.59 28 -13 5 244.01 13.54 28 -13 5 212.41 11.15 -28 13 -2 185.27 11.92 -28 13 -2 202.39 12.30 28 -13 2 205.64 11.63 28 -13 2 198.97 11.25 -28 13 1 91.34 7.60 -28 13 1 92.87 8.66 28 -13 -1 87.40 7.12 28 -13 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2.24 1.73 -13 29 -6 0.90 2.92 -13 29 -6 -2.03 1.59 13 -29 6 -1.02 3.99 -13 29 -3 5.94 2.40 -13 29 -3 6.50 2.15 -13 29 -3 7.65 4.71 13 -29 3 5.07 3.63 -13 29 0 1.54 5.23 -13 29 0 1.48 1.59 -13 29 0 1.97 2.26 -13 29 0 -0.44 3.14 -13 29 3 32.61 4.08 -13 29 3 28.67 3.91 -13 29 6 2.24 2.42 -13 29 6 -3.41 4.86 -13 29 6 4.23 6.35 -13 29 6 1.03 1.73 -14 28 -9 7.54 2.20 -14 28 -9 8.25 2.14 14 -28 9 8.04 2.50 14 -28 9 11.65 3.66 -14 28 -6 1.60 3.02 -14 28 -6 0.82 1.84 14 -28 6 -5.56 3.62 14 -28 6 -1.40 2.00 -14 28 -3 -0.80 1.90 -14 28 -3 1.96 2.55 -14 28 -3 0.74 2.19 -14 28 -3 2.41 1.88 -14 28 0 8.42 2.53 -14 28 0 9.50 2.97 -14 28 0 9.10 3.91 -14 28 0 5.43 2.47 -14 28 3 30.09 7.03 -14 28 3 30.91 5.10 -14 28 3 25.45 3.70 -14 28 3 27.43 3.88 -14 28 6 19.65 3.76 -14 28 6 20.37 3.67 -14 28 6 22.31 4.47 -14 28 9 14.09 5.91 -15 27 -12 5.30 1.88 -15 27 -12 3.82 2.56 15 -27 12 3.23 1.96 15 -27 12 4.91 2.86 -15 27 -9 30.54 3.54 -15 27 -9 30.03 3.62 15 -27 9 33.40 3.96 15 -27 9 38.20 4.81 -15 27 -6 37.62 4.58 -15 27 -6 41.23 4.43 -15 27 -6 45.85 4.52 15 -27 6 39.83 3.72 -15 27 -3 143.39 7.75 -15 27 -3 126.03 7.11 -15 27 -3 142.51 8.30 -15 27 -3 129.88 8.45 -15 27 0 1.57 2.55 -15 27 0 -3.06 3.45 -15 27 0 0.13 2.60 -15 27 0 -2.44 2.42 -15 27 3 27.05 5.68 -15 27 3 36.03 4.75 -15 27 3 27.01 3.62 -15 27 3 28.02 4.27 -15 27 6 120.87 7.96 -15 27 6 118.78 11.91 -15 27 6 115.23 7.42 -15 27 9 218.59 17.16 -15 27 9 217.18 13.68 -15 27 12 65.18 7.86 -15 27 12 64.39 9.59 -15 27 12 64.82 7.17 15 -27 -12 74.25 6.38 -16 26 -12 12.66 3.77 16 -26 12 19.59 3.24 -16 26 -9 82.59 5.02 -16 26 -9 83.80 6.55 16 -26 9 88.03 6.03 -16 26 -6 21.16 3.69 -16 26 -6 18.15 3.20 -16 26 -6 19.79 3.22 16 -26 6 19.15 2.98 -16 26 -3 82.02 6.29 -16 26 -3 68.10 6.06 -16 26 -3 76.36 5.85 16 -26 3 78.69 5.86 -16 26 0 63.62 6.12 -16 26 0 61.08 7.11 -16 26 0 60.31 5.13 -16 26 0 56.64 5.14 -16 26 3 11.77 4.70 -16 26 3 14.42 3.45 -16 26 3 16.43 3.42 -16 26 3 18.13 3.54 -16 26 6 76.36 7.23 -16 26 6 80.29 10.09 -16 26 6 82.97 6.24 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4.43 2.14 18 -24 3 3.70 2.19 -18 24 0 2.19 3.20 -18 24 0 6.62 2.80 -18 24 0 5.75 2.21 18 -24 0 2.85 3.25 -18 24 3 7.10 3.20 -18 24 3 5.03 3.10 -18 24 3 3.27 2.13 -18 24 3 4.26 3.48 -18 24 6 6.10 3.45 -18 24 6 3.02 2.36 -18 24 6 8.54 4.11 -18 24 9 6.29 2.86 -18 24 9 4.39 3.82 18 -24 -9 9.44 5.07 -18 24 12 2.89 3.65 -18 24 12 7.33 3.18 -18 24 12 9.27 3.35 18 -24 -12 11.76 5.88 -18 24 15 12.10 3.64 -18 24 15 12.20 5.78 18 -24 -15 10.84 4.54 18 -24 -15 12.30 4.08 -19 23 -15 12.30 4.69 19 -23 15 17.52 4.33 -19 23 -9 46.54 5.76 19 -23 9 51.14 5.14 -19 23 -6 50.27 2.64 -19 23 -6 45.38 5.77 -19 23 -6 50.26 3.13 19 -23 6 51.79 5.51 -19 23 -3 1.17 2.34 -19 23 -3 4.42 1.98 19 -23 3 3.24 3.09 -19 23 0 134.80 7.46 -19 23 0 138.84 9.00 -19 23 0 126.40 7.63 19 -23 0 141.00 8.70 -19 23 3 284.89 12.37 -19 23 3 287.66 12.99 -19 23 3 286.83 15.36 -19 23 3 283.13 12.94 -19 23 6 86.62 6.80 19 -23 -6 85.74 7.51 -19 23 9 42.36 5.40 -19 23 9 51.85 5.65 -19 23 9 54.63 5.29 19 -23 -9 56.43 7.26 -19 23 12 67.93 7.26 -19 23 12 70.48 7.38 -19 23 12 63.93 6.54 19 -23 -12 74.67 8.51 -19 23 15 35.08 6.32 -19 23 15 38.75 7.27 19 -23 -15 34.11 5.93 19 -23 -15 29.97 4.75 -20 22 -15 18.76 3.97 20 -22 15 17.67 4.70 -20 22 -12 26.35 4.52 20 -22 9 9.24 3.74 -20 22 -6 30.54 1.58 -20 22 -6 28.41 5.06 -20 22 -6 29.20 1.77 20 -22 6 33.64 4.97 -20 22 -3 130.14 8.74 20 -22 3 132.92 8.19 -20 22 0 212.17 11.25 -20 22 0 211.87 11.18 -20 22 0 194.17 8.76 20 -22 0 208.26 10.45 -20 22 3 81.41 6.19 -20 22 3 73.55 6.19 20 -22 -3 76.51 5.99 -20 22 6 163.01 9.37 -20 22 6 176.98 10.47 20 -22 -6 183.07 11.51 -20 22 9 418.92 17.40 -20 22 9 416.42 17.95 -20 22 9 349.62 17.61 20 -22 -9 424.16 18.80 -20 22 12 298.60 14.08 -20 22 12 292.09 15.33 -20 22 12 305.87 14.80 20 -22 -12 314.73 16.83 -20 22 15 181.88 11.23 -20 22 15 196.93 11.90 -20 22 15 168.64 12.94 20 -22 -15 152.23 12.95 -21 21 -15 4.08 2.90 21 -21 15 2.34 3.00 -21 21 -12 7.76 3.19 21 -21 12 5.37 3.78 21 -21 6 14.77 3.27 21 -21 3 -4.18 2.56 -21 21 0 84.89 5.25 21 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5.71 23 -19 15 22.24 5.43 -23 19 -12 4.80 3.18 23 -19 12 -0.42 3.66 -23 19 -9 -4.00 2.57 23 -19 9 2.94 2.72 -23 19 -6 0.73 2.49 -23 19 -6 0.88 0.90 23 -19 6 2.49 3.90 23 -19 6 -0.30 1.09 -23 19 -3 71.28 6.25 -23 19 0 4.41 2.72 -23 19 0 0.38 3.31 23 -19 0 1.28 2.70 -23 19 3 0.50 3.32 -23 19 3 -2.39 3.32 23 -19 -3 0.78 3.20 23 -19 -3 0.45 2.88 -23 19 6 3.80 2.76 -23 19 6 1.54 3.79 -23 19 6 4.94 3.82 -23 19 9 6.14 4.87 -23 19 9 2.52 3.05 -23 19 9 3.09 3.93 23 -19 -9 1.98 3.30 -23 19 12 53.62 5.74 -23 19 12 42.41 6.55 -23 19 12 44.43 6.09 23 -19 -12 50.95 6.54 -23 19 15 2.92 4.13 -23 19 15 3.85 3.01 -23 19 15 1.81 5.49 23 -19 -15 2.29 4.01 -24 18 -15 25.76 4.58 24 -18 15 22.75 5.09 -24 18 -12 2.16 2.86 24 -18 12 3.71 4.47 -24 18 -9 102.41 8.07 24 -18 9 111.90 8.22 -24 18 -6 164.73 10.24 -24 18 -6 151.93 6.26 24 -18 6 162.64 6.42 24 -18 6 158.05 9.72 -24 18 -3 31.77 4.57 -24 18 -3 30.44 3.41 24 -18 3 35.89 4.58 24 -18 3 33.14 3.46 -24 18 0 63.68 4.81 -24 18 0 57.92 5.77 24 -18 0 64.21 5.97 24 -18 0 67.29 5.59 -24 18 3 72.75 5.89 -24 18 3 68.58 6.27 24 -18 -3 69.88 6.38 24 -18 -3 70.40 6.41 -24 18 6 14.08 4.40 -24 18 6 15.22 3.59 -24 18 6 10.70 4.01 24 -18 -6 14.70 4.71 -24 18 9 180.28 11.35 -24 18 9 196.49 11.28 24 -18 -9 194.42 11.87 -24 18 12 38.76 5.41 -24 18 12 47.47 5.77 -24 18 12 37.07 4.82 24 -18 -12 46.98 7.52 -24 18 15 221.80 15.02 -24 18 15 219.59 13.17 -24 18 15 218.70 13.21 24 -18 -15 222.04 15.03 -25 17 -12 -1.77 2.51 25 -17 12 0.09 0.53 25 -17 12 7.29 4.29 25 -17 12 -0.17 0.23 -25 17 -9 0.70 1.44 -25 17 -9 -0.29 4.37 25 -17 9 -0.24 2.90 25 -17 9 1.15 1.18 -25 17 -6 -0.10 2.94 25 -17 6 0.78 3.74 -25 17 -3 5.97 2.62 -25 17 -3 3.26 3.20 25 -17 3 8.81 4.32 25 -17 3 4.11 2.19 -25 17 0 72.96 6.56 -25 17 0 72.62 5.77 25 -17 0 75.43 5.60 25 -17 0 71.41 6.45 -25 17 3 170.40 10.15 -25 17 3 166.75 10.56 25 -17 -3 179.73 9.90 25 -17 -3 186.47 11.06 -25 17 6 62.03 6.31 -25 17 6 65.73 6.12 -25 17 6 55.29 6.49 25 -17 -6 69.91 7.15 -25 17 9 137.87 9.76 -25 17 9 121.06 9.40 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15.88 -22 22 10 344.21 15.50 -22 22 13 106.68 10.29 -22 22 13 102.25 8.33 -22 22 13 104.87 8.78 22 -22 -13 97.28 9.12 -23 21 -14 4.25 3.24 23 -21 14 2.38 4.21 -23 21 -11 -1.12 2.49 23 -21 11 2.19 2.71 -23 21 -8 45.46 5.28 23 -21 8 47.81 6.12 -23 21 -5 31.97 2.64 -23 21 -5 35.89 2.53 -23 21 -5 40.00 5.31 23 -21 5 32.50 5.65 -23 21 -2 13.53 2.34 -23 21 -2 9.02 3.39 23 -21 2 12.49 2.57 -23 21 1 19.62 4.31 -23 21 1 13.99 3.14 23 -21 -1 18.50 3.74 23 -21 -1 13.73 3.50 -23 21 4 0.04 2.77 -23 21 4 2.71 3.28 -23 21 4 0.56 3.58 23 -21 -4 0.19 3.21 -23 21 7 7.05 4.20 -23 21 7 9.76 3.38 -23 21 7 13.71 3.38 23 -21 -7 16.03 4.83 -23 21 10 42.70 5.20 -23 21 10 39.11 5.68 -23 21 13 0.11 3.68 -23 21 13 -0.65 3.35 -23 21 13 -2.76 2.68 23 -21 -13 0.50 4.88 -24 20 -14 75.37 8.42 24 -20 14 78.32 7.38 -24 20 -11 12.64 3.51 24 -20 11 7.02 4.09 -24 20 -8 45.37 5.37 24 -20 8 50.07 6.21 -24 20 -5 73.63 6.48 24 -20 5 75.53 4.03 24 -20 5 79.75 7.59 -24 20 -2 9.57 2.39 -24 20 -2 9.02 4.46 24 -20 2 8.11 2.32 24 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24.74 4.24 -25 19 13 6.31 3.06 -25 19 13 7.42 4.01 -25 19 13 8.27 3.79 25 -19 -13 4.59 3.94 -26 18 -11 76.88 7.55 26 -18 11 96.04 8.09 -26 18 -8 86.66 5.02 -26 18 -8 97.48 8.78 26 -18 8 96.50 8.30 -26 18 -5 14.01 3.41 -26 18 -5 9.17 2.69 26 -18 5 11.00 2.40 26 -18 5 13.78 3.67 -26 18 -2 12.47 4.66 -26 18 -2 9.46 2.81 26 -18 2 11.19 3.42 26 -18 2 8.53 2.69 -26 18 1 28.60 4.28 -26 18 1 24.26 4.24 26 -18 -1 21.68 3.50 26 -18 -1 21.51 4.19 -26 18 4 -2.76 3.53 -26 18 4 4.08 2.87 26 -18 -4 5.46 3.97 26 -18 -4 1.04 3.76 -26 18 7 1.32 3.64 -26 18 7 -1.94 2.69 -26 18 7 0.44 2.76 26 -18 -7 1.86 3.89 -26 18 10 19.94 6.02 -26 18 10 21.80 5.23 -26 18 10 19.89 4.40 26 -18 -10 20.12 6.35 -27 17 -11 15.26 2.37 -27 17 -11 22.89 4.56 27 -17 11 16.16 1.85 27 -17 11 27.07 4.95 -27 17 -8 48.09 5.94 27 -17 8 51.05 7.09 -27 17 -5 41.57 5.28 -27 17 -5 45.47 4.52 27 -17 5 43.62 4.09 27 -17 5 38.07 6.08 -27 17 -2 79.17 6.28 -27 17 -2 90.46 8.42 27 -17 2 98.78 7.79 27 -17 2 79.47 6.15 -27 17 1 351.66 16.36 -27 17 1 333.18 14.61 27 -17 -1 327.97 16.11 27 -17 -1 342.37 15.01 -27 17 4 70.99 7.52 -27 17 4 66.21 7.08 27 -17 -4 70.14 6.83 27 -17 -4 69.64 7.01 -27 17 7 231.88 12.76 -27 17 7 234.94 12.97 27 -17 -7 231.95 13.05 -27 17 10 7.60 3.71 27 -17 -10 9.92 5.59 -28 16 -8 46.32 7.20 -28 16 -8 32.22 4.04 28 -16 8 44.07 5.73 28 -16 8 38.51 3.73 -28 16 -5 3.50 2.95 -28 16 -5 -0.36 2.89 28 -16 5 2.19 2.46 28 -16 5 -0.51 2.83 -28 16 -2 18.79 5.30 -28 16 -2 10.59 3.90 28 -16 2 12.66 3.52 28 -16 2 11.77 3.54 -28 16 1 5.05 3.48 -28 16 1 4.93 3.25 28 -16 -1 2.43 2.82 -28 16 4 5.10 4.35 28 -16 -4 5.84 4.33 28 -16 -4 1.53 4.26 -28 16 7 17.86 4.98 -28 16 7 21.58 4.38 -28 16 10 1.99 4.14 -28 16 10 5.00 3.98 -28 16 10 6.49 5.00 28 -16 -10 1.70 4.56 -29 15 -8 1.92 2.94 -29 15 -8 5.39 4.56 29 -15 8 0.30 4.27 29 -15 8 3.92 2.18 -29 15 -5 67.69 6.94 -29 15 -5 75.03 8.30 29 -15 5 69.67 6.03 -29 15 -2 67.10 6.57 29 -15 2 63.03 7.44 29 -15 2 58.69 5.57 -29 15 1 108.83 8.30 -29 15 1 118.86 9.05 29 -15 -1 112.56 8.35 29 -15 -1 131.62 9.46 -29 15 4 82.81 7.77 -29 15 4 82.25 7.36 29 -15 -4 83.33 7.27 29 -15 -4 86.41 7.60 -29 15 7 73.07 7.51 -29 15 7 93.79 7.98 -29 15 7 96.23 8.01 29 -15 -7 90.29 9.19 -30 14 -5 14.25 4.35 -30 14 -5 13.91 4.16 30 -14 5 18.24 3.74 30 -14 5 14.69 3.82 -30 14 -2 6.32 4.29 -30 14 -2 10.16 3.93 30 -14 2 8.62 3.78 30 -14 2 14.34 4.60 -30 14 1 5.50 2.99 -30 14 1 2.90 3.65 30 -14 -1 4.61 3.21 -30 14 4 11.35 4.47 30 -14 -4 12.33 4.69 -15 30 -3 207.25 9.88 -15 30 -3 203.40 12.28 -15 30 -3 203.13 9.47 -15 30 -3 192.26 10.90 -15 30 0 224.21 10.59 -15 30 0 218.70 12.55 -15 30 0 206.93 13.89 -15 30 0 206.91 10.08 -15 30 3 212.02 10.43 -15 30 3 212.26 10.32 -15 30 3 223.57 15.29 -16 29 -6 93.30 6.79 -16 29 -6 89.25 6.86 -16 29 -6 96.35 6.81 16 -29 6 97.23 6.54 -16 29 -3 26.75 4.46 -16 29 -3 30.98 3.44 -16 29 -3 25.39 4.71 -16 29 -3 25.23 3.15 -16 29 0 52.01 5.36 -16 29 0 46.98 4.79 -16 29 0 56.20 6.31 -16 29 0 44.15 4.23 -16 29 3 8.31 5.02 -16 29 3 0.13 1.86 -16 29 3 3.03 2.03 -16 29 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239.11 13.17 22 -23 -9 240.80 14.58 -22 23 12 49.92 7.70 -22 23 12 56.50 6.43 -22 23 12 59.04 6.55 22 -23 -12 60.86 8.39 -23 22 -12 6.90 3.13 23 -22 12 6.63 3.19 -23 22 -9 9.53 4.01 23 -22 9 11.97 4.51 -23 22 -6 29.17 4.19 23 -22 6 31.43 5.28 -23 22 -3 -4.86 3.50 23 -22 3 -0.40 2.43 -23 22 0 111.25 7.74 -23 22 0 114.74 6.77 23 -22 0 122.70 7.20 23 -22 0 119.80 8.01 -23 22 3 5.94 2.71 -23 22 3 10.78 3.49 23 -22 -3 5.16 3.35 23 -22 -3 7.06 4.34 -23 22 6 26.63 5.20 -23 22 6 34.64 5.11 -23 22 6 34.42 5.22 23 -22 -6 29.80 5.29 -23 22 9 6.17 4.20 -23 22 9 7.04 3.18 23 -22 -9 6.06 5.25 -23 22 12 13.34 4.31 -23 22 12 11.47 3.51 -23 22 12 16.52 3.93 23 -22 -12 21.50 4.89 -24 21 -12 32.85 6.15 24 -21 12 33.96 5.47 -24 21 -9 24.67 5.18 24 -21 9 27.00 5.28 -24 21 -6 7.24 3.83 24 -21 6 4.32 3.15 -24 21 -3 27.95 4.36 24 -21 3 34.40 5.69 -24 21 0 82.92 6.93 -24 21 0 88.59 6.02 24 -21 0 84.23 6.02 24 -21 0 83.89 7.08 -24 21 3 50.33 5.51 -24 21 3 51.93 5.52 24 -21 -3 52.76 6.30 24 -21 -3 58.67 5.77 -24 21 6 24.74 5.53 -24 21 6 15.83 5.13 -24 21 6 23.14 4.23 24 -21 -6 23.54 4.77 -24 21 9 4.56 4.31 -24 21 9 3.49 3.01 24 -21 -9 8.61 4.75 -24 21 12 -3.78 5.09 -24 21 12 0.62 3.54 -24 21 12 0.97 3.37 24 -21 -12 3.63 5.10 -25 20 -12 330.73 16.54 25 -20 12 320.67 15.72 -25 20 -9 332.04 16.61 25 -20 9 331.28 15.74 -25 20 -6 461.93 19.43 25 -20 6 467.30 19.46 25 -20 6 429.65 11.76 -25 20 -3 298.96 14.63 -25 20 -3 315.40 11.50 25 -20 3 300.82 11.26 25 -20 3 312.78 15.16 -25 20 0 333.89 12.88 -25 20 0 345.04 15.59 25 -20 0 352.47 15.39 25 -20 0 341.11 13.93 -25 20 3 327.40 14.48 -25 20 3 337.45 15.86 25 -20 -3 310.73 14.50 25 -20 -3 317.98 14.46 -25 20 6 442.45 18.73 -25 20 6 413.20 18.31 -25 20 6 418.58 17.94 25 -20 -6 372.31 16.98 -25 20 9 376.88 17.65 -25 20 9 376.22 17.20 -25 20 12 179.77 12.79 -25 20 12 152.79 10.04 -25 20 12 154.37 10.91 25 -20 -12 168.03 12.92 -26 19 -12 42.77 5.92 26 -19 12 47.06 5.87 -26 19 -9 142.40 9.79 26 -19 9 120.62 9.46 -26 19 -6 44.60 6.60 26 -19 6 47.19 6.11 26 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209.70 12.62 30 -15 -3 221.02 12.31 30 -15 -3 211.66 12.51 -16 30 -4 7.18 2.06 -16 30 -4 5.68 3.67 -16 30 -4 8.35 3.09 -16 30 -4 6.47 2.62 -16 30 -1 4.60 2.90 -16 30 -1 5.89 2.62 -16 30 -1 2.56 3.28 -16 30 -1 3.57 3.64 -16 30 2 10.27 2.74 -16 30 2 15.26 4.61 -16 30 2 9.86 3.22 -16 30 2 11.62 4.28 -16 30 5 15.80 3.28 -16 30 5 12.54 4.17 -16 30 5 15.99 3.49 -17 29 -7 1.75 2.35 -17 29 -7 4.30 2.98 -17 29 -7 3.25 1.88 17 -29 7 4.56 1.99 -17 29 -4 216.26 10.77 -17 29 -4 235.24 12.39 -17 29 -4 236.85 11.79 17 -29 4 236.56 10.87 -17 29 -1 25.68 5.37 -17 29 -1 25.68 4.56 -17 29 -1 27.70 3.66 -17 29 -1 28.11 3.55 -17 29 2 42.10 4.36 -17 29 2 47.42 5.28 -17 29 2 35.75 5.40 -17 29 2 38.96 4.64 -17 29 5 182.24 14.34 -17 29 5 178.46 10.14 -18 28 -7 27.53 3.38 -18 28 -7 27.53 3.18 -18 28 -7 31.11 4.05 18 -28 7 31.63 4.68 -18 28 -4 7.50 2.65 -18 28 -4 5.13 2.94 -18 28 -4 5.43 2.31 18 -28 4 2.16 3.12 -18 28 -1 4.49 2.30 -18 28 -1 8.61 3.10 -18 28 -1 0.10 4.01 -18 28 -1 8.82 3.03 -18 28 2 69.95 5.50 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276.75 13.00 -26 20 2 281.31 14.21 26 -20 -2 279.42 13.33 26 -20 -2 293.80 14.73 -26 20 5 64.88 6.26 -26 20 5 67.59 6.39 26 -20 -5 71.61 7.21 -26 20 8 43.27 5.48 -26 20 8 30.73 5.69 26 -20 -8 38.32 6.10 -26 20 11 45.78 5.76 -26 20 11 54.34 7.76 -26 20 11 59.23 7.11 26 -20 -11 59.66 7.77 -27 19 -10 11.16 3.95 27 -19 10 12.41 3.93 -27 19 -7 14.24 3.78 27 -19 7 17.79 4.00 -27 19 -4 46.97 6.55 -27 19 -4 42.72 4.19 27 -19 4 38.41 3.75 27 -19 4 53.26 6.61 -27 19 -1 18.64 3.02 -27 19 -1 17.48 4.02 27 -19 1 22.94 4.17 27 -19 1 20.61 3.66 -27 19 2 9.70 3.26 -27 19 2 14.52 4.06 27 -19 -2 15.17 4.17 27 -19 -2 14.52 3.62 -27 19 5 13.43 4.98 -27 19 5 13.61 4.61 27 -19 -5 16.35 4.49 27 -19 -5 18.44 3.92 -27 19 8 27.48 5.47 -27 19 8 26.15 4.33 -27 19 11 267.49 15.33 -27 19 11 267.71 14.21 -27 19 11 251.13 13.90 27 -19 -11 263.22 16.57 -28 18 -7 164.88 11.32 -28 18 -7 132.06 7.80 28 -18 7 150.39 10.54 28 -18 7 136.73 6.83 -28 18 -4 -0.30 1.50 -28 18 -4 0.92 4.19 28 -18 4 -1.26 2.83 28 -18 4 0.69 1.92 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256.65 12.15 -17 30 -2 272.39 12.10 -17 30 1 292.31 15.20 -17 30 1 287.83 15.77 -17 30 1 268.50 12.41 -17 30 1 290.92 12.93 -17 30 4 439.54 17.23 -17 30 4 466.47 23.35 -17 30 4 442.69 17.52 -18 29 -5 2.72 1.93 -18 29 -5 3.05 2.32 -18 29 -5 1.55 2.92 18 -29 5 0.83 2.78 -18 29 -2 -1.72 2.57 -18 29 -2 -1.47 3.01 -18 29 -2 2.69 1.99 -18 29 -2 -0.68 1.77 -18 29 1 3.87 3.34 -18 29 1 5.50 2.70 -18 29 1 -2.04 2.87 -18 29 1 2.83 4.34 -18 29 4 115.96 9.19 -18 29 4 130.36 10.59 -18 29 4 130.57 8.64 -18 29 7 0.43 2.27 -18 29 7 5.61 3.48 -18 29 7 0.65 2.81 -19 28 -8 45.47 5.45 19 -28 8 53.46 5.56 -19 28 -5 24.94 3.63 -19 28 -5 22.24 3.59 -19 28 -5 29.91 3.70 19 -28 5 34.16 4.11 -19 28 -2 27.00 4.48 -19 28 -2 30.40 4.75 -19 28 -2 31.78 4.00 19 -28 2 27.70 4.44 -19 28 1 0.99 2.84 -19 28 1 0.91 2.49 -19 28 1 -2.13 3.07 -19 28 1 1.34 2.79 -19 28 4 35.76 5.38 -19 28 4 36.01 5.58 -19 28 7 59.25 5.83 -19 28 7 55.02 5.43 20 -27 8 114.53 7.78 -20 27 -5 117.21 6.70 -20 27 -5 126.19 8.78 -20 27 -5 117.71 6.20 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276.61 12.52 -22 25 1 301.27 12.57 -22 25 1 308.15 15.39 -22 25 1 292.33 13.69 -22 25 4 405.49 16.81 -22 25 4 424.56 17.63 -22 25 4 408.78 17.07 22 -25 -4 385.19 16.87 -22 25 7 528.05 21.95 -22 25 7 506.56 20.18 -22 25 7 496.93 19.77 22 -25 -7 508.24 21.48 -22 25 10 420.45 20.15 -22 25 10 423.53 18.46 -22 25 10 428.61 18.53 22 -25 -10 435.28 20.61 -23 24 -11 19.56 4.42 23 -24 11 29.24 4.47 -23 24 -8 8.77 4.53 23 -24 8 8.08 4.08 -23 24 -5 13.02 3.49 -23 24 -5 10.85 1.82 -23 24 -5 10.95 1.55 23 -24 5 8.98 3.93 -23 24 -2 10.17 3.01 -23 24 -2 8.64 3.93 -23 24 -2 10.10 2.20 23 -24 2 13.99 3.37 -23 24 1 5.88 1.91 -23 24 1 5.94 2.65 23 -24 -1 5.76 3.06 23 -24 -1 6.58 2.93 -23 24 4 4.23 3.11 -23 24 4 8.86 3.21 -23 24 4 5.54 3.87 23 -24 -4 3.02 3.98 -23 24 7 60.43 6.16 -23 24 7 66.87 6.78 -23 24 7 68.81 6.54 23 -24 -7 62.87 7.70 -23 24 10 50.72 6.46 -23 24 10 45.36 5.87 -23 24 10 48.91 6.95 23 -24 -10 53.30 6.65 -24 23 -11 26.74 5.61 24 -23 11 32.33 4.96 -24 23 -8 30.33 5.50 24 -23 8 27.19 4.59 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22 10 36.76 5.57 -25 22 10 25.66 5.79 25 -22 -10 36.27 7.00 -26 21 -11 89.50 8.06 26 -21 11 84.84 8.28 -26 21 -8 97.06 8.66 26 -21 8 86.22 7.91 -26 21 -5 2.60 2.96 26 -21 5 0.54 2.73 26 -21 5 3.88 1.54 -26 21 -2 29.18 3.51 -26 21 -2 22.98 5.77 26 -21 2 25.04 3.56 26 -21 2 26.55 4.23 -26 21 1 147.60 9.57 -26 21 1 134.29 8.25 26 -21 -1 144.81 9.38 26 -21 -1 152.71 9.04 -26 21 4 2.12 2.23 -26 21 4 3.22 2.53 26 -21 -4 1.88 4.09 26 -21 -4 1.34 2.54 -26 21 7 63.22 7.24 -26 21 7 62.30 6.29 -26 21 7 52.35 6.12 26 -21 -7 58.27 7.16 -26 21 10 35.09 4.86 -26 21 10 30.37 5.04 -26 21 10 28.81 5.14 26 -21 -10 36.79 5.94 -27 20 -8 501.42 21.85 27 -20 8 496.07 20.59 -27 20 -5 242.46 9.45 -27 20 -5 275.34 14.07 27 -20 5 281.05 14.15 -27 20 -2 373.05 14.18 -27 20 -2 403.23 18.58 27 -20 2 401.58 17.44 27 -20 2 378.23 14.38 -27 20 1 174.43 11.00 -27 20 1 174.70 9.70 27 -20 -1 189.70 9.97 27 -20 -1 174.20 10.42 -27 20 4 631.32 23.29 -27 20 4 599.59 24.42 27 -20 -4 672.01 24.99 27 -20 -4 666.08 24.01 -27 20 7 441.53 19.29 -27 20 7 467.10 19.65 -27 20 7 460.39 20.18 27 -20 -7 485.43 21.62 -27 20 10 107.78 9.49 -27 20 10 89.33 8.19 -27 20 10 127.69 9.92 27 -20 -10 113.02 10.45 -28 19 -8 17.01 5.04 -28 19 -8 6.15 1.84 28 -19 8 13.50 5.29 28 -19 8 6.38 1.53 -28 19 -5 32.56 5.77 -28 19 -5 30.31 3.80 28 -19 5 31.95 3.51 28 -19 5 35.87 5.94 -28 19 -2 -3.03 3.92 -28 19 -2 1.06 2.66 28 -19 2 -2.32 2.69 28 -19 2 -0.42 1.65 -28 19 1 9.27 4.70 -28 19 1 9.23 3.63 28 -19 -1 4.91 3.40 28 -19 -1 7.00 3.25 -28 19 4 122.53 9.26 -28 19 4 114.10 8.92 28 -19 -4 129.06 8.88 28 -19 -4 119.50 9.42 -28 19 7 -4.50 4.26 -28 19 7 7.70 4.31 -29 18 -5 46.11 4.78 -29 18 -5 61.46 6.92 29 -18 5 57.95 6.35 29 -18 5 48.19 4.55 -29 18 -2 11.49 5.02 -29 18 -2 10.29 3.66 29 -18 2 16.44 5.01 29 -18 2 12.37 3.35 -29 18 1 33.82 6.20 -29 18 1 33.96 5.44 29 -18 -1 29.01 4.87 29 -18 -1 32.86 5.03 -29 18 4 51.98 5.87 -29 18 4 51.24 6.88 29 -18 -4 55.80 6.07 29 -18 -4 42.84 6.70 -29 18 7 75.62 7.31 -29 18 7 73.13 7.96 -29 18 7 72.55 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27 -21 -3 1.56 3.29 -27 21 6 8.50 3.49 -27 21 6 18.31 3.83 -27 21 6 13.47 3.78 27 -21 -6 17.63 4.86 -27 21 9 108.93 9.74 -27 21 9 102.50 8.17 -27 21 9 99.92 8.11 27 -21 -9 107.86 8.95 -28 20 -6 3.32 3.92 28 -20 6 -2.58 4.26 -28 20 -3 6.66 2.73 -28 20 -3 16.35 4.89 28 -20 3 7.99 2.71 28 -20 3 9.98 4.07 -28 20 0 2.15 4.13 -28 20 0 3.69 2.73 28 -20 0 -0.35 4.13 28 -20 0 5.41 2.87 -28 20 3 119.13 8.72 -28 20 3 120.93 9.80 28 -20 -3 124.21 8.37 28 -20 -3 128.09 9.09 -28 20 6 2.43 2.91 -28 20 6 -1.60 3.02 -28 20 6 1.00 3.70 28 -20 -6 6.49 4.57 -29 19 -6 28.13 3.58 -29 19 -6 26.54 5.14 29 -19 6 31.29 4.74 29 -19 6 24.81 3.23 -29 19 -3 1.02 3.05 -29 19 -3 0.50 2.54 29 -19 3 1.10 2.22 29 -19 3 -1.65 2.96 -29 19 0 36.39 5.14 -29 19 0 38.33 5.89 29 -19 0 40.59 6.35 29 -19 0 33.77 4.56 -29 19 3 14.11 3.74 -29 19 3 12.56 4.24 29 -19 -3 12.14 3.48 29 -19 -3 3.36 4.01 -29 19 6 55.16 6.33 -29 19 6 60.15 6.45 29 -19 -6 54.61 7.29 -30 18 -3 42.09 5.02 -30 18 -3 53.87 6.23 30 -18 3 40.66 4.87 30 -18 3 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199.25 9.56 -22 27 2 307.27 16.50 -22 27 2 305.86 14.04 -22 27 2 292.46 14.38 -22 27 2 310.92 14.52 -22 27 5 181.22 12.52 -22 27 5 191.21 10.91 -22 27 5 176.59 11.15 -22 27 5 187.85 10.77 -22 27 8 193.12 11.68 -22 27 8 207.79 11.92 -23 26 -7 92.31 7.56 23 -26 7 95.78 8.29 -23 26 -4 88.57 8.20 23 -26 4 94.66 7.54 -23 26 -1 12.21 4.55 -23 26 -1 12.33 2.84 -23 26 -1 9.90 3.56 23 -26 1 12.65 4.12 -23 26 2 18.57 4.56 -23 26 2 15.68 3.59 -23 26 2 17.85 3.98 -23 26 2 17.38 4.39 -23 26 5 75.94 7.32 -23 26 5 80.72 6.92 -23 26 5 75.60 6.62 23 -26 -5 81.94 7.73 -23 26 8 218.52 12.59 -23 26 8 200.71 11.94 -24 25 -7 284.32 14.66 24 -25 7 271.85 13.53 -24 25 -4 359.73 16.56 24 -25 4 387.73 16.76 -24 25 -1 48.05 5.50 -24 25 -1 45.25 4.18 -24 25 -1 55.82 5.69 24 -25 1 55.07 6.34 -24 25 2 113.73 7.19 -24 25 2 116.21 8.36 24 -25 -2 112.43 7.47 24 -25 -2 124.14 8.71 -24 25 5 249.49 13.27 -24 25 5 244.85 12.78 -24 25 5 252.13 12.97 -24 25 8 147.45 10.57 -24 25 8 163.96 10.26 24 -25 -8 171.40 11.60 -25 24 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2 -1.45 2.43 26 -24 2 0.64 1.84 -26 24 1 13.16 4.71 -26 24 1 10.75 3.29 26 -24 -1 7.11 3.06 26 -24 -1 8.98 3.54 -26 24 4 49.77 5.32 -26 24 4 40.20 6.29 -26 24 4 53.65 5.89 26 -24 -4 57.98 5.66 -26 24 7 167.61 10.57 -26 24 7 166.67 10.53 -26 24 7 169.15 10.64 26 -24 -7 166.23 11.83 -27 23 -5 163.68 10.85 27 -23 5 146.74 6.35 27 -23 5 172.19 10.59 -27 23 -2 106.75 8.85 -27 23 -2 94.58 5.90 27 -23 2 95.18 6.21 27 -23 2 97.28 8.04 -27 23 1 82.02 6.41 -27 23 1 93.80 8.57 27 -23 -1 86.83 8.08 27 -23 -1 86.69 7.04 -27 23 4 -0.57 2.91 -27 23 4 -1.06 3.20 27 -23 -4 -0.53 3.20 -27 23 7 -0.99 4.09 -27 23 7 0.02 3.17 27 -23 -7 -3.57 2.93 -28 22 -5 14.21 4.72 28 -22 5 20.45 4.48 -28 22 -2 116.52 6.95 -28 22 -2 110.90 9.48 28 -22 2 116.51 7.06 28 -22 2 118.43 9.36 -28 22 1 16.59 3.51 -28 22 1 11.72 5.02 28 -22 -1 14.95 3.84 28 -22 -1 13.30 4.70 -28 22 4 160.38 10.67 -28 22 4 171.19 10.30 28 -22 -4 163.99 10.47 28 -22 -4 189.45 11.06 -29 21 -5 0.76 2.68 -29 21 -5 2.53 1.80 29 -21 5 1.62 1.58 29 -21 5 1.24 3.82 -29 21 -2 22.89 4.60 -29 21 -2 22.72 3.61 29 -21 2 27.44 4.62 29 -21 2 24.30 3.60 -29 21 1 3.45 4.47 -29 21 1 2.50 2.96 29 -21 -1 1.08 3.76 29 -21 -1 -1.41 2.82 -29 21 4 10.44 4.17 -29 21 4 7.76 3.25 29 -21 -4 6.01 4.27 29 -21 -4 6.89 3.18 -30 20 1 187.50 11.12 -30 20 1 194.62 12.09 30 -20 -1 204.66 12.75 30 -20 -1 184.28 11.11 -22 29 -3 95.39 6.22 -22 29 -3 94.98 7.92 -22 29 -3 92.76 7.09 -22 29 0 89.93 6.70 -22 29 0 93.15 7.73 -22 29 0 87.70 7.12 -22 29 0 88.56 7.38 -22 29 3 185.52 13.45 -22 29 3 207.47 11.45 -22 29 3 207.50 12.01 -22 29 3 229.03 12.37 -23 28 -3 -2.31 3.30 -23 28 -3 2.78 2.09 -23 28 -3 2.24 3.37 23 -28 3 8.43 3.71 -23 28 0 130.79 8.02 -23 28 0 140.82 9.27 -23 28 0 130.07 9.68 23 -28 0 138.72 9.17 -23 28 3 43.67 6.69 -23 28 3 48.92 5.83 -23 28 3 45.26 5.38 -23 28 3 39.87 5.34 -24 27 -6 576.13 22.84 24 -27 6 576.25 22.67 -24 27 -3 156.85 7.33 -24 27 -3 150.33 8.30 -24 27 -3 159.28 10.13 24 -27 3 180.20 11.21 -24 27 0 346.58 13.89 -24 27 0 345.22 16.65 -24 27 0 355.46 16.44 24 -27 0 379.24 17.06 -24 27 3 154.73 9.73 -24 27 3 129.42 10.65 -24 27 3 156.32 9.81 -24 27 3 139.93 8.86 -24 27 6 209.93 12.47 -24 27 6 221.64 12.26 -24 27 6 236.10 12.73 24 -27 -6 228.15 13.08 -25 26 -6 15.06 3.75 25 -26 6 16.96 4.80 -25 26 -3 16.17 2.86 -25 26 -3 17.29 4.03 -25 26 -3 15.12 2.28 25 -26 3 13.96 4.88 -25 26 0 33.72 4.99 -25 26 0 47.42 6.21 -25 26 0 40.44 3.87 25 -26 0 55.86 6.37 -25 26 3 4.86 3.73 -25 26 3 3.11 2.77 -25 26 3 5.87 3.02 25 -26 -3 3.44 3.31 -25 26 6 38.75 5.04 -25 26 6 38.62 5.98 -25 26 6 42.21 6.15 25 -26 -6 39.86 6.17 -26 25 -6 34.19 4.91 26 -25 6 37.50 4.98 -26 25 -3 96.47 6.60 -26 25 -3 120.11 9.60 -26 25 -3 109.33 6.15 26 -25 3 118.00 8.64 -26 25 0 6.40 1.91 -26 25 0 11.60 3.78 26 -25 0 11.82 3.74 26 -25 0 11.58 2.95 -26 25 3 147.07 10.25 -26 25 3 133.91 8.51 -26 25 3 148.54 9.45 26 -25 -3 125.33 8.51 -26 25 6 5.70 4.33 -26 25 6 2.03 4.18 -26 25 6 3.36 2.86 26 -25 -6 4.29 2.89 -27 24 -6 16.09 5.22 27 -24 6 13.37 3.60 -27 24 -3 107.95 8.44 -27 24 -3 93.52 5.49 27 -24 3 98.92 5.96 27 -24 3 105.09 8.70 -27 24 0 183.97 12.03 -27 24 0 175.62 9.10 27 -24 0 176.45 9.76 27 -24 0 192.30 11.95 -27 24 3 254.17 14.15 -27 24 3 264.58 13.28 27 -24 -3 274.27 13.87 27 -24 -3 272.44 14.09 -27 24 6 130.19 9.26 -27 24 6 139.96 9.51 -27 24 6 134.67 9.28 27 -24 -6 127.40 9.92 -28 23 -3 70.96 7.98 -28 23 -3 62.41 4.71 28 -23 3 62.32 7.07 28 -23 3 72.34 5.12 -28 23 0 -2.54 3.78 -28 23 0 4.88 2.47 28 -23 0 -1.03 1.80 28 -23 0 -0.97 3.03 -28 23 3 196.47 11.14 -28 23 3 168.95 11.05 28 -23 -3 193.50 10.94 28 -23 -3 183.28 11.80 -29 22 -3 71.29 5.42 -29 22 -3 65.78 6.64 29 -22 3 73.44 8.03 29 -22 3 68.25 5.08 -29 22 0 202.48 10.71 -29 22 0 218.75 13.20 29 -22 0 219.64 11.37 29 -22 0 202.47 12.12 -29 22 3 419.10 18.01 -29 22 3 436.38 19.67 29 -22 -3 432.80 19.42 29 -22 -3 404.02 17.60 -24 28 -1 17.12 4.19 -24 28 -1 25.33 5.21 -24 28 -1 19.09 3.15 24 -28 1 14.32 4.18 -24 28 2 20.23 5.42 -24 28 2 21.73 4.05 -24 28 2 20.76 3.86 -24 28 2 21.16 5.10 -25 27 -4 50.99 5.70 25 -27 4 49.10 6.64 -25 27 -1 47.13 5.70 -25 27 -1 38.63 4.03 -25 27 -1 37.63 4.96 25 -27 1 47.26 6.33 -25 27 2 76.42 6.12 -25 27 2 70.28 6.66 -25 27 2 71.48 7.81 -25 27 2 78.50 6.86 25 -27 -2 74.65 6.18 -26 26 -4 48.71 5.82 26 -26 4 54.33 5.95 -26 26 -1 12.71 3.61 -26 26 -1 7.79 3.78 26 -26 1 11.50 3.57 -26 26 2 8.67 3.00 -26 26 2 11.16 3.06 26 -26 -2 12.48 4.93 26 -26 -2 5.47 3.74 -26 26 5 4.38 3.17 -26 26 5 4.58 4.09 26 -26 -5 7.80 4.23 -27 25 -4 88.13 8.28 27 -25 4 76.76 7.87 -27 25 -1 143.36 9.80 -27 25 -1 126.88 7.17 27 -25 1 146.14 9.77 27 -25 1 139.34 7.57 -27 25 2 2.32 3.03 -27 25 2 4.59 2.89 27 -25 -2 6.88 3.07 27 -25 -2 2.52 3.37 -28 24 -1 3.59 2.28 -28 24 -1 6.45 3.93 28 -24 1 0.98 2.75 28 -24 1 -1.03 2.32 -28 24 2 34.40 4.98 -28 24 2 40.93 4.75 28 -24 -2 43.52 5.39 28 -24 -2 41.06 6.17 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 41417