data_exp_135_auto _audit_creation_date 2023-06-09 _audit_creation_method ; Olex2 1.5-ac5-024 (compiled 2022.04.12 svn.rca3783a0 for Rigaku Oxford Diffraction, GUI svn.r6498) ; _shelx_SHELXL_version_number '2018/1' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C16 H20 I Si, C F3 O3 S' _chemical_formula_sum 'C17 H20 F3 I O3 S Si' _chemical_formula_weight 516.38 _chemical_melting_point ? _chemical_oxdiff_formula 'C17 H20 I O3 S F3 Si' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.3257 6.8362 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 61 _space_group_name_H-M_alt 'P b c a' _space_group_name_Hall '-P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 13.8862(9) _cell_length_b 12.7268(9) _cell_length_c 23.2752(13) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4113.4(5) _cell_formula_units_Z 8 _cell_measurement_reflns_used 8630 _cell_measurement_temperature 93.15 _cell_measurement_theta_max 77.9860 _cell_measurement_theta_min 3.8370 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 14.117 _exptl_absorpt_correction_T_max 0.707 _exptl_absorpt_correction_T_min 0.249 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.74a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.668 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 2048 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -8 3 3 0.0369 3 8 1 0.0556 8 -3 -4 0.0163 -3 -8 -1 0.0540 0 1 15 0.0296 2 4 13 0.0335 -8 3 4 0.0401 -2 -1 -15 0.0069 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.054 _exptl_crystal_size_min 0.042 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -8.1857 2.9023 3.4957 0.0051 -0.1063 0.9943 2.7126 7.8304 1.4979 -0.0791 0.9786 0.1901 8.1480 -2.9850 -3.5087 -0.0042 0.0955 -0.9954 -3.4586 -7.5974 -1.1888 0.0799 -0.9916 -0.1013 -0.1310 1.3801 14.9031 0.9068 0.2688 0.3247 1.6867 4.0381 12.8716 0.7333 0.6269 0.2632 -7.8820 3.4625 3.7327 0.0095 -0.0293 0.9995 -2.0111 -1.3918 -14.5101 -0.9171 -0.3819 -0.1147 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0345 _diffrn_reflns_av_unetI/netI 0.0304 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 14890 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 68.209 _diffrn_reflns_theta_min 3.798 _diffrn_ambient_temperature 93.15 _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -153.00-125.00 0.50 3.82 -- -106.00 -40.00 -3.00 56 2 \w -121.00 -96.00 0.50 3.82 -- -106.00 -40.00 -3.00 50 3 \w 46.00 102.00 0.50 3.82 -- 111.50-107.00 138.00 112 4 \w 70.00 138.00 0.50 3.82 -- 111.50 -87.00-133.00 136 5 \w -21.00 4.00 0.50 0.96 -- -48.39 38.00 -30.00 50 6 \w -23.00 31.00 0.50 0.96 -- 48.39 -40.00 -3.00 108 7 \w 47.00 74.00 0.50 0.96 -- 48.39-125.00-180.00 54 8 \w -15.00 20.00 0.50 0.96 -- 48.39 -19.00 120.00 70 9 \w -24.00 21.00 0.50 0.96 -- 48.39 -19.00-150.00 90 10 \w -67.00 -42.00 0.50 3.82 -- -106.00 57.00 0.00 50 11 \w -169.00 -95.00 0.50 3.82 -- -106.00 -38.00 -30.00 148 12 \w -67.00 -36.00 0.50 3.82 -- -106.00 57.00 -60.00 62 13 \w -62.00 -37.00 0.50 3.82 -- -106.00 57.00-180.00 50 14 \w 40.00 65.00 0.50 3.82 -- 111.50 -57.00-150.00 50 15 \w 40.00 66.00 0.50 3.82 -- 111.50 -57.00 60.00 52 16 \w 40.00 65.00 0.50 3.82 -- 111.50 -57.00 -30.00 50 17 \w 40.00 65.00 0.50 3.82 -- 111.50 -57.00 -90.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0166035000 _diffrn_orient_matrix_UB_12 -0.0280210000 _diffrn_orient_matrix_UB_13 0.0635881000 _diffrn_orient_matrix_UB_21 0.0538520000 _diffrn_orient_matrix_UB_22 0.1046292000 _diffrn_orient_matrix_UB_23 0.0088194000 _diffrn_orient_matrix_UB_31 -0.0954242000 _diffrn_orient_matrix_UB_32 0.0542824000 _diffrn_orient_matrix_UB_33 0.0159235000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3465 _reflns_number_total 3766 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.42.74a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.74a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.74a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/1 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _refine_diff_density_max 1.070 _refine_diff_density_min -0.506 _refine_diff_density_rms 0.087 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 239 _refine_ls_number_reflns 3766 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0312 _refine_ls_R_factor_gt 0.0283 _refine_ls_restrained_S_all 1.053 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0348P)^2^+4.9556P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0706 _refine_ls_wR_factor_ref 0.0721 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C6(H6), C12(H12), C4(H4), C9(H9), C3(H3), C13(H13), C11(H11), C10(H10) 2.b Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C15(H15A,H15B,H15C), C16(H16A,H16B,H16C), C17(H17A,H17B, H17C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I7 I 0.69196(2) 0.59406(2) 0.49576(2) 0.02081(8) Uani 1 1 d . . . . . S19 S 0.52359(5) 0.39462(5) 0.60074(3) 0.02374(16) Uani 1 1 d . . . . . Si14 Si 0.90100(6) 0.44778(6) 0.69938(3) 0.02272(17) Uani 1 1 d . . . . . F23 F 0.67589(14) 0.27296(17) 0.61030(8) 0.0421(5) Uani 1 1 d . . . . . O25 O 0.45530(15) 0.43185(17) 0.64181(9) 0.0297(5) Uani 1 1 d . . . . . F21 F 0.64171(17) 0.3581(2) 0.68604(9) 0.0603(7) Uani 1 1 d . . . . . O26 O 0.48439(17) 0.3228(2) 0.55883(10) 0.0451(6) Uani 1 1 d . . . . . F22 F 0.55565(17) 0.2274(2) 0.66194(13) 0.0681(8) Uani 1 1 d . . . . . O24 O 0.58682(18) 0.4717(2) 0.57779(13) 0.0542(8) Uani 1 1 d . . . . . C1 C 0.80645(18) 0.5066(2) 0.53141(12) 0.0180(5) Uani 1 1 d . . . . . C5 C 0.88395(19) 0.4497(2) 0.61878(12) 0.0209(6) Uani 1 1 d . . . . . C8 C 0.7734(2) 0.6933(2) 0.44083(12) 0.0212(6) Uani 1 1 d . . . . . C2 C 0.8634(2) 0.4431(2) 0.49633(11) 0.0200(6) Uani 1 1 d . . . . . C6 C 0.81504(19) 0.5116(2) 0.59113(12) 0.0200(6) Uani 1 1 d . . . . . H6 H 0.774374 0.556774 0.612764 0.024 Uiso 1 1 calc R U . . . C12 C 0.8926(2) 0.8251(2) 0.42876(13) 0.0238(6) Uani 1 1 d . . . . . H12 H 0.939214 0.871839 0.444196 0.029 Uiso 1 1 calc R U . . . C4 C 0.9413(2) 0.3856(2) 0.58402(13) 0.0249(6) Uani 1 1 d . . . . . H4 H 0.988464 0.342427 0.601781 0.030 Uiso 1 1 calc R U . . . C9 C 0.7567(2) 0.6868(2) 0.38229(12) 0.0251(6) Uani 1 1 d . . . . . H9 H 0.710537 0.639418 0.366916 0.030 Uiso 1 1 calc R U . . . C3 C 0.9322(2) 0.3824(2) 0.52507(13) 0.0245(6) Uani 1 1 d . . . . . H3 H 0.973658 0.337952 0.503489 0.029 Uiso 1 1 calc R U . . . C13 C 0.8399(2) 0.7606(2) 0.46539(13) 0.0230(6) Uani 1 1 d . . . . . H13 H 0.849321 0.762761 0.505805 0.028 Uiso 1 1 calc R U . . . C18 C 0.8553(2) 0.4386(2) 0.43202(12) 0.0232(6) Uani 1 1 d . . . . . H18A H 0.787395 0.431829 0.421129 0.035 Uiso 1 1 calc R U . . . H18B H 0.891321 0.377871 0.417573 0.035 Uiso 1 1 calc R U . . . H18C H 0.881838 0.503126 0.415389 0.035 Uiso 1 1 calc R U . . . C11 C 0.8776(2) 0.8217(2) 0.37002(13) 0.0250(6) Uani 1 1 d . . . . . H11 H 0.913378 0.866599 0.345389 0.030 Uiso 1 1 calc R U . . . C15 C 0.8896(2) 0.3082(3) 0.72361(14) 0.0330(7) Uani 1 1 d . . . . . H15A H 0.826038 0.281162 0.712910 0.049 Uiso 1 1 calc R U . . . H15B H 0.897222 0.304747 0.765423 0.049 Uiso 1 1 calc R U . . . H15C H 0.939668 0.265653 0.705179 0.049 Uiso 1 1 calc R U . . . C20 C 0.6031(2) 0.3096(2) 0.64192(13) 0.0276(6) Uani 1 1 d . . . . . C10 C 0.8103(2) 0.7527(2) 0.34697(13) 0.0282(7) Uani 1 1 d . . . . . H10 H 0.800884 0.750558 0.306564 0.034 Uiso 1 1 calc R U . . . C16 C 0.8080(2) 0.5320(3) 0.73417(14) 0.0313(7) Uani 1 1 d . . . . . H16A H 0.817843 0.605297 0.722756 0.047 Uiso 1 1 calc R U . . . H16B H 0.813487 0.525930 0.776023 0.047 Uiso 1 1 calc R U . . . H16C H 0.743816 0.508931 0.722047 0.047 Uiso 1 1 calc R U . . . C17 C 1.0242(2) 0.4979(3) 0.71563(14) 0.0328(7) Uani 1 1 d . . . . . H17A H 1.072239 0.450963 0.698560 0.049 Uiso 1 1 calc R U . . . H17B H 1.033478 0.500609 0.757346 0.049 Uiso 1 1 calc R U . . . H17C H 1.031637 0.568632 0.699528 0.049 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I7 0.02264(13) 0.02079(13) 0.01898(11) 0.00482(6) -0.00122(6) 0.00100(6) S19 0.0246(3) 0.0261(4) 0.0205(3) 0.0024(3) 0.0001(3) 0.0043(3) Si14 0.0265(4) 0.0246(4) 0.0170(4) 0.0014(3) -0.0022(3) 0.0000(3) F23 0.0407(10) 0.0534(13) 0.0323(10) -0.0061(9) -0.0027(8) 0.0238(9) O25 0.0298(11) 0.0322(11) 0.0270(11) -0.0043(9) 0.0024(9) 0.0070(9) F21 0.0610(14) 0.0794(17) 0.0405(12) -0.0274(12) -0.0250(10) 0.0355(13) O26 0.0411(13) 0.0545(16) 0.0395(13) -0.0235(12) -0.0166(11) 0.0203(12) F22 0.0587(15) 0.0469(14) 0.099(2) 0.0424(14) 0.0061(13) 0.0077(11) O24 0.0390(13) 0.0534(16) 0.0703(19) 0.0362(15) 0.0144(13) 0.0043(12) C1 0.0176(13) 0.0150(13) 0.0213(14) 0.0036(11) -0.0031(10) -0.0007(10) C5 0.0226(13) 0.0200(14) 0.0201(13) 0.0014(11) -0.0003(11) -0.0010(11) C8 0.0247(14) 0.0173(13) 0.0216(13) 0.0068(11) 0.0021(11) 0.0013(11) C2 0.0207(14) 0.0195(14) 0.0197(14) 0.0000(10) -0.0001(10) -0.0058(12) C6 0.0223(13) 0.0170(14) 0.0207(14) 0.0014(11) 0.0003(10) -0.0012(10) C12 0.0208(13) 0.0204(14) 0.0302(15) 0.0001(12) 0.0000(11) 0.0019(11) C4 0.0241(14) 0.0253(15) 0.0252(15) 0.0006(12) -0.0023(12) 0.0034(12) C9 0.0322(15) 0.0203(14) 0.0227(14) 0.0022(11) -0.0025(12) -0.0019(12) C3 0.0232(14) 0.0234(14) 0.0268(15) -0.0022(12) 0.0007(11) 0.0019(11) C13 0.0269(14) 0.0180(14) 0.0240(14) -0.0012(11) -0.0038(11) 0.0019(11) C18 0.0263(14) 0.0237(14) 0.0196(14) -0.0020(11) -0.0002(11) -0.0020(12) C11 0.0258(14) 0.0177(14) 0.0315(15) 0.0075(12) 0.0044(12) 0.0024(11) C15 0.0411(17) 0.0311(16) 0.0267(15) 0.0060(13) -0.0011(13) 0.0003(14) C20 0.0312(15) 0.0262(16) 0.0255(15) -0.0017(12) -0.0016(12) 0.0014(13) C10 0.0374(17) 0.0245(16) 0.0226(15) 0.0036(12) 0.0009(12) 0.0031(13) C16 0.0351(17) 0.0353(18) 0.0235(15) -0.0024(13) 0.0010(12) 0.0010(13) C17 0.0323(15) 0.0414(19) 0.0248(15) 0.0066(13) -0.0060(13) -0.0041(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I7 C1 2.111(3) . ? I7 C8 2.123(3) . ? S19 O25 1.427(2) . ? S19 O26 1.444(2) . ? S19 O24 1.421(3) . ? S19 C20 1.819(3) . ? Si14 C5 1.891(3) . ? Si14 C15 1.870(3) . ? Si14 C16 1.863(3) . ? Si14 C17 1.865(3) . ? F23 C20 1.334(4) . ? F21 C20 1.313(4) . ? F22 C20 1.321(4) . ? C1 C2 1.395(4) . ? C1 C6 1.397(4) . ? C5 C6 1.397(4) . ? C5 C4 1.398(4) . ? C8 C9 1.385(4) . ? C8 C13 1.384(4) . ? C2 C3 1.399(4) . ? C2 C18 1.502(4) . ? C12 C13 1.391(4) . ? C12 C11 1.384(4) . ? C4 C3 1.378(4) . ? C9 C10 1.391(4) . ? C11 C10 1.389(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 I7 C8 98.59(10) . . ? O25 S19 O26 114.35(14) . . ? O25 S19 C20 104.35(13) . . ? O26 S19 C20 102.00(14) . . ? O24 S19 O25 115.65(16) . . ? O24 S19 O26 114.62(19) . . ? O24 S19 C20 103.54(15) . . ? C15 Si14 C5 107.50(13) . . ? C16 Si14 C5 109.70(14) . . ? C16 Si14 C15 110.89(15) . . ? C16 Si14 C17 110.54(15) . . ? C17 Si14 C5 108.16(13) . . ? C17 Si14 C15 109.96(15) . . ? C2 C1 I7 120.2(2) . . ? C2 C1 C6 124.1(2) . . ? C6 C1 I7 115.55(19) . . ? C6 C5 Si14 123.4(2) . . ? C6 C5 C4 116.9(3) . . ? C4 C5 Si14 119.7(2) . . ? C9 C8 I7 117.9(2) . . ? C13 C8 I7 118.4(2) . . ? C13 C8 C9 123.7(3) . . ? C1 C2 C3 115.3(2) . . ? C1 C2 C18 124.2(3) . . ? C3 C2 C18 120.5(3) . . ? C1 C6 C5 119.4(3) . . ? C11 C12 C13 120.5(3) . . ? C3 C4 C5 122.8(3) . . ? C8 C9 C10 117.1(3) . . ? C4 C3 C2 121.4(3) . . ? C8 C13 C12 117.6(3) . . ? C12 C11 C10 120.2(3) . . ? F23 C20 S19 112.1(2) . . ? F21 C20 S19 112.3(2) . . ? F21 C20 F23 106.6(3) . . ? F21 C20 F22 107.5(3) . . ? F22 C20 S19 110.8(2) . . ? F22 C20 F23 107.2(3) . . ? C11 C10 C9 120.9(3) . . ? _shelx_res_file ; TITL exp_135_auto_a.res in Pbca exp_135_auto.res created by SHELXL-2018/1 at 14:14:32 on 09-Jun-2023 REM Old TITL exp_135_auto in Pbca REM SHELXT solution in Pbca REM R1 0.075, Rweak 0.002, Alpha 0.042, Orientation as input REM Formula found by SHELXT: C17 O24 F22 Si S I CELL 1.54184 13.8862 12.7268 23.2752 90 90 90 ZERR 8 0.0009 0.0009 0.0013 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H F I O S Si UNIT 136 160 24 8 24 8 8 L.S. 4 PLAN 5 TEMP -180 fmap 2 ACTA REM REM REM WGHT 0.034800 4.955600 FVAR 1.49823 I7 4 0.691955 0.594061 0.495763 11.00000 0.02264 0.02079 = 0.01898 0.00482 -0.00122 0.00100 S19 6 0.523592 0.394617 0.600738 11.00000 0.02464 0.02607 = 0.02051 0.00235 0.00010 0.00432 SI14 7 0.900997 0.447783 0.699382 11.00000 0.02652 0.02461 = 0.01703 0.00141 -0.00217 -0.00004 F23 3 0.675885 0.272962 0.610301 11.00000 0.04070 0.05341 = 0.03229 -0.00614 -0.00267 0.02377 O25 5 0.455303 0.431850 0.641811 11.00000 0.02985 0.03222 = 0.02697 -0.00435 0.00236 0.00696 F21 3 0.641706 0.358135 0.686043 11.00000 0.06100 0.07938 = 0.04054 -0.02738 -0.02496 0.03547 O26 5 0.484386 0.322759 0.558832 11.00000 0.04109 0.05453 = 0.03955 -0.02355 -0.01661 0.02033 F22 3 0.555651 0.227408 0.661942 11.00000 0.05874 0.04688 = 0.09872 0.04236 0.00610 0.00773 O24 5 0.586817 0.471736 0.577794 11.00000 0.03899 0.05336 = 0.07030 0.03619 0.01438 0.00432 C1 1 0.806454 0.506585 0.531410 11.00000 0.01760 0.01503 = 0.02133 0.00362 -0.00305 -0.00072 C5 1 0.883949 0.449700 0.618779 11.00000 0.02260 0.02000 = 0.02007 0.00142 -0.00035 -0.00103 C8 1 0.773367 0.693314 0.440831 11.00000 0.02469 0.01734 = 0.02155 0.00682 0.00214 0.00133 C2 1 0.863424 0.443069 0.496327 11.00000 0.02069 0.01946 = 0.01971 0.00000 -0.00012 -0.00581 C6 1 0.815042 0.511626 0.591135 11.00000 0.02228 0.01704 = 0.02065 0.00140 0.00028 -0.00122 AFIX 43 H6 2 0.774374 0.556774 0.612764 11.00000 -1.20000 AFIX 0 C12 1 0.892576 0.825088 0.428761 11.00000 0.02083 0.02041 = 0.03022 0.00011 -0.00002 0.00193 AFIX 43 H12 2 0.939214 0.871839 0.444196 11.00000 -1.20000 AFIX 0 C4 1 0.941266 0.385608 0.584018 11.00000 0.02414 0.02530 = 0.02522 0.00057 -0.00234 0.00339 AFIX 43 H4 2 0.988464 0.342427 0.601781 11.00000 -1.20000 AFIX 0 C9 1 0.756665 0.686830 0.382294 11.00000 0.03222 0.02031 = 0.02271 0.00220 -0.00247 -0.00193 AFIX 43 H9 2 0.710537 0.639418 0.366916 11.00000 -1.20000 AFIX 0 C3 1 0.932247 0.382366 0.525071 11.00000 0.02324 0.02340 = 0.02677 -0.00218 0.00072 0.00188 AFIX 43 H3 2 0.973658 0.337952 0.503489 11.00000 -1.20000 AFIX 0 C13 1 0.839933 0.760645 0.465392 11.00000 0.02691 0.01802 = 0.02398 -0.00117 -0.00376 0.00192 AFIX 43 H13 2 0.849321 0.762761 0.505805 11.00000 -1.20000 AFIX 0 C18 1 0.855288 0.438584 0.432015 11.00000 0.02629 0.02374 = 0.01958 -0.00204 -0.00025 -0.00205 AFIX 137 H18A 2 0.787395 0.431829 0.421129 11.00000 -1.50000 H18B 2 0.891321 0.377871 0.417573 11.00000 -1.50000 H18C 2 0.881838 0.503126 0.415389 11.00000 -1.50000 AFIX 0 C11 1 0.877589 0.821678 0.370020 11.00000 0.02584 0.01768 = 0.03153 0.00748 0.00441 0.00242 AFIX 43 H11 2 0.913378 0.866599 0.345389 11.00000 -1.20000 AFIX 0 C15 1 0.889628 0.308231 0.723606 11.00000 0.04107 0.03114 = 0.02670 0.00599 -0.00107 0.00025 AFIX 137 H15A 2 0.826038 0.281162 0.712910 11.00000 -1.50000 H15B 2 0.897222 0.304747 0.765423 11.00000 -1.50000 H15C 2 0.939668 0.265653 0.705179 11.00000 -1.50000 AFIX 0 C20 1 0.603089 0.309571 0.641918 11.00000 0.03116 0.02617 = 0.02549 -0.00169 -0.00159 0.00145 C10 1 0.810338 0.752729 0.346971 11.00000 0.03743 0.02452 = 0.02255 0.00358 0.00094 0.00306 AFIX 43 H10 2 0.800884 0.750558 0.306564 11.00000 -1.20000 AFIX 0 C16 1 0.808019 0.531959 0.734174 11.00000 0.03514 0.03530 = 0.02350 -0.00242 0.00105 0.00098 AFIX 137 H16A 2 0.817843 0.605297 0.722756 11.00000 -1.50000 H16B 2 0.813487 0.525930 0.776023 11.00000 -1.50000 H16C 2 0.743816 0.508931 0.722047 11.00000 -1.50000 AFIX 0 C17 1 1.024203 0.497947 0.715631 11.00000 0.03234 0.04139 = 0.02482 0.00663 -0.00596 -0.00406 AFIX 137 H17A 2 1.072239 0.450963 0.698560 11.00000 -1.50000 H17B 2 1.033478 0.500609 0.757346 11.00000 -1.50000 H17C 2 1.031637 0.568632 0.699528 11.00000 -1.50000 AFIX 0 HKLF 4 REM exp_135_auto_a.res in Pbca REM R1 = 0.0283 for 3465 Fo > 4sig(Fo) and 0.0312 for all 3766 data REM 239 parameters refined using 0 restraints END WGHT 0.0348 4.9556 REM Highest difference peak 1.070, deepest hole -0.506, 1-sigma level 0.087 Q1 1 0.6930 0.5934 0.4572 11.00000 0.05 1.07 Q2 1 0.6920 0.5947 0.5371 11.00000 0.05 0.90 Q3 1 0.7519 0.5826 0.4950 11.00000 0.05 0.75 Q4 1 0.6460 0.6419 0.5021 11.00000 0.05 0.71 Q5 1 0.7421 0.6306 0.5007 11.00000 0.05 0.67 ; _shelx_res_checksum 83422 _shelx_hkl_file ; 0 0 -2 556942. 21910.7 8 0 0 -3 82.0467 106.681 8 0 0 -4 61053.6 2445.86 8 0 0 -5 79.9755 179.836 8 0 0 -6 118914. 4741.02 8 0 0 -7 142.765 202.370 8 0 0 -8 226599. 8990.61 8 0 0 -9 87.5599 192.553 8 0 0 -10 422932. 16723.6 8 0 0 -11-34.6354 195.503 8 0 0 -12 104357. 4221.17 8 0 0 -13 161.642 202.011 8 0 0 14 168110. 6824.93 6 0 0 15-147.276 269.561 6 0 0 16 88796.1 3579.44 4 0 0 16 93988.8 3785.18 6 0 0 17 83.5775 265.176 6 0 0 18 68920.5 2983.56 6 0 0 19-151.586 299.754 6 0 0 20 110674. 4651.16 6 0 0 21 97.7811 288.735 6 0 0 22 32257.9 1568.09 6 0 0 -23 10.2192 129.964 2 0 0 24 11008.0 510.786 16 0 0 -24 11324.3 497.738 2 0 0 25 57.2925 129.663 16 0 0 -25-73.0727 110.038 2 0 0 26 31971.6 1313.52 16 0 0 -26 32903.6 1310.67 2 0 0 -27 83.6383 80.5323 2 0 0 -28 21744.3 876.010 2 0 -1 0 23.0184 25.8090 9 0 1 1 15.0845 48.1744 6 0 1 2 102.911 84.3370 6 0 1 3 102.773 49.7557 7 0 1 3 4.32048 116.073 6 0 1 4 54.1485 160.538 6 0 1 5 182.247 207.579 6 0 1 6-145.073 204.412 6 0 1 -7 81.1181 187.132 8 0 1 7 324.390 219.641 6 0 1 -8-45.8915 184.909 8 0 1 8 144.009 226.636 6 0 1 -9 10.2941 193.285 8 0 1 9 259.227 228.474 6 0 1 -10-103.176 196.554 8 0 1 10-61.5848 249.125 6 0 1 -11 25.1020 202.247 8 0 1 11 102.120 261.923 6 0 1 -12-13.5420 203.023 8 0 1 12 296.589 270.736 6 0 1 -13 86.8641 207.146 8 0 1 13-20.2134 253.216 6 0 1 -14 61.8563 201.065 8 0 1 14-21.9487 254.170 6 0 1 -15 229.706 216.495 8 0 1 15-70.2522 255.614 6 0 1 -16 17.4295 215.851 8 0 1 16-150.302 257.389 6 0 1 17-163.382 285.470 6 0 -1 17-175.352 284.730 6 0 1 18-263.353 305.745 6 0 -1 18-31.0999 324.946 6 0 -1 19-191.505 282.738 6 0 1 19 396.799 302.847 6 0 1 20-156.243 310.117 6 0 -1 20-224.900 309.470 6 0 1 -21-54.8710 132.559 2 0 -1 21-225.526 293.069 6 0 1 21 157.157 269.419 6 0 1 22-6.78741 162.486 16 0 1 -22 5.36599 133.420 2 0 -1 22-355.912 348.900 6 0 1 22-459.157 295.920 6 0 1 -23 10.1253 129.336 2 0 1 23-18.9151 158.144 16 0 1 -24-91.9774 125.680 2 0 -1 -24-91.8919 121.107 2 0 1 24 198.050 152.032 16 0 1 -25-24.0050 107.616 2 0 -1 -25 56.1105 110.896 2 0 -1 25 144.074 130.020 16 0 1 25 57.6339 132.513 16 0 -1 -26 50.3084 93.0118 2 0 1 -26 73.6929 95.1084 2 0 1 26 102.276 116.505 16 0 -1 26-85.3972 112.289 16 0 -1 -27-26.7678 78.2616 2 0 1 -27-48.3697 76.2033 2 0 -2 0 91656.7 3622.35 9 0 -2 -1 194122. 7588.08 9 0 -2 -1 191079. 7586.68 5 0 2 2 32155.9 1303.61 6 0 2 3 85332.8 3403.21 6 0 2 4 173423. 6954.74 7 0 2 4 182673. 6988.70 6 0 2 5 1089.76 197.765 6 0 2 5 847.672 90.1211 7 0 2 6 1522.57 216.854 6 0 2 7 2093.68 253.528 6 0 2 8 22714.0 1025.65 6 0 2 -9 851.294 227.332 8 0 2 9 864.851 234.928 6 0 2 10 141367. 6111.40 6 0 2 -10 162075. 6103.72 8 0 2 11 94341.1 3994.16 6 0 2 -11 100405. 3972.45 8 0 2 12 28286.5 1350.94 6 0 2 -12 30925.8 1326.83 8 0 2 13 25141.8 1251.98 6 0 2 -13 28441.9 1226.94 8 0 2 14 38120.9 1749.01 6 0 2 -14 39575.5 1702.76 8 0 2 15 5368.32 468.459 6 0 2 -15 6373.12 432.886 8 0 2 16 7533.49 553.199 6 0 2 -16 7732.59 501.278 8 0 2 -17 9684.00 588.222 8 0 2 17 10467.3 667.348 6 0 2 18 808.001 309.361 6 0 2 -18 630.540 133.146 2 0 -2 19 2143.55 386.094 6 0 2 19 1692.37 348.624 6 0 2 -19 1963.33 170.495 2 0 2 20 15744.8 931.027 6 0 -2 20 17169.7 982.243 6 0 2 20 16693.1 740.591 16 0 2 -20 17029.4 720.806 2 0 -2 21 39785.4 1957.75 6 0 2 21 39704.4 1932.27 6 0 2 21 44244.3 1736.41 16 0 2 -21 41812.4 1717.22 2 0 -2 22 6465.07 565.796 6 0 2 22 5835.88 538.264 6 0 2 -22 7666.79 349.162 2 0 2 22 6602.96 369.135 16 0 2 -23 39348.5 1580.77 2 0 2 23 38404.7 1594.09 16 0 2 -24 11307.3 472.224 2 0 2 24 9639.21 481.524 16 0 2 -25 8974.62 406.185 2 0 -2 -25 8638.55 404.932 2 0 2 25 9951.85 424.014 16 0 2 -26 2953.08 163.309 2 0 -2 -26 2887.42 162.346 2 0 2 26 2294.99 172.829 16 0 -2 26 2422.89 165.155 16 0 2 -27 7206.04 318.449 11 0 -2 -27 6933.76 310.011 2 0 -3 0-19.2977 82.3049 9 0 -3 -1 35.1203 62.5512 5 0 -3 -1 6.29437 77.6353 9 0 -3 -2-3.18978 62.4510 5 0 -3 -2 142.573 86.2927 9 0 3 3 186.902 140.935 6 0 3 4 35.0175 147.048 6 0 3 5-65.4163 161.243 6 0 3 6 96.0087 88.7019 7 0 3 6 105.364 179.296 6 0 3 7 142.664 193.166 6 0 3 8 265.540 214.106 6 0 3 9 87.1791 229.929 6 0 3 -10-13.9976 221.170 8 0 3 10 95.2675 245.810 6 0 3 -11-30.6655 222.037 8 0 3 11 17.3222 242.164 6 0 3 -12-33.1297 222.971 8 0 3 12-57.1544 236.482 6 0 3 -13-89.3059 230.267 8 0 3 13 230.227 256.162 6 0 3 -14 76.5523 237.558 8 0 3 -14 44.0997 108.665 2 0 3 14 22.8601 244.220 6 0 3 -15 81.1608 242.368 8 0 3 -15 135.835 116.530 2 0 3 15-123.116 277.472 6 0 3 16-33.1103 150.274 16 0 3 -16 188.318 253.082 8 0 3 -16 267.344 120.515 2 0 3 16 26.1258 283.481 6 0 3 17 109.218 160.080 16 0 3 -17 21.6741 245.589 8 0 3 -17 5.01677 115.260 2 0 3 17-164.962 287.218 6 0 3 18 236.472 164.100 16 0 3 -18 21.4015 247.862 8 0 3 -18 41.2692 123.062 2 0 3 18 142.129 269.512 6 0 3 19 56.2345 164.843 16 0 3 -19-194.967 245.463 8 0 3 19 116.941 268.214 6 0 3 -19-5.25670 123.114 2 0 3 -20 79.2114 126.939 2 0 -3 20 239.291 325.361 6 0 3 20 117.385 264.631 6 0 3 20-111.932 161.812 16 0 3 -21 5.20419 124.864 2 0 -3 21-337.715 307.194 6 0 3 21 201.021 252.052 6 0 3 21-61.4269 164.362 16 0 3 -22-15.0406 125.120 2 0 3 22-27.6381 232.257 6 0 -3 22-221.100 270.738 6 0 3 22-26.1693 161.197 16 0 3 23-18.3190 152.202 16 0 3 -23 9.38177 123.069 2 0 3 24 159.037 144.830 16 0 3 -24 158.194 117.451 2 0 3 25-14.0089 129.847 16 0 3 -25 3.75256 101.814 2 0 3 -25 54.9967 111.313 11 0 3 -26 3.74886 99.2170 11 0 -3 26-32.4616 94.7091 16 0 -3 -26 34.2083 87.1889 2 0 3 -27 38.7181 74.5172 1 0 3 -27 66.4704 82.5679 11 0 -3 -27 12.2892 72.2213 2 0 -4 0 31367.2 1276.69 9 0 -4 -1 3646.04 195.667 5 0 -4 -1 3901.52 203.001 9 0 -4 -2 218067. 8751.09 5 0 -4 -2 225635. 8754.69 9 0 -4 -3 5108.41 259.950 9 0 -4 -4 83026.2 3364.75 9 0 4 4 86120.5 3393.76 6 0 4 5 30523.4 1295.41 6 0 4 6 84833.0 3492.60 7 0 4 6 93109.9 3546.94 6 0 4 7 8429.53 393.853 7 0 4 7 9170.87 477.064 6 0 4 8 86031.7 3509.13 6 0 4 9 1126.88 245.555 6 0 4 10 132879. 5383.36 6 0 4 11 29537.8 1412.14 6 0 4 -11 33496.3 1415.66 8 0 4 12 94175.4 4085.03 6 0 4 -12 104560. 4087.82 8 0 4 -13 10337.8 465.318 2 0 4 13 11046.8 639.743 6 0 4 -13 11846.5 631.748 8 0 4 -14 34177.4 1407.49 2 0 4 14 35094.1 1588.03 6 0 4 -14 36772.7 1572.52 8 0 4 15 24983.6 1055.03 16 0 4 -15 24895.8 1031.90 2 0 4 15 23778.2 1213.37 6 0 4 -15 26272.2 1205.69 8 0 4 16 64962.4 2745.11 16 0 4 -16 69803.5 2728.29 2 0 4 16 68400.8 2929.36 6 0 4 -16 71081.3 2901.97 8 0 4 17 24700.0 962.959 16 0 4 -17 20796.8 927.652 2 0 4 17 21761.4 1134.27 6 0 4 -17 22777.3 1104.60 8 0 4 -18 30829.4 1508.25 8 0 4 18 33366.5 1368.76 16 0 4 -18 32599.2 1344.34 2 0 4 18 34791.4 1573.86 6 0 4 19 771.815 298.964 6 0 4 -19 1317.13 286.241 8 0 4 -19 1282.94 147.077 2 0 4 19 907.203 189.613 16 0 4 20 38107.9 1729.20 6 0 4 20 36976.9 1526.35 16 0 4 -20 32926.0 1647.26 8 0 4 -20 37768.8 1505.67 2 0 4 21 16155.8 926.914 6 0 -4 21 16390.8 986.175 6 0 4 -21 16300.7 732.016 2 0 4 21 19265.9 764.806 16 0 4 -22 38862.9 1543.39 2 0 4 22 36821.3 1558.41 16 0 4 -23 2205.52 192.768 11 0 4 23 2826.87 214.065 16 0 4 -24 5041.62 267.769 11 0 4 -25 12735.7 550.038 11 0 4 -26 2522.32 158.519 11 0 4 -26 2713.99 153.702 1 0 4 -27 8533.70 359.088 11 0 4 -27 8515.14 356.393 1 0 -4 -27 8079.23 355.269 2 0 -5 0 29.6768 97.2083 9 0 -5 -1 45.1131 91.9811 9 0 -5 -1-22.1418 73.4738 5 0 -5 -2-69.1844 91.3592 9 0 -5 -2 5.34614 71.1108 5 0 -5 -3 90.8222 101.695 9 0 -5 -4 81.0242 104.109 9 0 -5 -5 7.43850 110.611 9 0 5 6 98.0690 192.307 6 0 -5 -6 16.5246 117.812 9 0 5 7 148.431 208.004 6 0 5 7 94.8928 106.323 7 0 5 8 43.7996 211.424 6 0 5 8-5.84754 80.9991 7 0 5 9-15.9414 211.168 6 0 5 10-17.5958 221.919 6 0 5 11 38.9047 236.373 6 0 5 -11 37.2294 96.3609 2 0 5 -12-19.8189 243.725 8 0 5 12 20.7374 229.707 6 0 5 -12-84.9088 100.810 2 0 5 -13-211.665 246.410 8 0 5 13-44.2219 247.035 6 0 5 -13 65.3901 108.221 2 0 5 14 7.00863 161.349 16 0 5 -14-44.4369 269.328 8 0 5 14-212.807 264.178 6 0 5 -14 9.34259 109.975 2 0 5 15 87.8722 169.594 16 0 5 -15-279.397 268.181 8 0 5 15-25.2460 269.702 6 0 5 -15 24.9301 121.756 2 0 5 16-60.7065 175.450 16 0 5 -16 312.821 271.176 8 0 5 16-345.393 286.514 6 0 5 -16-159.455 133.312 2 0 5 17 231.555 184.395 16 0 5 -17-159.637 131.520 2 0 5 -17-73.9510 267.433 8 0 5 17-221.983 279.269 6 0 5 18 224.019 184.414 16 0 5 -18 27.3303 132.999 2 0 5 -18-128.534 147.558 11 0 5 -18-193.530 262.441 8 0 5 18-84.8945 274.585 6 0 5 19 159.492 184.484 16 0 5 -19-134.606 129.372 2 0 5 -19 106.765 153.125 11 0 5 -19-399.835 271.650 8 0 5 19-312.220 304.181 6 0 5 -20-12.9766 146.804 11 0 5 20 27.8076 239.548 6 0 5 -20-489.474 272.986 8 0 5 20-117.589 174.299 16 0 5 21 111.309 171.513 16 0 5 -21 18.5612 142.354 11 0 5 -22 34.4563 141.409 11 0 5 -23-25.9685 126.679 11 0 5 -24 101.313 106.519 1 0 5 -24 27.0435 113.912 11 0 5 -25 68.7530 90.9163 1 0 5 -25-26.0976 98.4244 11 0 5 -26 23.3956 73.6885 1 0 5 -26 63.4548 80.0712 11 0 -6 0 166717. 6623.86 5 0 -6 -1 2957.47 199.373 9 0 -6 -1 2435.37 170.095 5 0 -6 -2 150994. 5672.13 9 0 -6 -2 135809. 5656.48 5 0 -6 -3 4338.74 253.392 9 0 -6 -4 84771.1 3407.34 9 0 -6 -5 2667.30 203.648 9 0 -6 -6 263702. 10452.9 9 0 -6 -7 514.749 140.115 9 0 6 7 705.377 136.477 7 0 -6 -8 174092. 6368.64 9 0 6 8 149875. 6328.01 7 0 -6 -9 4175.75 279.287 9 0 6 9 3552.21 333.886 6 0 -6 -10 156815. 5979.56 9 0 6 10 154999. 6038.15 6 0 6 -10 144460. 5881.78 1 0 6 -10 149993. 5891.36 11 0 6 -11 1439.67 145.150 11 0 6 11 1038.27 269.565 6 0 6 -12 111473. 4530.11 8 0 6 12 111314. 4544.34 6 0 6 -12 109390. 4373.88 11 0 6 12 109792. 4391.82 16 0 6 -13 57615.3 2392.60 8 0 6 13 58032.0 2403.22 6 0 6 -13 55641.8 2220.72 11 0 6 13 52598.5 2236.13 16 0 6 -14 43141.2 1845.25 8 0 6 14 39450.7 1835.56 6 0 6 -14 41125.2 1668.07 11 0 6 14 40113.4 1684.42 16 0 6 15 6711.53 514.636 6 0 6 -15 6364.75 341.261 11 0 6 15 6899.16 375.061 16 0 6 -16 34813.6 1640.34 8 0 6 16 36341.2 1487.62 16 0 6 -16 35611.7 1468.30 11 0 6 16 33697.0 1648.45 6 0 6 -17 1350.00 307.510 8 0 6 -17 1114.90 181.006 11 0 6 17 1183.10 219.327 16 0 6 17 915.735 308.029 6 0 6 -18 50500.8 2053.13 11 0 6 -18 48698.4 2211.06 8 0 6 18 52258.4 2259.09 6 0 6 -19 541.669 158.227 11 0 6 -19 695.921 256.615 8 0 6 19 619.407 265.806 6 0 6 20 80685.9 3491.16 6 0 6 -20 85736.5 3296.83 1 0 6 -20 79316.1 3303.77 11 0 6 -21 928.772 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195.117 8 -4 -5 0 2051.26 214.781 5 -4 -5 0 2049.24 203.642 9 -4 5 1 252.221 127.243 8 -4 5 -1 65.9713 164.935 8 -4 -5 1 208.772 148.054 5 -4 -5 -1 278.082 143.649 5 -4 -5 -1 417.773 145.248 9 -4 -5 1 186.230 139.852 9 -4 -5 -2 25420.9 1109.35 9 -4 -5 2 27389.3 1148.03 5 -4 5 -2 25401.8 1101.86 8 -4 5 2 24555.6 1045.52 8 -4 5 2 27740.8 1164.78 7 -4 -5 -3 2892.03 237.431 9 -4 -5 3 2699.19 250.792 5 -4 5 3 2814.67 273.311 7 -4 5 -3 3032.72 264.643 8 -4 5 4 15702.7 751.675 7 -4 -5 -4 15734.6 722.284 9 -4 5 -4 14591.2 725.867 8 -4 5 5 264.134 170.439 7 -4 5 -5 329.540 203.814 8 -4 -5 -5 404.625 161.084 9 -4 5 6 3127.86 270.798 7 -4 5 -6 3468.30 311.739 8 -4 -5 -6 3423.58 277.364 9 -4 5 7 385.190 159.744 7 -4 5 -7 343.989 207.891 8 -4 -5 -7 184.986 164.328 9 -4 5 -8 306.628 226.521 8 -4 -5 -8 430.129 182.714 9 -4 -5 -9 1732.21 240.979 9 -4 5 -9 1834.44 283.194 8 4 5 -9 1782.67 150.308 11 -4 5 9 2233.03 242.462 6 4 5 9 1725.17 241.955 6 -4 -5 -10 1499.06 240.857 9 -4 5 10 1143.09 214.237 6 4 5 10 1472.44 246.547 6 -4 5 -10 1037.15 260.066 8 4 5 -10 1705.54 150.975 11 -4 5 -11 10824.2 631.602 8 4 5 11 10853.5 624.948 6 -4 5 11 10434.9 591.163 6 4 5 -11 10961.2 491.873 11 4 5 -12 23318.9 983.349 11 -4 5 -12 22973.5 957.612 11 -4 5 12 23753.4 990.259 16 -4 5 12 23487.2 1098.55 6 4 5 12 23576.5 1126.32 6 -4 5 -12 24256.1 1132.16 8 4 5 -13 10650.4 479.480 11 -4 5 -13 9864.56 442.125 11 -4 5 13 10930.5 596.186 6 4 5 13 9823.77 617.125 6 -4 5 13 9243.90 444.893 4 -4 5 -13 10184.0 619.133 8 -4 -5 13 11133.3 485.389 17 -4 5 14 2451.05 306.909 6 4 5 14 2063.38 331.350 6 -4 5 14 2333.76 166.570 4 4 5 -14 2705.24 218.612 11 -4 5 -14 2697.64 171.864 11 -4 5 -14 3205.21 362.882 8 -4 -5 14 2733.23 224.293 17 4 5 -15 1133.59 247.724 8 4 5 -15 1085.82 183.492 11 -4 5 -15 1100.88 128.492 11 -4 5 15 1033.22 124.333 4 -4 -5 15 1059.26 132.170 4 -4 -5 15 1277.15 185.737 17 -4 5 15 955.266 245.644 6 4 5 15 1257.73 293.992 6 4 5 -16 4670.40 286.784 11 -4 5 -16 4121.42 228.130 11 -4 5 16 3928.04 232.068 4 -4 -5 16 4187.89 240.694 4 -4 -5 16 4117.93 268.754 17 -4 5 16 3799.28 385.310 6 4 5 -16 3892.05 361.004 8 4 5 16 4197.54 422.737 6 -4 5 -17 2205.79 166.919 11 4 5 -17 3089.96 241.246 11 -4 -5 17 1922.92 169.956 4 -4 5 17 2178.03 170.283 4 -4 -5 17 2684.25 214.304 17 -4 5 17 2872.91 248.867 16 4 5 -17 2161.49 289.944 8 -4 5 17 2489.83 315.400 6 4 5 17 2113.50 335.531 6 -4 5 18 5496.15 294.659 4 -4 -5 18 5093.37 292.467 4 4 5 18 5651.90 481.186 6 -4 5 18 5387.28 439.249 6 4 5 -18 6354.31 343.621 11 -4 5 -18 5538.51 279.008 11 -4 5 18 6714.41 352.030 16 4 5 -18 4590.58 394.097 8 -4 -5 -19 24212.2 1279.21 9 -4 5 19 28044.0 1147.10 16 -4 5 19 25626.7 1275.41 6 4 5 19 26962.4 1311.62 6 4 5 -19 29319.8 1143.04 11 -4 5 -19 25893.3 1102.69 11 4 5 -20 1759.68 155.143 1 4 5 -20 1704.68 191.767 11 -4 5 -20 1311.32 126.530 11 -4 5 20 1722.71 225.190 16 4 5 -21 40402.1 1667.36 11 -4 5 21 41581.3 1681.24 16 -4 5 -21 40624.4 1646.30 1 4 5 -21 40868.8 1648.59 1 -4 5 -22 1930.15 138.264 1 4 5 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-6 -7 6626.36 410.191 9 -4 6 7 6754.58 404.764 7 -4 6 -7 6723.87 435.331 8 4 6 -7 6201.72 305.099 11 -4 6 -8 5432.54 397.006 8 -4 6 -8 5133.87 243.256 1 4 6 -8 4970.03 243.875 1 4 6 -8 5222.16 265.329 11 -4 -6 -8 5910.82 384.445 9 -4 6 -9 3222.13 337.037 8 -4 -6 -9 3122.04 303.278 9 -4 6 -9 3305.44 176.093 1 4 6 -9 3184.79 179.453 1 4 6 -9 3455.91 207.161 11 -4 6 10 2823.63 222.585 16 -4 6 -10 2473.14 328.125 8 -4 -6 -10 3316.37 312.973 9 -4 6 -10 2770.71 162.851 1 4 6 -10 2764.94 166.756 1 -4 6 -10 2588.73 163.630 11 4 6 -10 2778.74 196.827 11 -4 6 11 11626.4 503.044 16 -4 6 -11 10803.0 624.334 8 -4 -6 -11 12308.3 644.155 9 -4 6 -11 9708.42 448.206 1 4 6 -11 10014.8 455.518 1 -4 6 -11 10055.7 450.823 11 4 6 -11 11009.7 482.775 11 -4 6 12 7100.22 382.940 16 -4 6 -12 7254.45 511.010 8 -4 -6 -12 7293.36 509.758 9 -4 6 -12 7042.23 331.354 1 4 6 -12 7197.67 341.136 1 -4 6 -12 7230.28 334.406 11 4 6 -12 7402.06 370.899 11 -4 -6 -13 1093.19 256.961 9 -4 6 -13 949.470 116.528 1 4 6 -13 1178.68 134.796 1 -4 6 -13 891.058 283.091 8 -4 6 -13 775.029 114.879 11 4 6 -13 517.945 167.259 11 -4 -6 13 778.387 178.783 17 -4 -6 -14 100.656 207.231 9 -4 6 -14 162.499 103.764 1 4 6 -14 117.616 118.112 1 -4 6 -14-23.6338 263.361 8 -4 -6 14 234.315 166.778 17 -4 6 -14 111.923 101.631 11 4 6 -14 319.376 160.907 11 -4 -6 15 838.963 180.991 17 -4 -6 -15 859.194 245.925 9 -4 6 -15 1243.35 128.270 1 4 6 -15 1218.44 144.216 1 -4 6 15 741.981 106.138 4 -4 6 -15 1419.23 291.308 8 4 6 -15 1084.32 272.288 8 -4 6 -15 845.836 122.807 11 4 6 -15 1200.89 192.909 11 -4 -6 16 686.593 170.591 17 -4 -6 -16 611.227 240.443 9 -4 6 -16 405.859 117.176 1 4 6 -16 795.178 138.658 1 -4 6 16 398.566 98.8060 4 -4 6 -16 487.744 111.314 11 4 6 -16 609.204 181.232 11 4 6 -16 392.310 241.506 8 -4 6 -16 121.269 252.475 8 -4 -6 -17 1379.86 282.091 9 4 6 -17 1780.62 281.812 8 -4 6 17 1929.80 238.443 16 -4 6 -17 1474.26 140.388 11 4 6 -17 1570.39 209.574 11 -4 6 -17 1983.73 154.035 1 4 6 -17 2071.04 167.826 1 -4 -6 17 1721.00 185.647 17 -4 6 -18 500.688 118.091 1 4 6 -18 652.155 132.739 1 4 6 -18 262.049 220.944 8 -4 -6 -18 332.923 213.991 9 -4 6 -18 499.780 105.900 11 4 6 -18 723.733 189.174 11 -4 6 18 491.357 198.979 16 -4 6 19 4650.29 303.274 16 -4 6 -19 3892.92 218.167 11 4 6 -19 4451.73 282.819 11 -4 6 -19 4167.79 229.660 1 4 6 -19 4592.09 247.126 1 4 6 -20 277.235 160.644 11 -4 6 20 639.765 199.384 16 -4 6 -20 640.040 114.888 1 4 6 -20 587.886 122.022 1 4 6 -21 1508.76 175.083 11 4 6 -21 1653.32 141.260 1 -4 6 -21 1712.50 134.653 1 -4 6 -22 4290.96 208.247 1 4 6 -22 3965.21 208.852 1 4 6 -22 3665.79 234.103 11 -4 6 -23 34.1095 80.7438 1 4 6 -23 61.6415 80.9120 1 4 6 -23-26.3670 115.480 11 -4 6 -24 550.553 77.0339 1 4 6 -24 538.418 79.6770 1 4 6 -24 368.175 104.854 11 -4 7 0 108288. 4369.94 13 -4 -7 0 109595. 4461.62 9 -4 -7 0 118311. 4515.58 5 -4 7 -1 15147.5 639.989 13 -4 7 1 14472.7 635.537 13 -4 -7 -1 14913.1 728.830 9 -4 -7 1 15783.5 770.288 5 -4 7 2 53168.0 2173.63 7 4 7 -2 48801.4 1999.09 11 -4 -7 2 53446.9 2157.84 5 -4 7 2 49698.3 2005.07 13 -4 7 -2 47835.2 2076.73 8 -4 -7 -2 52041.5 2106.80 9 -4 -7 -3 1511.76 220.560 9 -4 7 -3 1179.08 213.138 8 -4 7 3 1842.92 269.375 7 4 7 -3 1541.45 136.023 11 4 7 3 1434.75 137.402 11 -4 -7 3 1828.27 232.006 5 -4 7 3 1420.55 136.587 13 -4 7 4 97593.0 3901.24 7 4 7 -4 92314.7 3743.67 11 -4 -7 4 106287. 3932.57 5 4 7 4 94092.5 3744.98 11 -4 -7 -4 98134.9 3861.03 9 -4 7 -4 90860.7 3837.58 8 -4 7 4 93264.8 3749.60 13 -4 7 5 2099.66 267.118 7 4 7 -5 2401.47 169.195 11 -4 -7 5 2470.04 279.510 5 -4 7 -5 2142.51 269.403 8 4 7 5 2418.03 171.598 11 -4 -7 -5 2583.76 258.372 9 4 7 -6 61398.2 2490.93 11 -4 7 -6 61854.3 2476.65 1 4 7 -6 61863.5 2477.41 1 -4 -7 -6 68333.0 2622.89 9 -4 7 -6 60177.5 2601.69 8 -4 7 6 65993.9 2632.72 7 -4 7 7 3766.46 327.851 7 -4 7 -7 3924.63 212.621 1 4 7 -7 4194.37 216.155 1 -4 7 -7 4336.93 360.682 8 -4 -7 -7 4409.00 349.397 9 4 7 -7 4480.48 239.564 11 -4 7 -8 70452.0 2989.10 8 -4 7 8 73444.2 2973.09 7 -4 7 -8 70822.9 2844.67 11 4 7 -8 70177.3 2859.52 11 -4 7 -8 72717.0 2844.54 1 4 7 -8 70630.8 2844.44 1 -4 -7 -8 76149.2 2999.49 9 -4 -7 -9 3595.80 322.542 9 -4 7 9 2685.99 190.344 3 -4 7 -9 3253.07 343.638 8 4 7 -9 3876.59 221.284 11 -4 7 -9 3863.60 190.022 11 -4 7 -9 2927.53 176.659 1 4 7 -9 2874.89 182.296 1 -4 7 -10 96393.2 3858.56 1 4 7 -10 97957.1 3862.19 1 4 7 -10 98429.4 3880.84 11 -4 7 -10 95043.6 3859.40 11 -4 -7 -10 108412. 4049.74 9 -4 7 -10 95412.1 4019.40 8 4 7 -11 1653.65 148.299 1 -4 7 -11 1319.34 134.121 1 4 7 -11 2302.52 188.774 11 -4 7 -11 1813.46 143.085 11 -4 -7 -11 1875.58 292.070 9 -4 7 -11 1934.75 313.532 8 -4 7 -12 46028.8 1832.17 1 4 7 -12 46624.7 1839.35 1 4 7 -12 47437.1 1862.41 11 -4 7 -12 42815.2 1831.76 11 -4 7 -12 43716.9 2008.01 8 -4 -7 -12 48856.8 2035.56 9 -4 -7 -13 7523.00 520.567 9 -4 7 -13 6681.95 347.691 1 4 7 -13 6793.90 358.176 1 -4 7 -13 7964.31 355.541 11 4 7 -13 8644.82 399.487 11 -4 7 -13 7316.53 528.642 8 -4 -7 13 9073.52 399.576 17 -4 -7 -14 29897.3 1423.59 9 -4 7 -14 31520.7 1236.69 1 4 7 -14 31595.6 1245.28 1 -4 7 -14 29028.1 1234.83 11 4 7 -14 30551.4 1269.20 11 -4 7 -14 29465.6 1418.97 8 -4 -7 14 28686.3 1257.77 17 -4 7 -15 1760.99 152.837 1 4 7 -15 1543.16 167.460 1 -4 7 -15 2336.11 157.656 11 4 7 -15 2596.10 222.888 11 4 7 -15 1829.49 314.061 8 -4 7 -15 1936.32 336.188 8 -4 -7 -15 2054.78 298.894 9 -4 7 -16 45310.9 1731.54 1 4 7 -16 44227.7 1737.66 1 -4 7 -16 40954.4 1725.85 11 4 7 -16 43305.2 1764.17 11 4 7 -16 38839.2 1891.43 8 -4 -7 -16 42190.8 1920.65 9 -4 7 -16 38791.5 1892.66 8 -4 7 -17 6243.59 300.309 1 4 7 -17 6291.46 312.893 1 -4 7 -17 5925.96 294.300 11 4 7 -17 7064.70 362.215 11 4 7 -17 5627.13 451.869 8 -4 7 -17 5325.32 457.469 8 -4 -7 -17 5313.11 450.978 9 -4 7 -18 49509.4 2016.85 1 4 7 -18 50372.3 2024.82 1 4 7 -18 51347.5 2054.87 11 -4 7 -19 7775.19 377.761 1 4 7 -19 8270.64 390.886 1 -4 7 -20 51354.7 2048.78 1 4 7 -20 51876.1 2053.69 1 4 7 -20 49822.8 2073.48 11 -4 7 -21 1852.11 138.187 1 4 7 -21 1967.25 146.684 1 -4 7 -22 27283.4 1097.90 1 4 7 -22 27752.6 1099.46 1 4 7 -22 26123.5 1114.92 11 -4 7 -23 6337.77 274.188 1 4 7 -23 6119.67 274.533 1 -4 -7 23 5524.25 274.276 10 4 7 -24 9910.41 397.709 11 -4 7 -24 10324.5 380.856 1 4 7 -24 10494.5 381.806 1 -4 8 0 15231.2 653.725 11 4 8 0 14996.0 662.054 11 -4 -8 0 14299.4 793.258 5 -4 8 0 16943.7 678.716 15 -4 8 1 4967.38 260.985 13 -4 -8 1 5254.91 388.242 5 -4 8 1 4666.58 247.566 11 4 8 -1 4697.52 253.870 11 4 8 1 4758.11 257.213 11 -4 8 -1 4779.48 244.909 11 -4 8 2 3093.52 345.725 7 -4 8 -2 3022.73 271.594 8 -4 8 2 2893.82 191.768 13 -4 8 -2 2362.81 167.683 11 4 8 2 2814.73 190.490 11 -4 -8 -2 3265.87 286.068 9 -4 -8 2 3254.27 316.376 5 4 8 -2 2887.13 186.204 11 -4 -8 3 1184.47 227.699 5 4 8 -3 726.734 127.369 11 4 8 3 850.857 131.642 11 -4 8 -3 823.158 109.183 11 -4 -8 -3 742.898 198.451 9 -4 8 3 750.284 126.948 13 -4 8 -3 648.789 199.518 8 -4 8 3 939.888 250.450 7 -4 -8 -4 89.4818 161.665 9 -4 8 -4 339.307 148.597 15 -4 -8 4 50.0553 180.853 5 4 8 -4 339.580 116.994 11 4 8 4 317.944 123.473 11 -4 8 -4 257.672 95.2985 11 -4 8 -4 178.568 198.438 8 -4 8 4 47.2118 210.264 7 -4 8 5 178.811 202.434 7 4 8 -5-73.8854 113.199 11 -4 -8 5 26.0664 174.736 5 4 8 5 106.995 120.899 11 -4 8 -5 15.9678 93.2499 11 -4 -8 -5 18.5285 173.550 9 -4 8 -5-50.9852 149.165 15 -4 8 -5-156.018 208.084 8 -4 8 6 150.093 189.951 7 4 8 -6 92.4873 119.500 11 -4 -8 6 27.3724 189.249 5 -4 8 -6 16.2613 94.5108 11 -4 8 -6 238.556 215.326 8 -4 8 -6 128.546 160.323 15 -4 -8 -6 57.5711 172.312 9 -4 8 7 257.464 177.152 7 -4 -8 7 287.766 202.000 5 -4 -8 -7 237.452 179.349 9 -4 8 -7 79.2285 104.643 11 -4 8 -7-58.2914 224.514 8 -4 8 -7 141.936 171.459 15 4 8 -7 357.471 130.722 11 -4 8 -8 471.574 105.185 11 -4 -8 -8 825.979 226.559 9 -4 8 -8 655.686 245.218 8 -4 8 -8 646.854 104.951 1 4 8 -8 522.789 104.927 1 -4 -8 8 609.169 226.914 5 4 8 -8 697.098 148.951 11 -4 8 8 639.612 185.371 7 -4 8 -9 2995.03 192.694 11 4 8 -9 3555.94 228.750 11 -4 8 9 2886.14 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183.923 9 -4 8 -15-4.47726 96.8510 11 4 8 -15-45.9364 171.076 11 -4 8 -15 65.4301 110.027 1 4 8 -15 43.3968 128.689 1 -4 8 -15 189.022 242.765 8 4 8 -15-250.092 291.145 8 -4 8 -16-89.0434 98.6109 11 4 8 -16 196.487 165.218 11 -4 8 -16 55.5187 109.702 1 4 8 -16-31.7086 126.963 1 4 8 -16-262.662 247.820 8 -4 8 -16-389.361 264.524 8 -4 8 -17 88.1172 104.932 1 4 8 -17 45.3692 123.479 1 4 8 -17-59.3062 175.985 11 4 8 -18 122.703 121.577 1 -4 8 -18 110.413 105.205 1 4 8 -18 142.920 168.189 11 -4 8 -19 1137.78 120.596 1 4 8 -19 1310.27 138.393 1 4 8 -19 1267.87 181.718 11 -4 -8 19 979.707 113.936 10 -4 8 -20 1206.88 111.142 1 4 8 -20 1282.61 120.672 1 4 8 -20 1053.20 157.869 11 -4 -8 20 834.296 95.8706 10 4 8 -21 1654.08 153.701 11 -4 8 -21 1875.59 121.234 1 4 8 -21 1622.24 121.594 1 4 8 -22-11.3292 103.791 11 -4 8 -22-11.3887 68.5833 1 -4 9 0 98237.8 3914.29 11 4 9 0 98604.8 3924.03 11 -4 9 1 4073.38 256.708 15 -4 9 1 3093.10 374.121 7 -4 9 -1 3428.03 217.297 11 4 9 -1 3562.22 233.808 11 4 9 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649.209 11 -5 7 -4 15834.9 751.159 8 5 7 -5 44820.6 1817.97 11 -5 7 -5 43979.4 1919.72 8 -5 -7 -5 44786.5 1940.90 9 -5 -7 5 46651.9 2007.00 5 -5 7 5 46476.1 1973.88 7 -5 7 6 4195.24 341.497 7 -5 -7 6 3528.50 350.307 5 -5 7 -6 3711.78 333.537 8 5 7 -6 3484.59 217.506 11 -5 7 6 4409.22 231.585 3 -5 7 -6 3729.60 221.532 3 -5 -7 6 3585.42 204.144 10 -5 -7 -6 4432.42 340.460 9 -5 7 -7 12010.1 509.813 1 5 7 -7 11318.1 510.579 1 5 7 -7 13524.4 536.904 11 -5 -7 7 13228.8 730.551 5 -5 7 7 11994.2 651.780 7 -5 7 -7 13084.9 666.202 8 -5 7 7 12469.3 534.070 3 -5 7 -7 11522.7 530.111 3 -5 -7 7 11511.4 521.914 10 -5 -7 -7 12482.5 661.284 9 -5 -7 -8 1324.67 229.593 9 -5 7 -8 690.916 99.4206 1 5 7 -8 637.990 101.150 1 -5 -7 8 583.741 212.668 5 -5 7 -8 671.937 121.561 3 -5 7 8 680.059 124.463 3 -5 -7 8 784.849 106.645 10 5 7 -8 1030.68 140.049 11 -5 7 -8 1025.22 253.214 8 -5 7 9 48841.2 2088.51 3 5 7 -9 55750.1 2104.61 11 -5 -7 -9 55287.4 2257.28 9 -5 7 -9 52419.2 2078.70 1 5 7 -9 50663.7 2079.73 1 -5 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129.427 181.883 16 -6 -6 15 210.441 194.805 17 6 6 -16 12256.2 559.321 11 -6 -6 -16 11226.5 703.689 9 -6 6 16 11371.4 524.660 4 -6 6 -16 11950.3 514.486 1 6 6 -16 11705.2 521.706 1 -6 6 16 12575.3 572.433 16 -6 -6 16 13685.1 578.404 17 -6 -6 17 656.608 190.694 17 6 6 -17 1098.53 124.637 1 -6 6 -17 1117.59 109.500 1 -6 -6 17 1238.28 265.225 5 6 6 -17 821.492 171.052 11 -6 6 17 760.460 110.098 4 -6 6 17 1005.84 199.828 16 -6 -6 -17 1070.07 253.174 9 6 6 -18 21179.4 858.805 1 -6 6 -18 20774.9 852.281 1 -6 -6 18 20417.3 889.352 17 -6 6 18 19737.8 897.417 16 6 6 -18 21169.3 891.069 11 -6 6 -19 592.012 88.5816 1 6 6 -19 613.397 105.657 1 6 6 -19 646.651 158.704 11 -6 6 19 874.310 190.345 16 6 6 -20 9049.83 433.076 11 6 6 -20 9519.33 406.130 1 6 6 -21 2318.15 176.031 11 6 6 -21 2253.55 134.168 1 6 6 -22 4803.24 247.609 11 6 6 -23 1038.02 110.308 11 -6 -6 23 947.967 89.6093 10 -6 7 0 49722.5 1973.09 13 6 7 0 48483.5 1964.50 11 -6 7 0 47053.7 1980.44 3 -6 7 0 50121.5 1978.69 15 -6 -7 1 1099.68 226.306 5 -6 -7 -1 730.435 211.218 9 -6 7 -1 883.245 154.154 15 -6 7 -1 566.775 135.889 3 -6 7 1 787.894 121.106 13 -6 7 -1 814.674 127.898 13 6 7 -1 778.393 120.393 11 6 7 1 571.404 118.722 11 -6 7 -1 675.445 263.775 7 -6 -7 2 51123.8 2063.52 5 -6 7 2 45271.8 1843.72 13 -6 7 -2 46833.6 1850.05 13 -6 7 -2 45635.2 1854.93 15 -6 7 2 47751.4 2040.13 7 -6 7 -2 48989.7 2071.93 7 -6 -7 -2 45174.1 1964.30 9 6 7 -2 45721.9 1838.65 11 6 7 2 45908.2 1839.29 11 -6 7 -2 42331.2 1849.27 3 -6 -7 3-81.4764 86.2320 10 -6 -7 3 133.750 207.059 5 -6 -7 -3 18.6446 184.980 9 6 7 -3 65.4712 109.243 11 6 7 3-51.1265 116.976 11 -6 7 -3 100.008 152.268 15 -6 7 -3-167.526 255.069 7 -6 7 3 25.0164 210.221 7 -6 7 -3-5.90634 131.601 3 -6 7 3 6.03254 133.249 3 -6 7 3-41.9941 112.769 13 6 7 4 127637. 5064.81 11 -6 -7 4 136430. 5281.83 5 -6 7 -4 130072. 5085.82 15 -6 7 4 128257. 5070.76 15 -6 7 -4 122882. 5138.81 8 -6 7 -4 130662. 5297.71 7 -6 7 4 134860. 5255.01 7 -6 -7 4 122757. 5066.80 10 -6 -7 -4 131655. 5204.28 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9216.61 407.496 1 -6 -7 9 10460.3 654.882 5 6 7 -9 10617.0 448.005 11 -6 7 -9 8656.55 604.076 7 -6 7 -9 8671.85 422.380 3 -6 7 9 8665.08 423.786 3 -6 -7 9 9873.28 436.043 10 -6 -7 -9 10287.2 586.486 9 -6 7 -10 38518.3 1836.13 8 -6 7 -10 39438.5 1899.32 7 -6 7 -10 43523.9 1696.58 1 -6 -7 10 44073.2 1979.73 5 6 7 -10 43751.5 1726.99 11 -6 7 10 40866.6 1704.00 3 -6 -7 10 42199.1 1726.33 10 -6 -7 -10 42223.5 1887.12 9 -6 -7 -11 1845.07 292.236 9 -6 7 -11 1736.82 289.554 8 -6 7 -11 2243.35 143.470 1 6 7 -11 2241.64 151.854 1 6 7 -11 2012.44 192.722 11 -6 -7 11 1950.12 171.267 10 -6 -7 11 1933.33 330.319 5 -6 7 -11 1743.99 298.137 7 -6 7 -12 22396.2 887.043 1 6 7 -12 21548.7 890.998 1 -6 -7 12 20851.6 1152.37 5 -6 7 -12 19073.8 1038.21 8 -6 -7 -12 21268.5 1086.20 9 6 7 -12 21783.7 922.279 11 -6 7 -12 18943.7 1060.71 7 -6 7 -13 128.213 93.2724 1 6 7 -13 106.112 108.408 1 6 7 -13 290.296 162.064 11 -6 -7 -13 447.234 231.019 9 -6 7 -13 241.823 204.366 7 -6 -7 13 370.924 226.019 5 -6 -7 -14 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355.122 201.530 8 -6 8 -10 3583.48 359.170 8 -6 8 -10 3437.44 399.357 7 6 8 -10 4682.83 266.207 11 -6 8 -10 4187.37 230.504 3 -6 8 10 4494.42 235.158 3 -6 -8 -10 3772.60 388.464 9 -6 -8 10 4085.22 245.731 10 -6 -8 10 4404.68 443.387 5 -6 8 -11 6355.72 510.323 7 6 8 -11 7413.32 371.097 11 -6 8 11 6635.39 325.975 3 -6 -8 11 7633.69 360.880 10 -6 8 -11 6448.74 473.872 8 -6 -8 11 6924.52 580.826 5 6 8 -12 5296.61 301.424 11 -6 -8 12 5477.68 281.593 10 -6 8 -12 4331.06 416.660 7 -6 -8 -12 4825.37 425.284 9 -6 -8 12 5231.60 489.336 5 6 8 -13 7030.99 364.307 11 -6 -8 13 6935.37 373.910 17 -6 -8 13 7434.63 350.366 10 -6 8 -13 5040.34 452.593 7 -6 -8 13 7025.48 569.317 5 -6 -8 -13 5647.20 480.311 9 6 8 -14 527.681 167.052 11 -6 -8 14 263.997 228.577 5 -6 -8 14 1029.32 183.849 17 -6 -8 -14 514.848 223.913 9 -6 -8 14 497.716 126.255 10 6 8 -15 2240.55 208.278 11 -6 -8 15 2057.93 171.434 10 -6 -8 15 2526.65 212.849 17 6 8 -16 39.1282 155.755 11 -6 -8 16 306.482 151.602 17 -6 -8 16 190.095 103.609 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35387.7 1475.72 3 -6 9 8 36289.1 1479.77 3 -6 9 -8 31993.4 1687.95 7 6 9 -8 35621.3 1483.41 11 -6 -9 8 37239.3 1746.73 5 -6 9 -9 251.796 234.335 7 -6 -9 9 748.131 281.692 5 -6 9 -9 620.650 126.178 3 -6 9 9 792.994 133.024 3 -6 -9 -9 801.374 253.725 9 6 9 -9 392.712 156.893 11 -6 9 9 351.548 159.489 15 -6 -9 10 13032.8 817.033 5 -6 9 -10 11902.1 534.946 3 -6 9 10 12067.0 537.379 3 -6 9 -10 10266.5 724.691 7 6 9 -10 12505.0 565.999 11 -6 9 10 13874.1 562.026 15 -6 -9 -10 11075.3 716.064 9 -6 9 -11 952.891 262.171 7 -6 9 11 773.448 106.003 3 -6 -9 -11 318.157 227.102 9 -6 -9 11 775.377 263.719 5 6 9 -11 769.897 169.497 11 -6 9 11 939.393 152.498 15 6 9 -12 21231.1 913.031 11 -6 -9 -12 19537.1 1062.59 9 -6 9 12 21719.6 893.289 15 6 9 -13 260.037 161.314 11 -6 -9 13 44.2128 164.005 17 6 9 -14 26919.1 1089.73 11 -6 -9 14 25001.6 1076.23 17 6 9 -15 1241.98 172.714 11 6 9 -16 14463.8 636.597 11 6 9 -17 6653.45 336.736 11 6 9 -18 6142.58 307.883 11 6 9 -19 970.672 123.079 11 6 9 -20 8592.59 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41161.6 1650.14 17 -7 -4 15 38487.7 1615.09 4 -7 4 15 38859.5 1616.01 4 7 4 -15 40213.3 1624.15 11 -7 -4 15 40266.9 1836.06 5 -7 4 -16 919.352 100.324 1 -7 -4 16 1328.21 249.508 5 -7 4 16 1330.15 191.115 16 -7 -4 16 1105.61 135.168 4 -7 4 16 988.817 131.256 4 7 4 -16 1336.67 177.536 11 -7 -4 16 1323.90 224.208 17 -7 -4 17 13070.5 784.705 5 7 4 -17 13175.7 609.624 11 -7 -4 17 13803.9 602.947 4 -7 4 17 14350.6 605.057 4 -7 4 -17 13146.1 571.098 1 -7 4 17 14718.7 628.942 16 -7 -4 17 13909.9 638.955 17 -7 -4 18 10895.0 512.820 4 -7 4 18 10853.5 512.636 4 7 4 -18 11848.7 528.121 11 -7 -4 18 12248.7 554.695 17 -7 4 18 12103.0 544.191 16 -7 -4 19 14190.8 627.390 4 -7 4 19 13852.0 627.438 4 7 4 -19 15091.9 637.797 11 -7 4 19 14697.5 652.319 16 -7 4 20 1929.52 206.373 16 7 4 -20 2072.52 175.202 11 -7 -4 20 2302.39 160.677 4 -7 4 20 1951.21 162.115 4 -7 4 21 10668.4 497.228 16 7 4 -21 11064.1 476.307 11 -7 -4 21 10647.5 473.569 4 -7 4 21 10187.9 472.915 4 -7 4 22 2006.83 193.315 16 7 4 -22 2081.16 152.966 11 7 4 -23 2883.00 166.814 11 7 4 -24 1973.81 124.935 11 -7 -4 24 1954.02 123.395 10 -7 5 0-44.6524 208.277 7 -7 -5 1 38113.3 1609.83 10 -7 -5 1 41227.7 1708.32 9 -7 5 1 41367.5 1776.14 7 -7 -5 2 4845.90 251.407 10 -7 -5 2 5656.18 401.173 5 -7 5 -2 4838.72 411.527 7 -7 -5 3 48471.1 2038.89 5 -7 5 -3 51575.7 2072.28 7 -7 -5 3 44928.0 1869.44 10 -7 -5 4 1941.73 265.845 5 -7 -5 4 1952.99 143.470 10 -7 5 -4 1952.63 305.358 7 -7 -5 5 45977.2 1871.21 10 -7 5 -5 47809.7 2053.50 7 -7 -5 6 1166.08 115.249 10 -7 5 -6 1127.89 260.392 7 -7 5 -7 45005.0 2002.83 7 7 5 -7 47033.0 1822.28 11 -7 -5 -7 45127.1 1837.00 12 -7 -5 7 43144.8 1830.40 10 -7 5 -8 1308.68 259.195 7 7 5 -8 1567.63 140.615 11 -7 5 -8 1296.67 128.358 3 -7 5 8 1434.68 125.847 3 -7 -5 -8 1275.43 141.483 12 -7 -5 -9 8936.05 410.233 12 -7 5 9 8236.51 388.602 4 -7 -5 9 9837.80 596.656 5 -7 5 -9 8816.47 567.916 7 7 5 -9 9154.66 407.104 11 -7 5 9 9845.38 422.991 16 -7 5 9 8217.05 389.122 3 7 5 -10 26.3174 117.025 11 -7 5 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344.097 108.116 3 -8 -5 6 580.964 109.409 10 -8 5 -7-123.650 218.062 7 -8 5 7 97.9914 73.8440 4 -8 -5 -7-59.4718 174.803 9 -8 -5 7 139.133 178.987 5 -8 -5 7 71.6116 95.5597 10 -8 5 -7 29.1439 105.400 3 -8 5 7 4.66320 98.8626 3 -8 -5 -7-48.2004 121.717 12 -8 5 -8 680.233 226.886 7 -8 5 8 1033.54 144.989 16 -8 5 -8 726.769 118.691 3 -8 5 8 688.124 111.746 3 -8 -5 8 664.753 99.4092 4 -8 5 8 802.068 99.4061 4 -8 -5 8 861.490 228.325 5 -8 -5 8 948.314 121.348 10 -8 -5 -8 835.933 138.248 12 -8 5 -9 605.341 218.937 7 -8 5 9 862.164 101.333 4 -8 -5 9 726.106 102.196 4 -8 -5 -9 572.566 129.095 12 -8 5 -9 700.619 111.936 3 -8 5 9 747.938 105.186 3 -8 -5 9 616.549 120.500 10 -8 -5 9 773.992 242.726 5 -8 5 9 525.348 147.008 16 -8 -5 10 3300.98 366.720 5 -8 -5 10 2774.32 197.304 10 -8 5 10 3108.83 212.671 16 -8 5 10 2554.90 164.755 3 -8 -5 -10 2867.90 197.449 12 -8 -5 10 2950.15 175.760 4 -8 5 10 2899.22 173.763 4 -8 5 -10 2391.58 292.218 7 8 5 -10 2816.87 193.903 11 -8 5 11 542.103 105.069 4 -8 -5 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134.261 3 -8 -6 3 237.960 105.075 10 -8 6 -3 255.812 239.112 7 -8 -6 3 371.680 135.537 14 -8 -6 4 50579.9 1938.13 14 -8 6 -4 49983.0 2147.80 7 -8 -6 4 47094.4 1934.82 10 -8 6 4 46464.6 1928.20 3 -8 6 -4 45881.4 1927.63 3 -8 -6 4 49794.5 2152.18 5 -8 -6 5 1087.90 128.629 10 -8 6 -5 965.039 137.301 3 -8 6 5 1109.52 139.217 3 -8 -6 5 1217.00 266.624 5 -8 6 -5 1072.65 262.343 7 -8 6 -6 88810.4 3608.74 3 -8 6 6 90138.8 3608.38 3 -8 6 -6 92341.2 3823.03 7 -8 -6 6 92791.1 3624.60 10 -8 6 -7 1028.35 136.624 3 -8 6 7 1234.23 137.320 3 -8 -6 7 1114.64 134.464 10 -8 -6 -7 1026.87 150.933 12 -8 6 -8 57105.4 2390.68 3 -8 6 8 59555.9 2391.65 3 -8 -6 8 59799.5 2414.80 10 -8 -6 -8 59105.5 2410.06 12 -8 6 -8 59471.6 2593.76 7 8 6 -8 62893.6 2396.10 11 -8 6 -9 2092.16 154.259 3 -8 6 9 2191.60 149.158 3 -8 -6 -9 1564.79 159.891 12 8 6 -9 1947.87 167.626 11 -8 6 9 1925.91 135.212 4 -8 -6 9 2069.45 173.545 10 -8 6 -9 1949.19 297.256 7 -8 6 10 29111.4 1250.65 4 8 6 -10 34241.6 1268.13 11 -8 -6 10 32959.0 1285.76 10 -8 6 -10 29321.0 1430.75 7 -8 -6 10 34314.9 1537.07 5 -8 -6 -10 29634.7 1264.88 12 -8 6 -10 30214.3 1248.07 3 -8 6 10 29705.7 1246.48 3 8 6 -11 291.708 133.859 11 -8 6 11 297.552 88.7088 4 -8 -6 -11 217.171 103.342 12 -8 6 -11 297.358 194.437 7 -8 -6 11 381.694 234.688 5 -8 -6 11 239.587 119.408 10 -8 6 11 269.386 81.8120 3 -8 -6 12 38743.4 1736.52 5 -8 -6 12 35430.8 1481.55 10 8 6 -12 38399.2 1470.30 11 -8 6 12 33596.8 1451.98 4 -8 -6 -12 36543.6 1646.33 9 8 6 -13 287.796 147.741 11 -8 -6 -13 358.756 213.286 9 -8 6 13 145.292 85.8045 4 -8 -6 13 105.047 234.849 5 -8 -6 13 198.186 119.258 10 -8 -6 14 57435.4 2164.02 17 -8 -6 14 53843.5 2388.70 5 -8 6 14 52069.9 2115.41 4 -8 -6 -14 48627.6 2289.86 9 -8 -6 14 50533.9 2141.77 10 8 6 -14 52786.5 2127.85 11 -8 -6 15 2187.87 182.860 10 8 6 -15 2378.36 190.521 11 -8 -6 15 2084.03 248.318 17 -8 6 15 2286.60 148.736 4 -8 -6 16 39686.7 1683.26 10 -8 -6 16 43337.0 1699.34 17 8 6 -16 40645.0 1670.84 11 8 6 -17 765.065 140.911 11 -8 -6 17 899.306 192.797 17 -8 -6 17 849.590 133.502 10 -8 -6 18 29107.6 1260.60 10 -8 -6 18 31513.0 1272.74 17 8 6 -18 31417.5 1255.04 11 -8 -6 19 577.825 105.429 10 8 6 -19 937.659 123.993 11 8 6 -20 16005.3 654.701 11 -8 -6 20 15219.7 661.334 10 -8 -6 21 114.152 74.1457 10 8 6 -21-13.7291 82.2160 11 -8 -6 22 12289.1 508.467 10 8 6 -22 11975.0 497.926 11 -8 7 0 42149.0 1782.91 3 -8 -7 0 44576.7 1780.84 14 -8 7 0 43444.8 1985.89 7 -8 7 0 43768.7 1788.22 15 -8 7 0 44266.8 1773.91 13 -8 7 1-21.7620 109.989 13 -8 7 -1 11.2990 114.712 13 -8 7 1 97.1887 156.984 15 -8 -7 1-31.4323 132.094 14 -8 -7 -1-12.2817 129.139 14 -8 7 -1 293.137 241.304 7 -8 7 -1-25.9223 131.130 3 -8 -7 -2 36533.1 1479.12 14 -8 -7 2 37528.1 1485.84 14 -8 7 -2 34477.3 1480.69 3 -8 7 2 36134.8 1485.31 15 -8 7 2 35969.2 1472.58 13 -8 7 -2 35584.4 1476.30 13 -8 7 -2 38071.1 1716.13 7 -8 -7 3 65.6457 132.367 14 -8 -7 -3-162.114 123.382 14 -8 7 -3 54.2092 120.167 13 -8 7 -3-62.6239 261.792 7 -8 7 -3 24.7468 133.930 3 -8 7 3 138.463 140.736 3 -8 7 3 77.9523 148.169 15 -8 -7 4 733.983 125.864 10 -8 7 4 1194.03 155.564 3 -8 7 -4 969.328 146.446 3 -8 7 -4 1211.92 300.928 7 -8 -7 -4 937.504 225.517 9 -8 7 -4 605.614 136.748 13 -8 -7 -4 619.600 133.201 14 -8 7 4 755.783 151.351 15 -8 -7 5 507.052 250.143 5 -8 -7 5 664.466 122.531 10 -8 7 -5 458.539 251.562 7 -8 -7 -5 354.787 197.119 9 -8 7 5 791.352 142.496 3 -8 7 -5 684.337 137.595 3 -8 7 -6 1138.58 142.980 3 -8 7 6 1269.11 147.934 3 -8 -7 -6 805.380 149.800 12 -8 -7 6 933.034 134.611 10 -8 -7 6 827.747 271.884 5 -8 7 -6 1320.73 299.743 7 -8 -7 -6 1449.84 256.210 9 8 7 -6 1161.40 138.674 11 -8 7 -7 527.878 126.992 3 -8 7 7 788.145 130.207 3 -8 7 -7 441.408 235.509 7 -8 -7 -7 567.663 131.290 12 -8 -7 7 490.174 119.313 10 -8 -7 7 386.907 244.163 5 -8 -7 -7 613.199 221.123 9 8 7 -7 534.125 126.344 11 -8 -7 -8 5949.09 316.986 12 -8 7 -8 6168.73 487.783 7 8 7 -8 6441.23 316.408 11 -8 -7 8 5995.03 525.197 5 -8 7 -8 5883.66 304.205 3 -8 7 8 6179.12 306.279 3 -8 -7 8 6703.96 331.070 10 -8 -7 -8 5722.39 451.463 9 -8 7 -9 3354.63 204.896 3 -8 -7 -9 3256.63 213.659 12 -8 7 -9 3112.89 358.167 7 -8 -7 9 3834.25 232.739 10 -8 7 9 3609.58 206.499 3 -8 -7 -9 4151.58 373.630 9 8 7 -9 3823.12 225.617 11 -8 -7 -10 1912.42 294.431 9 -8 7 10 1405.60 126.599 3 8 7 -10 1450.59 163.281 11 -8 -7 10 1631.97 161.488 10 -8 7 -10 1173.56 127.748 3 -8 7 -10 1124.18 255.700 7 -8 7 -11 2544.43 304.937 7 -8 7 11 2455.30 160.247 3 -8 -7 11 3529.89 223.119 10 -8 -7 -11 2517.38 322.931 9 8 7 -11 3536.38 214.689 11 -8 -7 12 8167.15 410.173 10 8 7 -12 8327.17 399.551 11 -8 -7 -12 7361.01 538.803 9 -8 -7 13 592.212 134.522 10 -8 -7 -13 357.906 216.927 9 8 7 -13 546.299 147.369 11 -8 -7 14-23.0615 117.046 10 8 7 -14-40.6086 134.539 11 -8 -7 14-7.88906 193.683 17 -8 -7 15 7.31972 113.153 10 8 7 -15 110.952 130.605 11 -8 -7 15-81.0710 186.219 17 -8 -7 16 525.371 117.513 10 8 7 -16 358.460 128.337 11 -8 -7 16 252.827 176.738 17 -8 -7 17 974.492 129.207 10 -8 -7 17 973.628 170.207 17 8 7 -17 926.081 137.123 11 8 7 -18 5896.38 275.578 11 -8 -7 18 5001.18 286.969 17 -8 -7 18 5405.68 277.509 10 -8 -7 19 89.4011 83.1017 10 8 7 -19 153.081 99.5505 11 -8 -7 20 1198.57 102.249 10 8 7 -20 1084.71 106.937 11 -8 -7 21 2175.74 120.166 10 8 7 -21 1871.87 116.747 11 -8 8 0 27233.5 1156.76 13 -8 -8 0 28745.3 1160.02 14 -8 8 0 30244.6 1173.68 3 -8 8 0 25321.2 1168.67 15 -8 8 -1 1012.91 169.265 3 -8 8 1 1199.97 197.237 15 -8 8 1 1319.89 152.325 13 -8 8 -1 1480.51 155.526 13 -8 -8 1 1712.98 164.054 14 -8 -8 -1 1044.93 151.086 14 -8 8 -1 1175.01 291.736 7 -8 8 2 3550.59 371.750 7 -8 8 -2 3173.21 390.051 7 -8 8 -2 3483.55 230.262 3 -8 -8 -2 3105.55 204.486 14 -8 8 -2 2562.02 201.557 13 8 8 -2 2797.33 200.936 11 -8 8 2 2350.14 226.850 15 -8 8 -3 32.7531 253.815 7 -8 8 3 334.913 147.341 3 -8 8 3 306.582 160.977 15 8 8 -3 350.306 130.265 11 -8 -8 -3 188.706 124.828 14 -8 8 -3 445.288 130.617 13 -8 8 -3 314.197 140.385 3 -8 -8 -4 23.6902 194.027 9 -8 8 -4-228.964 270.699 7 -8 8 4 186.817 133.996 3 -8 8 -4 24.8022 128.019 3 -8 8 4-100.158 162.918 15 8 8 -4 145.906 124.306 11 -8 8 -4 120.852 132.440 13 -8 -8 -4 328.807 127.390 14 -8 -8 -5 3556.35 350.354 9 -8 8 5 3470.98 243.564 15 8 8 -5 3626.65 227.508 11 -8 8 -5 3929.28 246.062 13 -8 -8 -5 3804.20 229.640 14 -8 8 -5 3895.65 238.841 3 -8 8 5 3964.62 238.308 3 -8 8 -5 3943.03 417.661 7 8 8 -6 104.139 124.407 11 -8 -8 -6-47.7498 190.241 9 -8 8 6-140.007 141.106 15 -8 8 -6 90.7011 124.780 3 -8 8 6 223.196 128.234 3 -8 -8 -6 86.2909 122.095 12 -8 8 -6 189.718 139.575 13 -8 -8 -6 79.2764 118.707 14 -8 -8 6 148.730 232.903 5 -8 8 -6-344.054 261.515 7 -8 -8 7 1883.42 163.849 10 -8 -8 7 2031.34 328.968 5 -8 8 7 2177.38 172.619 15 -8 -8 -7 1790.45 167.540 12 -8 8 -7 1424.46 158.017 3 -8 8 7 1923.83 165.816 3 -8 -8 -7 2033.56 171.576 14 8 8 -7 1835.54 172.453 11 -8 -8 -7 1881.46 277.604 9 -8 8 -7 1462.53 288.802 7 -8 -8 -8-106.790 130.386 14 8 8 -8 22.6926 130.865 11 -8 -8 8-76.9056 247.328 5 -8 8 -8-80.9128 110.799 3 -8 8 8 198.780 112.722 3 -8 -8 8 36.9863 108.928 10 -8 -8 -8-99.1165 190.659 9 -8 8 -8 29.4254 218.072 7 -8 -8 9 2635.94 384.970 5 -8 8 -9 2317.22 175.270 3 -8 8 9 3091.26 186.258 3 -8 8 -9 2727.33 335.342 7 8 8 -9 3048.68 203.945 11 -8 -8 -9 2682.75 319.296 9 -8 -8 9 3011.53 202.877 10 8 8 -10-99.4467 136.737 11 -8 -8 10-77.6594 229.558 5 -8 8 -10 79.9672 97.2166 3 -8 8 10 17.3417 98.2495 3 -8 -8 10 76.9122 117.103 10 -8 8 -10-238.192 206.075 7 -8 -8 -10 52.2788 210.595 9 8 8 -11 9047.03 439.839 11 -8 8 11 9425.70 410.271 3 -8 -8 11 10172.6 454.614 10 8 8 -12 52.2220 134.920 11 -8 -8 12-45.5519 112.711 10 -8 -8 13 6194.39 318.867 10 8 8 -13 5846.30 312.769 11 -8 -8 13 5981.50 349.209 17 8 8 -14 668.099 142.691 11 -8 -8 14 744.980 128.503 10 -8 -8 14 608.627 176.722 17 -8 -8 15 4041.72 232.775 10 8 8 -15 3832.21 233.316 11 -8 -8 15 4025.98 262.358 17 8 8 -16 509.788 124.031 11 -8 -8 16 526.359 111.805 10 -8 -8 16 351.084 146.516 17 -8 -8 17 8479.72 377.505 10 8 8 -17 8434.84 374.297 11 -8 -8 17 7665.19 379.420 17 -8 -8 18 8.32489 77.0306 10 8 8 -18 72.4215 94.3879 11 8 8 -19 4893.09 220.864 11 -8 -8 19 4267.99 215.327 10 8 9 0 147.676 133.870 11 -8 9 0 441.716 148.565 3 -8 9 0 330.749 136.764 13 -8 9 1 51.4434 176.470 15 8 9 -1 137.624 133.216 11 -8 9 1-240.863 235.841 7 -8 9 -1 114.328 149.246 3 -8 9 -1 214.180 134.419 13 -8 9 2 1257.15 196.467 15 -8 9 2 1486.11 290.962 7 -8 9 -2 605.866 281.057 7 8 9 -2 1061.70 157.381 11 -8 9 -2 1235.66 166.941 3 -8 9 -2 1246.68 157.541 13 -8 9 -3 3849.13 252.015 3 -8 9 3 4283.21 256.796 3 -8 9 3 3958.44 267.203 15 -8 9 -3 4170.39 252.386 13 8 9 -3 3631.88 241.446 11 -8 9 -4 2927.55 217.280 3 -8 9 4 3245.15 222.284 3 -8 9 4 2922.22 232.512 15 -8 9 -4 3348.15 225.468 13 8 9 -4 3077.56 215.245 11 -8 9 -4 2505.45 368.088 7 -8 9 -5 347.919 135.099 3 -8 9 5 181.203 132.216 3 -8 9 5 75.9756 153.921 15 -8 9 -5 133.523 139.357 13 -8 9 -5 257.366 241.589 7 -8 -9 -5 21.7743 132.925 12 8 9 -5 230.702 134.280 11 -8 -9 -6 73.2753 190.374 9 -8 9 6 108.463 143.651 15 -8 9 -6 187.548 224.166 7 -8 9 -6 145.237 121.407 3 -8 9 6 323.575 133.289 3 -8 9 -6 453.131 147.930 13 8 9 -6 183.580 132.341 11 -8 -9 -6 215.175 119.308 12 -8 9 -7 5031.06 293.944 13 -8 9 7 5301.31 274.121 3 -8 9 -7 5040.99 271.697 3 8 9 -7 5347.59 280.030 11 -8 9 -7 5491.84 462.757 7 -8 9 7 4647.99 275.713 15 -8 -9 -7 4492.25 402.564 9 -8 9 -8 4345.53 242.907 3 -8 9 8 4875.33 248.534 3 8 9 -8 4423.99 258.733 11 -8 9 -8 4308.66 413.776 7 -8 -9 -8 3816.80 373.606 9 -8 9 -8 4817.99 279.434 13 -8 9 -9 1607.76 182.237 13 -8 9 -9 1642.11 139.298 3 -8 9 9 1444.25 139.644 3 8 9 -9 1595.49 166.478 11 -8 9 -10 4225.98 228.684 3 -8 9 10 4828.41 232.881 3 -8 9 -10 4621.57 274.427 13 8 9 -10 4690.42 263.571 11 -8 -9 11 270.088 109.878 10 8 9 -11 211.098 136.082 11 8 9 -12 4919.92 269.841 11 -8 -9 12 4874.58 264.711 10 -8 -9 13 3042.43 194.479 10 -8 -9 13 3343.49 234.832 17 8 9 -13 3182.83 208.256 11 -8 -9 14 319.254 97.1940 10 -8 -9 14 230.936 147.199 17 8 9 -14 273.349 122.296 11 -8 -9 15 82.4323 83.8677 10 -8 -9 15 195.565 132.236 17 8 9 -15-128.151 112.316 11 -8 -9 16 267.393 110.879 17 8 9 -16 250.493 105.595 11 8 9 -17 3853.52 199.938 11 8 9 -18 1190.13 100.612 11 -8 10 0 45546.2 2218.82 7 -8 10 0 51472.6 2040.84 3 8 10 -1 804.502 160.164 11 -8 10 -1 960.335 170.190 3 8 10 -2 62942.5 2489.14 11 -8 10 2 58060.0 2501.15 15 -8 10 -2 64533.3 2497.30 3 -8 10 -2 61562.1 2498.66 13 8 10 -3 190.421 151.832 11 -8 10 -3 194.508 144.041 3 -8 10 -3 272.975 145.878 13 -8 10 3 316.448 184.696 15 8 10 -4 58286.2 2327.00 11 -8 10 4 55927.2 2335.47 15 -8 10 -4 60860.2 2331.17 3 -8 10 4 61863.1 2332.57 3 -8 10 -4 57878.2 2336.71 13 -8 -10 -4 51840.6 2329.75 12 8 10 -5 85.8184 137.890 11 -8 10 -5 88.3833 121.072 3 -8 10 5 307.834 135.397 3 -8 10 -5 88.5289 143.551 13 -8 10 5 162.786 165.039 15 8 10 -6 46481.1 1905.37 11 -8 10 6 44438.0 1906.92 15 -8 10 -6 49180.9 1904.06 3 -8 10 6 49212.6 1904.82 3 -8 10 -6 45588.3 1914.46 13 -8 10 -7 508.305 121.380 3 -8 10 7 365.625 120.697 3 8 10 -7 535.235 144.742 11 -8 10 -7 440.709 149.652 13 -8 10 -8 30111.3 1285.72 13 -8 10 -8 30278.7 1263.91 3 -8 10 8 33291.3 1268.86 3 8 10 -8 30152.7 1275.35 11 -8 10 9 1634.62 137.600 3 -8 10 -9 1512.44 134.658 3 -8 10 -9 1928.97 177.658 13 8 10 -9 1989.28 171.404 11 -8 10 -10 43825.8 1763.81 3 -8 10 -10 44339.5 1794.85 13 8 10 -10 44222.9 1785.15 11 8 10 -11 213.898 130.911 11 -8 10 -11 264.026 131.252 13 8 10 -12 26550.6 1074.27 11 -8 10 -12 26955.3 1084.61 13 -8 -10 12 24773.9 1080.09 17 8 10 -13 1158.41 139.698 11 -8 -10 13 1397.19 156.347 17 -8 -10 14 19677.3 876.485 17 8 10 -14 22777.0 882.588 11 -8 10 -14 22081.0 891.411 13 8 10 -15 2694.80 163.234 11 8 10 -16 21607.2 877.962 11 -8 11 0 1161.40 160.557 3 -8 11 -1 894.827 149.588 3 -8 11 -2 800.661 145.657 3 -8 11 -3 461.494 133.721 3 8 11 -3 476.911 133.211 11 -8 11 -4 415.297 125.890 3 -8 11 4 485.213 127.321 3 8 11 -4 364.030 132.661 11 -8 11 -4 390.387 139.123 13 -8 11 5 630.758 122.458 3 -8 11 -5 482.864 123.289 3 8 11 -5 696.312 144.474 11 -8 11 -5 733.395 147.043 13 -8 11 -6 44.9967 111.960 3 -8 11 6 155.976 108.952 3 8 11 -6 56.8319 128.683 11 -8 11 -6 114.933 126.750 13 -8 11 7 821.155 114.753 3 -8 11 -7 582.715 114.329 3 8 11 -7 617.828 138.081 11 -8 11 -7 468.924 137.065 13 -8 11 8 2238.51 145.724 3 -8 11 -8 2039.27 141.956 3 -8 11 -8 1947.26 173.861 13 8 11 -8 2013.22 171.189 11 8 11 -9 1185.02 147.327 11 -8 11 -9 1460.42 110.034 3 -8 11 -9 1476.13 151.672 13 -8 -11 10 660.398 147.187 17 8 11 -10 851.115 128.154 11 -8 11 -10 1110.68 135.246 13 -8 11 -10 792.000 82.1224 3 8 11 -11 73.0118 111.126 11 -8 11 -11 47.9037 109.847 13 -8 -11 11 7.79426 121.258 17 -8 11 -12 1683.26 142.600 13 8 11 -12 1612.58 136.682 11 8 11 -13 2378.58 151.348 11 8 11 -14-5.23359 85.4235 11 -8 12 0 19380.1 813.229 3 -8 12 -1 220.881 121.165 3 -8 12 -2 16846.6 712.931 3 -8 12 -3 625.161 122.270 3 -8 12 4 14636.9 623.833 3 -8 12 -4 14802.0 624.946 3 -8 12 -5 242.743 104.000 3 -8 12 5 7.49302 97.2235 3 8 12 -6 18782.3 848.532 11 -8 12 -6 20961.3 844.912 3 -8 12 6 21769.2 845.825 3 -8 12 7 4177.55 201.160 3 -8 12 -7 4175.68 200.702 3 8 12 -8 12708.9 582.693 11 -8 12 -8 13575.8 569.314 3 8 12 -9 268.112 106.170 11 -8 12 -9 318.588 62.4909 3 -8 12 -9 413.118 108.804 13 8 12 -10 11069.7 522.448 11 -8 12 -10 14618.0 538.260 13 8 12 -11 160.662 85.5169 11 -8 12 -11 113.386 90.1897 13 -8 13 0 969.003 109.271 3 -8 13 -1 458.582 100.336 3 -8 13 -2 6212.46 287.374 3 -8 13 -3-8.99625 88.4253 3 -8 13 -4 345.723 82.7670 3 -8 13 4 372.431 82.8620 3 -8 13 -5 163.463 74.0656 3 -8 13 5 70.6964 72.8959 3 -8 13 -6 390.623 71.1562 3 -8 13 6 415.937 73.0000 3 -9 0 0 25.5471 114.683 12 -9 0 -1-51.3622 86.1644 9 -9 0 -1-12.8542 106.239 12 -9 0 2 4586.42 237.614 10 -9 0 -2 4629.87 271.677 9 -9 0 -2 5310.05 269.963 12 -9 0 3 42.5139 78.9222 10 -9 0 -3 132.845 97.5222 9 -9 0 -3-6.54430 116.092 12 -9 0 4 229.990 81.7971 10 -9 0 -4 325.072 108.341 9 -9 0 5 140.221 78.0592 10 -9 0 -5-53.9943 107.169 9 -9 0 -6 4852.14 260.933 12 -9 0 -6 4599.85 290.503 9 -9 0 6 4124.68 223.678 10 -9 0 -7 35.1202 119.978 12 -9 0 -7-76.8080 119.912 9 -9 0 7 19.4594 83.5069 4 -9 0 7 83.3501 73.2689 10 -9 0 8 2861.34 234.116 17 -9 0 -8 2802.83 246.932 9 -9 0 -8 3099.12 220.595 12 -9 0 8 3554.00 189.748 4 -9 0 8 3068.77 182.859 10 -9 0 9 72.7244 161.465 17 -9 0 9-21.8485 78.5797 10 -9 0 -9 208.345 125.100 12 -9 0 -9 88.8099 130.526 9 -9 0 9 21.3543 95.2365 4 -9 0 -10 353.043 161.386 9 -9 0 10 432.480 110.297 4 -9 0 10 679.858 181.135 17 -9 0 -11-52.0426 155.745 9 -9 0 11-11.8302 105.387 4 -9 0 11 227.428 182.835 17 -9 0 -12 25335.6 1195.86 9 -9 0 12 25735.9 1089.56 4 -9 0 12 27334.1 1122.01 17 -9 0 -13 37.9734 160.359 9 -9 0 13-38.4167 113.951 4 -9 0 13-121.757 192.567 17 -9 0 -14 20320.5 1047.14 9 -9 0 14 21768.5 941.236 4 -9 0 -15 139.041 164.506 9 -9 0 15 117.123 122.932 4 -9 0 15 353.174 191.739 17 -9 0 16 456.382 137.022 4 -9 0 -16 593.153 192.145 9 -9 0 17 41.2225 124.595 4 -9 0 18 2534.83 195.807 4 -9 0 19 127.880 130.037 4 -9 0 20 12190.2 546.454 4 -9 0 21-27.8651 80.9723 10 -9 0 21-103.455 137.313 16 -9 0 21-27.2010 112.086 4 -9 0 22 19141.2 844.712 10 -9 0 22 21565.3 858.706 16 -9 0 22 21758.0 863.948 4 -9 0 23 93.5617 107.018 16 -9 0 23 75.9085 63.9089 10 -9 1 0 18.4439 108.794 12 -9 1 -1 853.004 126.577 12 -9 1 1 1018.86 131.039 12 -9 -1 1 700.802 100.212 10 -9 -1 -1 627.437 130.200 9 -9 1 -2 7497.27 346.567 12 -9 -1 2 6705.83 319.806 10 -9 1 2 6397.90 310.769 10 -9 -1 -2 7390.91 376.459 9 -9 -1 3 2090.19 145.433 10 -9 1 3 2175.38 137.773 10 -9 1 -3 1890.51 154.207 9 -9 -1 -3 1882.82 186.243 9 -9 -1 4 2998.00 172.618 10 -9 1 4 2772.22 163.900 10 -9 1 -4 2597.89 190.059 9 -9 -1 -4 3223.65 233.640 9 -9 1 -4 2958.06 199.020 12 -9 -1 5 13483.5 573.486 10 -9 1 5 12598.6 565.193 10 -9 -1 -5 13772.9 594.265 12 -9 1 -5 14342.7 600.099 12 -9 1 -5 12233.8 601.714 9 -9 -1 -5 13604.5 639.852 9 -9 1 6 1069.86 104.831 10 -9 1 6 1029.75 117.301 3 -9 1 -6 1008.20 119.992 3 -9 -1 -6 1099.32 171.389 9 -9 1 -6 1107.49 138.730 9 -9 -1 -6 1262.85 144.421 12 -9 -1 6 877.512 104.313 10 -9 -1 6 1191.58 134.071 14 -9 -1 -7 1909.01 173.615 12 -9 1 -7 1837.63 142.421 3 -9 1 7 1627.28 134.331 3 -9 -1 7 1789.58 135.788 10 -9 1 7 1714.19 128.262 10 -9 -1 7 2024.99 135.584 4 -9 -1 -7 2037.24 212.330 9 -9 1 -7 1562.30 173.821 9 -9 -1 8 1286.92 122.970 4 -9 1 8 1380.89 181.367 17 -9 -1 -8 1579.49 152.184 12 -9 1 -8 1325.22 153.545 12 -9 1 8 1114.05 106.940 10 -9 -1 8 1240.37 115.385 10 -9 1 8 1086.97 118.240 3 -9 -1 -8 1310.25 193.547 9 -9 1 -8 1115.81 162.426 9 -9 -1 9 4491.20 233.098 10 -9 1 9 4204.75 221.113 10 -9 1 9 4928.81 278.936 17 -9 -1 -9 3944.26 315.300 9 -9 1 -9 3281.13 277.381 9 -9 -1 9 3928.68 227.237 4 -9 -1 -9 4495.27 258.647 12 -9 -1 -10 135.917 126.447 12 -9 -1 10 7.80463 179.312 17 -9 1 10 86.1587 164.624 17 -9 -1 10 67.8135 95.2230 4 -9 -1 10-22.1870 131.174 5 -9 1 10-21.6155 82.5384 10 -9 -1 -10-69.4888 152.479 9 -9 1 -10 87.6735 132.921 9 -9 -1 11 183.853 105.231 4 -9 1 11 111.583 168.287 17 -9 -1 11 201.464 187.044 17 -9 -1 11 89.5251 150.231 5 -9 1 -11 300.499 151.906 9 -9 -1 -11 335.595 169.035 9 -9 -1 12 172.264 110.332 4 -9 1 12 452.907 184.209 17 -9 -1 12 198.352 196.385 17 -9 -1 12 178.821 142.800 5 -9 1 -12 166.445 151.006 9 -9 -1 -12 332.787 186.525 9 -9 1 13 859.234 194.700 17 -9 -1 13 1212.70 220.823 17 -9 -1 -13 954.591 213.310 9 -9 1 -13 849.224 181.271 9 -9 -1 13 924.907 135.548 4 -9 -1 -14 1426.92 242.397 9 -9 -1 14 1515.29 158.114 4 -9 1 14 1279.14 208.674 17 -9 -1 -15 6191.72 474.372 9 -9 -1 15 7954.42 375.577 4 -9 -1 16 186.829 125.366 4 -9 -1 -16 379.925 185.456 9 -9 1 -16 162.161 150.121 9 -9 -1 17 1201.54 153.643 4 -9 -1 18 2273.60 186.108 4 -9 1 18 2164.26 207.561 16 -9 -1 19 2596.96 190.368 4 -9 1 19 2433.85 210.633 16 -9 -1 20 2662.74 190.279 4 -9 1 20 2520.53 205.061 16 -9 1 20 2624.85 161.691 10 -9 -1 21 530.115 96.2219 10 -9 1 21 597.325 84.4537 10 -9 -1 21 590.613 119.358 4 -9 1 21 517.432 138.538 16 -9 -1 22 56.9788 71.1951 10 -9 -1 22 23.3177 96.2357 4 -9 -1 22-12.6714 123.934 16 -9 1 22-124.525 125.029 16 -9 -1 23 158.367 110.208 16 -9 1 23 23.9060 105.726 16 -9 -1 23 39.8890 63.1316 10 -9 2 0 53.4945 107.316 12 -9 -2 0-35.7754 130.154 9 -9 -2 -1 121069. 4982.40 9 -9 2 -1 125584. 4933.67 12 -9 2 -2 1803.86 164.889 12 -9 -2 -2 1787.33 195.733 9 -9 -2 -3 91222.3 3846.10 9 -9 2 -3 96301.5 3796.24 12 -9 -2 -3 95737.1 3801.49 12 -9 -2 4 3571.46 210.031 14 -9 -2 -4 3583.71 228.353 12 -9 2 -4 3930.27 224.319 12 -9 2 4 3129.59 197.478 3 -9 2 -4 3518.53 203.275 3 -9 2 4 3225.84 180.962 10 -9 -2 -4 3257.68 258.823 9 -9 -2 -5 66820.5 2768.95 9 -9 -2 -5 66991.0 2705.87 12 -9 2 -5 70352.8 2709.61 12 -9 2 5 65794.1 2683.60 3 -9 2 -5 65617.1 2684.98 3 -9 2 5 63534.2 2678.88 10 -9 -2 5 74355.1 2699.46 14 -9 2 6 6143.27 317.370 10 -9 2 -6 6583.57 326.931 3 -9 2 6 7075.66 327.540 3 -9 2 6 7282.91 323.149 4 -9 -2 6 7197.78 325.060 4 -9 -2 -6 7571.39 359.625 12 -9 2 -6 7112.81 358.142 12 -9 -2 -6 6948.87 412.339 9 -9 -2 6 7413.92 349.295 14 -9 2 7 75079.1 3092.01 10 -9 -2 7 89049.9 3298.83 5 -9 -2 -7 83886.5 3121.54 12 -9 2 7 77034.8 3093.94 4 -9 -2 7 79070.0 3096.59 4 -9 -2 -7 83803.2 3206.09 9 -9 2 -7 74844.0 3091.97 3 -9 2 7 75197.3 3090.42 3 -9 -2 -8 1416.47 214.284 9 -9 2 8 1422.20 122.635 4 -9 -2 8 1532.41 126.819 4 -9 -2 -8 1804.54 162.466 12 -9 2 8 1321.44 125.877 3 -9 2 8 1879.94 184.229 17 -9 -2 8 1318.20 224.610 5 -9 2 8 1365.09 116.870 10 -9 2 -8 1429.72 131.672 3 -9 -2 -9 114203. 4266.03 12 -9 2 9 109572. 4256.90 17 -9 -2 9 119373. 4443.93 5 -9 2 9 100012. 4235.33 10 -9 -2 -9 111934. 4368.66 9 -9 2 9 104317. 4240.40 4 -9 -2 9 109812. 4244.92 4 -9 2 9 103816. 4231.29 3 -9 2 -9 106760. 4233.61 3 -9 -2 -10 3061.93 216.519 12 -9 2 10 3577.99 237.118 17 -9 -2 10 3376.65 192.694 4 -9 2 10 2895.85 184.097 4 -9 -2 10 3150.17 318.001 5 -9 -2 -10 2854.01 294.404 9 -9 2 10 2876.50 172.849 10 -9 2 10 2693.33 172.333 3 -9 -2 11 107921. 4213.89 4 -9 2 11 104729. 4209.70 4 -9 -2 -11 107099. 4227.81 12 -9 2 11 106574. 4226.35 17 -9 -2 11 111371. 4399.55 5 -9 2 11 103635. 4210.54 16 -9 -2 -11 113516. 4357.37 9 -9 2 11 102527. 4206.51 10 -9 -2 12 3051.42 322.325 5 -9 -2 -12 2799.47 306.526 9 -9 -2 12 3328.50 206.474 4 -9 2 12 2968.00 198.268 4 -9 2 12 3420.30 222.005 16 -9 -2 13 51319.8 2208.81 5 -9 -2 13 50734.0 2037.96 4 -9 2 13 49220.8 2033.17 4 -9 2 13 50967.4 2038.48 16 -9 -2 -13 49158.8 2172.78 9 -9 2 14 56.5202 109.578 4 -9 -2 14 124.419 115.715 4 -9 -2 -14-22.0659 183.607 9 -9 -2 14 222.200 150.439 5 -9 2 14 264.408 152.329 16 -9 -2 15 20679.4 842.463 4 -9 2 15 19903.4 837.037 4 -9 -2 -15 17170.2 956.506 9 -9 -2 15 20168.0 871.342 17 -9 2 15 18746.0 842.504 16 -9 -2 -16 1035.83 228.297 9 -9 -2 16 865.213 215.421 17 -9 -2 16 1538.82 157.375 4 -9 2 16 1276.30 148.242 4 -9 2 16 978.269 177.676 16 -9 -2 17 48698.8 1874.91 4 -9 2 17 47417.1 1870.85 4 -9 2 17 43850.9 1869.87 16 -9 -2 17 43746.1 1884.85 17 -9 -2 18 2894.53 208.348 4 -9 2 18 3271.04 209.210 4 -9 2 18 3571.00 235.332 16 -9 -2 19 40879.2 1552.03 4 -9 2 19 39703.9 1548.77 4 -9 2 19 34716.4 1528.02 10 -9 2 19 38009.4 1548.10 16 -9 2 20 4762.99 272.513 16 -9 -2 20 4866.67 258.052 4 -9 2 20 4887.97 257.148 4 -9 -2 21 37418.7 1583.17 10 -9 2 21 37794.3 1584.96 16 -9 -2 21 41764.3 1591.51 4 -9 2 21 40012.9 1588.37 4 -9 -2 22 1657.58 119.244 10 -9 2 22 1733.69 154.751 16 -9 -2 22 1733.60 133.245 4 -9 2 22 1479.09 132.246 4 -9 2 23 19045.3 798.733 16 -9 -2 23 19061.1 795.430 10 -9 -2 23 20195.9 800.736 16 -9 3 0 47.5371 118.024 3 -9 3 0-11.8170 104.196 12 -9 -3 0-13.4840 131.827 9 -9 3 1 2648.56 180.665 12 -9 3 -1 2930.12 188.652 12 -9 -3 1 3038.36 179.909 14 -9 -3 1 2646.62 172.989 10 -9 -3 -1 2523.04 230.296 9 -9 3 -1 2425.49 179.026 3 -9 -3 2-10.4535 102.775 14 -9 3 -2 6.25670 114.319 12 -9 3 -2-20.9324 112.945 3 -9 -3 2 51.2803 81.1027 10 -9 -3 -2 123.376 132.009 9 -9 -3 3 3442.27 204.614 14 -9 3 -3 3559.12 216.319 12 -9 -3 -3 3445.96 265.529 9 -9 -3 3 3109.19 198.752 10 -9 3 3 3476.80 204.561 3 -9 3 -3 3373.33 207.392 3 -9 3 -4 5656.21 302.808 3 -9 3 4 5714.54 301.358 3 -9 -3 -4 6842.10 332.230 12 -9 -3 4 6583.67 312.312 14 -9 -3 -4 6786.43 392.214 9 -9 -3 4 6122.03 304.279 10 -9 -3 -5 50.2045 122.800 12 -9 3 -5 14.7269 101.977 3 -9 3 5-4.73205 97.8131 3 -9 -3 5 59.7830 91.8601 10 -9 -3 5-5.88683 114.891 14 -9 -3 -5-109.157 146.655 9 -9 3 6 2440.24 146.455 4 -9 -3 6 2382.17 150.785 4 -9 -3 -6 2257.24 190.521 12 -9 -3 6 2301.35 166.016 10 -9 3 6 2212.02 158.985 3 -9 3 -6 2145.62 163.267 3 -9 -3 6 2611.47 186.457 14 -9 -3 6 2311.15 288.062 5 -9 -3 -6 2450.77 248.234 9 -9 -3 7 30.9890 94.6828 10 -9 -3 7 100.467 85.6476 4 -9 3 7 73.7969 79.2927 4 -9 -3 -7 14.3299 124.330 12 -9 -3 7-77.5738 182.729 5 -9 3 -7 92.7655 103.742 3 -9 3 7 61.8864 94.4014 3 -9 -3 -7 68.1253 149.501 9 -9 -3 -8 1469.21 224.212 9 -9 3 8 1564.33 121.514 4 -9 -3 8 1409.99 124.968 4 -9 3 -8 1477.46 129.966 3 -9 3 8 1473.51 128.163 3 -9 -3 -8 1193.38 155.952 12 -9 3 8 920.793 153.164 17 -9 -3 8 1289.07 237.026 5 -9 -3 8 1239.07 132.830 10 -9 -3 -9 143.606 130.136 12 -9 -3 9 253.380 100.740 10 -9 3 9 186.112 70.8244 10 -9 3 -9 240.135 99.9558 3 -9 3 9 355.312 95.6607 3 -9 3 9 276.845 90.6913 4 -9 -3 9 366.317 101.338 4 -9 -3 -9 38.5897 173.492 9 -9 -3 9 133.561 172.081 5 -9 -3 -10 860.139 204.793 9 -9 -3 -10 1051.92 149.726 12 -9 3 10 862.438 135.501 16 -9 3 10 842.225 106.030 3 -9 -3 10 760.117 213.097 5 -9 -3 10 914.907 131.497 10 -9 3 10 841.530 92.8454 10 -9 3 10 986.744 113.547 4 -9 -3 10 982.087 123.680 4 -9 3 11 333.528 135.647 16 -9 -3 -11 565.522 134.081 12 -9 3 11 648.315 112.518 4 -9 -3 11 435.911 108.175 4 -9 -3 -11 388.241 187.510 9 -9 -3 11 446.682 118.687 10 -9 3 11 453.517 79.7916 10 -9 -3 11 55.0511 193.925 5 -9 3 12 17.2628 136.443 16 -9 -3 -12-14.3532 119.873 12 -9 -3 12 27.6914 168.663 5 -9 -3 12-223.002 204.643 17 -9 -3 -12 156.259 184.735 9 -9 3 12 18.5390 68.8484 10 -9 3 12 153.334 104.670 4 -9 -3 12 218.104 107.381 4 -9 -3 13 344.078 118.077 4 -9 3 13 284.526 107.295 4 -9 3 13 405.989 78.3631 10 -9 3 13 545.518 150.459 16 -9 -3 13 223.127 173.700 5 -9 -3 13 449.320 210.866 17 -9 -3 -13 275.286 196.208 9 -9 3 14 3369.15 227.203 16 -9 -3 14 3414.35 210.743 4 -9 3 14 2890.21 199.449 4 -9 -3 14 2874.67 332.532 5 -9 3 14 2996.87 177.669 10 -9 -3 14 3790.39 283.945 17 -9 -3 -14 3165.50 330.365 9 -9 3 15 3376.51 217.768 16 -9 -3 15 2462.69 189.509 4 -9 3 15 2870.43 191.057 4 -9 -3 15 2144.85 279.222 5 -9 3 15 2504.68 156.514 10 -9 -3 15 2803.37 266.186 17 -9 -3 -15 2203.04 291.286 9 -9 3 16 3516.50 245.040 16 -9 -3 16 4254.01 228.312 4 -9 3 16 3684.96 218.699 4 -9 3 16 3185.51 188.191 10 -9 -3 -16 3471.67 339.134 9 -9 -3 16 3648.07 286.552 17 -9 -3 17 1276.10 214.311 17 -9 -3 17 1721.34 154.985 4 -9 3 17 1732.50 151.404 4 -9 3 17 1374.99 178.586 16 -9 3 18-5.86531 145.733 16 -9 3 18 153.943 102.436 4 -9 -3 18 52.3832 103.872 4 -9 -3 18 154.485 182.634 17 -9 -3 19 151.927 107.570 4 -9 3 19 330.885 108.659 4 -9 3 19 209.139 148.953 16 -9 -3 20 386.664 103.310 4 -9 3 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1403.71 10 -9 4 11 33574.9 1379.50 4 -9 -4 11 33597.3 1380.85 4 -9 -4 -11 36158.0 1552.92 9 -9 4 11 34219.9 1385.43 16 -9 4 11 31743.4 1360.49 3 -9 4 12 19749.8 808.915 4 -9 -4 12 19360.2 809.573 4 -9 4 12 17655.1 811.626 16 -9 -4 12 19125.1 829.235 10 -9 -4 -12 19570.0 822.445 12 -9 -4 -12 18953.2 965.303 9 -9 -4 12 18960.0 1016.46 5 -9 -4 13 39358.6 1786.53 5 -9 -4 -13 37323.3 1720.39 9 -9 -4 13 37904.2 1559.53 4 -9 4 13 37708.3 1557.82 4 -9 4 13 37115.1 1562.77 16 -9 -4 13 40637.0 1600.52 17 -9 -4 13 38778.1 1582.44 10 -9 -4 14 6650.24 525.154 5 -9 -4 14 7152.98 375.426 10 -9 4 14 7448.49 371.940 16 -9 -4 14 8390.44 425.371 17 -9 -4 14 7660.33 358.164 4 -9 4 14 7007.37 352.321 4 -9 -4 -14 6253.44 485.905 9 -9 -4 15 9195.59 464.005 10 -9 -4 15 9806.66 446.895 4 -9 4 15 10244.7 447.341 4 -9 4 15 9829.05 460.044 16 -9 -4 15 9844.45 501.793 17 -9 -4 16 714.729 125.901 4 -9 4 16 986.118 129.213 4 -9 -4 16 975.494 222.118 17 -9 4 16 1237.22 173.122 16 -9 -4 16 1028.54 147.550 10 -9 4 17 39181.9 1674.87 16 -9 -4 17 39799.3 1692.26 17 -9 -4 17 41966.7 1670.91 4 -9 4 17 42679.9 1671.34 4 -9 -4 17 41481.3 1686.09 10 9 4 -18 444.544 106.655 11 -9 -4 18 479.232 106.745 4 -9 4 18 570.990 107.792 4 -9 -4 18 302.181 114.514 10 -9 4 18 557.293 154.174 16 -9 -4 19 24322.5 1065.53 10 -9 -4 19 26028.3 1060.89 4 -9 4 19 26377.9 1060.86 4 -9 4 19 26151.1 1070.01 16 -9 -4 20 1428.65 123.008 10 -9 -4 20 1568.45 123.621 4 -9 4 20 1311.86 122.012 4 -9 4 20 1297.95 158.619 16 -9 4 21 9798.18 410.616 4 -9 -4 21 8896.18 412.172 10 -9 -4 22 6716.71 302.949 10 -9 -5 0 6.01548 116.629 14 -9 5 0-23.7224 127.108 3 -9 -5 -1 1017.80 140.315 14 -9 5 -1 1346.56 157.304 3 -9 -5 1 1433.58 148.325 14 -9 -5 -1 1099.72 195.429 9 -9 -5 -2 9704.26 552.822 9 -9 5 -2 8783.11 454.634 3 -9 5 -2 10280.1 440.178 13 -9 -5 2 10631.8 461.830 14 -9 -5 3 189.022 108.094 10 -9 5 -3 236.049 220.579 7 -9 -5 -3 179.525 166.330 9 -9 -5 3 237.234 126.417 14 -9 5 -3 323.317 122.519 3 -9 5 3 189.896 124.316 3 -9 5 -4 2435.13 320.324 7 -9 -5 4 2687.67 185.365 10 -9 5 4 2377.89 149.376 4 -9 -5 4 2375.36 153.903 4 -9 -5 -4 2190.75 263.174 9 -9 5 4 2605.76 181.621 3 -9 5 -4 2451.73 180.214 3 -9 -5 4 3088.10 202.079 14 -9 5 -5 2945.43 344.303 7 -9 5 5 2798.83 162.045 4 -9 -5 5 2790.38 167.422 4 -9 -5 -5 2743.50 280.528 9 -9 -5 5 2787.36 203.870 14 -9 5 5 2930.41 192.634 3 -9 5 -5 2579.53 191.080 3 -9 -5 5 2681.82 192.438 10 -9 -5 -6 60.6320 172.401 9 -9 -5 6-122.450 186.447 5 -9 5 -6 252.236 223.435 7 -9 5 -6 115.349 114.207 3 -9 5 6 75.6481 113.028 3 -9 5 6 40.2342 77.7678 4 -9 -5 6 4.70430 87.4288 4 -9 -5 6 7.20888 105.471 10 -9 -5 -6 146.714 134.301 12 -9 5 -7 8029.57 367.196 3 -9 5 7 7912.33 361.472 3 -9 5 7 7327.20 350.382 4 -9 -5 7 7912.82 357.062 4 -9 -5 -7 7341.89 490.718 9 -9 -5 -7 7272.57 386.951 12 -9 -5 7 8606.23 580.971 5 -9 -5 7 7854.87 381.602 10 -9 5 -7 7224.35 509.021 7 -9 5 -8 526.668 218.339 7 -9 -5 -8 788.020 142.595 12 -9 5 -8 634.695 115.444 3 -9 5 8 439.582 111.968 3 -9 -5 8 770.357 109.224 4 -9 5 8 563.232 97.8353 4 -9 -5 8 830.335 241.109 5 -9 -5 -8 651.778 210.786 9 -9 -5 8 875.918 132.562 10 -9 5 -9 114.913 189.529 7 -9 -5 -9 232.143 132.749 12 -9 -5 9 64.9516 219.717 5 -9 -5 -9 179.928 190.291 9 -9 -5 9 365.424 113.777 10 -9 5 -9 173.218 100.888 3 -9 5 9 350.298 98.2581 3 -9 -5 9 351.712 96.1806 4 -9 5 9 371.343 93.9155 4 -9 -5 -10 240.790 124.867 12 -9 -5 10-32.9550 222.726 5 -9 -5 -10 187.035 202.402 9 -9 -5 10 320.661 126.483 10 -9 5 -10 214.406 99.3293 3 -9 5 10 36.3765 88.1287 3 -9 -5 10 16.0268 92.9538 4 -9 5 10 179.830 89.2013 4 -9 -5 -11 800.550 130.955 12 -9 -5 -11 406.527 212.004 9 -9 -5 11 398.557 234.044 5 -9 -5 11 651.400 135.814 10 -9 5 11 523.618 87.7024 3 -9 5 11 459.726 104.213 4 -9 -5 11 586.891 112.732 4 -9 5 12 1231.99 130.888 4 -9 -5 -12 1478.66 150.248 12 -9 -5 -12 797.086 235.443 9 -9 -5 12 1533.62 160.868 10 -9 5 12 1523.15 173.154 16 -9 -5 12 1549.64 141.281 4 -9 -5 12 1290.98 259.014 5 -9 -5 -13 2625.73 322.793 9 -9 -5 13 3496.44 199.446 4 -9 5 13 3496.77 200.079 4 -9 -5 13 3225.87 372.779 5 -9 -5 13 2948.42 218.474 10 -9 5 13 2907.12 220.664 16 -9 -5 13 3400.21 285.837 17 -9 -5 -14 1475.98 261.825 9 -9 5 14 2229.47 191.447 16 -9 -5 14 2447.24 254.398 17 -9 -5 14 1757.32 167.019 10 -9 -5 14 1630.70 147.839 4 -9 5 14 1730.05 147.046 4 -9 5 15 5397.23 299.599 16 -9 -5 15 6059.20 350.204 17 9 5 -15 4849.52 274.227 11 -9 -5 15 5066.28 290.924 10 -9 -5 15 5665.48 277.070 4 -9 5 15 5324.58 273.896 4 -9 5 16 749.057 160.984 16 9 5 -16 577.470 124.450 11 -9 -5 16 794.998 112.440 4 -9 5 16 632.400 110.118 4 -9 -5 16 751.426 129.152 10 -9 -5 16 916.917 206.034 17 9 5 -17 170.513 104.709 11 -9 -5 17 276.042 94.6110 4 -9 5 17 307.433 94.7520 4 -9 -5 17 152.827 107.281 10 -9 -5 17 90.5292 178.025 17 9 5 -18 385.631 101.213 11 -9 5 18 405.470 89.6673 4 -9 -5 18 422.559 93.2135 4 -9 -5 18 506.250 110.377 10 -9 -5 18 292.926 167.745 17 -9 -5 19 127.514 77.6388 4 -9 -5 19 209.237 97.4154 10 9 5 -19 62.1704 89.9777 11 -9 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214.293 7 -9 -6 -6 94.5056 136.504 12 -9 -6 -6 88.0689 182.215 9 -9 6 -6 54.3095 116.436 3 -9 6 6 31.9861 117.443 3 -9 -6 6 52.3781 112.020 10 -9 6 7 2406.76 159.688 4 -9 6 -7 2222.89 319.938 7 -9 -6 7 3309.69 206.686 10 -9 6 -7 3299.24 194.477 3 -9 6 7 2952.57 187.123 3 -9 -6 -7 2929.72 216.145 12 -9 -6 -7 2824.34 313.528 9 -9 -6 -8 257.259 204.394 9 -9 6 8 170.983 81.4349 4 -9 -6 -8 161.844 129.260 12 -9 6 -8 161.832 106.634 3 -9 6 8 28.7112 102.476 3 -9 -6 8 34.7492 201.278 5 -9 -6 8 268.295 127.450 10 -9 6 -8 25.5528 200.213 7 -9 -6 9 17508.1 929.871 5 -9 6 9 15641.0 641.595 3 -9 6 -9 15474.7 643.064 3 -9 -6 -9 14146.5 662.375 12 -9 -6 9 17166.5 683.964 10 -9 6 9 14029.4 637.185 4 -9 -6 -9 14901.1 811.702 9 -9 6 -9 12970.5 793.467 7 -9 -6 -10 8460.09 392.311 12 -9 -6 10 8858.08 619.420 5 -9 -6 10 9547.55 413.233 10 -9 6 10 7449.21 362.379 4 -9 -6 -10 7744.04 534.468 9 -9 6 -10 6727.04 495.655 7 -9 6 -10 7918.15 362.613 3 -9 6 10 7758.36 359.092 3 -9 6 11 19921.3 844.300 3 -9 -6 11 22712.5 898.638 10 -9 -6 -11 19358.7 868.577 12 -9 6 11 20800.9 856.528 4 -9 -6 12 8255.21 388.012 10 -9 6 12 7199.69 341.167 4 -9 -6 12 6948.72 570.266 5 -9 -6 -12 7031.06 351.846 12 9 6 -13 840.353 135.122 11 -9 -6 13 988.068 222.862 17 -9 6 13 851.292 103.814 4 -9 -6 13 1123.00 150.996 10 -9 -6 14 16958.5 736.578 17 -9 -6 14 16922.2 716.624 10 9 6 -14 15212.7 683.781 11 -9 -6 15 8235.04 427.231 17 -9 -6 15 8581.66 400.448 10 9 6 -15 7537.26 370.661 11 -9 -6 16 2496.10 228.028 17 -9 -6 16 2093.59 178.677 10 9 6 -16 2286.22 160.063 11 -9 -6 17 3087.79 226.161 17 -9 -6 17 2595.88 186.071 10 9 6 -17 2513.41 165.960 11 -9 -6 18 2036.06 184.340 17 -9 -6 18 1929.42 147.550 10 9 6 -18 1550.44 128.308 11 -9 -6 19 12626.1 546.992 10 -9 -6 20 7879.02 353.392 10 -9 7 0 65.2447 108.875 13 -9 -7 0 66.9879 133.416 14 -9 7 0-6.48729 141.830 3 -9 7 1 8369.30 399.024 13 -9 7 -1 8584.89 403.804 13 -9 -7 1 9101.23 422.349 14 -9 -7 -1 9545.64 422.964 14 -9 7 -1 7999.16 595.279 7 -9 7 -1 7918.81 415.527 3 -9 -7 -2 6126.40 320.410 14 -9 -7 2 6186.46 327.998 14 -9 7 -2 6374.03 508.843 7 -9 7 -2 5720.40 322.580 3 -9 7 -2 6212.68 310.569 13 -9 -7 -3 103.390 128.130 14 -9 7 -3 60.1068 227.037 7 -9 7 -3 74.2311 131.156 3 -9 7 3 149.527 137.236 3 -9 7 -3-23.4428 114.194 13 -9 -7 -4 1280.76 157.358 14 -9 7 -4 1454.64 291.125 7 -9 7 -4 1445.99 161.931 3 -9 7 4 1534.00 165.807 3 -9 7 -4 1357.76 148.086 13 -9 7 -5 292.864 230.960 7 -9 7 5 252.178 132.051 3 -9 7 -5 139.040 131.189 3 -9 -7 -5 460.830 133.140 14 -9 7 -5 256.947 122.904 13 -9 -7 6 1610.67 159.671 10 -9 7 -6 1856.50 305.423 7 -9 -7 -6 1551.38 175.536 12 -9 7 -6 1461.41 158.965 3 -9 7 6 1477.21 154.842 3 -9 -7 7 245.684 122.306 10 -9 7 -7 55.2475 220.169 7 -9 -7 -7 111.112 130.606 12 -9 7 -7 93.4565 113.816 3 -9 7 7 163.140 118.067 3 -9 7 -8 2569.76 324.348 7 -9 -7 -8 2475.02 194.797 12 -9 7 8 2812.65 179.845 3 -9 7 -8 2587.00 180.333 3 -9 -7 8 2879.09 200.584 10 -9 7 -9 3343.08 358.201 7 -9 -7 -9 4046.09 234.862 12 -9 7 -9 3562.66 210.585 3 -9 7 9 3611.54 210.661 3 -9 7 -10 857.469 219.484 7 -9 7 10 423.199 98.1420 3 -9 7 -10 492.688 102.391 3 -9 -7 10 601.097 135.500 10 -9 -7 -10 181.297 112.174 12 -9 -7 10 263.287 236.192 5 -9 -7 11 490.813 136.040 10 9 7 -11 183.555 121.196 11 -9 7 11 173.352 75.6980 3 9 7 -12-63.6559 126.591 11 -9 -7 12 32.2641 121.672 10 9 7 -13 407.965 124.617 11 -9 -7 13 796.237 205.202 17 -9 -7 13 676.860 136.522 10 9 7 -14 364.280 118.259 11 -9 -7 14 311.960 186.931 17 -9 -7 14 326.617 120.192 10 -9 -7 15 1741.05 207.195 17 -9 -7 15 1673.69 152.131 10 9 7 -15 1384.96 139.903 11 9 7 -16 716.109 112.501 11 -9 -7 16 911.581 172.552 17 -9 -7 16 814.158 121.282 10 9 7 -17-61.0466 93.6078 11 -9 -7 17 5.02746 140.182 17 -9 -7 17 77.7757 96.7256 10 -9 -7 18 4.74790 83.5418 10 9 7 -18-47.7808 81.4566 11 -9 -7 19 403.540 81.7574 10 -9 8 0 100.412 127.845 13 -9 8 0 143.938 145.215 3 -9 -8 0 99.8679 144.525 14 -9 8 -1 82503.7 3260.33 3 -9 -8 -1 80289.5 3257.62 14 -9 8 -1 77532.3 3467.31 7 -9 8 -1 81930.7 3254.09 13 -9 8 -2 8792.68 403.492 3 -9 -8 -2 7998.36 396.692 14 -9 8 -2 7628.37 389.667 13 -9 8 -2 7441.12 573.193 7 -9 8 -3 60682.8 2495.94 3 -9 8 3 63403.2 2500.21 3 -9 -8 -3 62437.2 2497.69 14 -9 8 -3 61065.1 2496.61 13 -9 8 -3 63514.0 2725.18 7 -9 8 -4 1175.48 159.554 3 -9 8 4 1203.25 158.920 3 -9 8 -4 1455.27 285.664 7 -9 -8 -4 1000.84 153.695 14 -9 8 -4 1415.83 158.342 13 -9 8 -5 40409.1 1698.25 3 -9 8 5 43705.8 1703.89 3 -9 8 -5 39806.2 1902.11 7 -9 -8 -5 40495.7 1861.53 9 -9 8 -5 41285.3 1706.72 13 -9 -8 -5 41641.4 1721.46 12 -9 -8 -5 42721.3 1705.63 14 -9 -8 -6 1370.71 159.255 14 -9 8 -6 1092.24 148.188 3 -9 8 6 1223.85 152.181 3 -9 -8 -6 1170.54 241.804 9 -9 8 -6 1064.25 271.814 7 -9 -8 -6 1474.00 165.949 12 -9 8 -6 1327.82 160.792 13 -9 8 7 39844.2 1506.94 3 -9 8 -7 36075.0 1500.41 3 -9 -8 -7 34565.6 1514.75 12 -9 -8 -7 37904.8 1514.46 14 -9 -8 -7 35526.6 1669.73 9 -9 8 -7 37685.0 1519.49 13 -9 8 -7 32039.3 1676.19 7 -9 8 -8 527.004 214.785 7 -9 8 -8 725.420 122.378 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9 1278.46 108.134 4 -14 4 9 1110.43 105.148 4 -14 -4 -9 1241.03 142.146 14 -14 -4 9 1012.84 166.346 17 -14 -4 -10 1760.85 150.322 14 -14 -4 10 1669.06 121.530 4 -14 4 10 1810.28 122.077 4 -14 4 11 350.027 76.3191 4 -14 -4 11 409.290 78.3788 4 -14 -4 -11 515.697 114.107 14 -14 -4 11 448.058 137.537 17 -14 -4 -12 3346.21 195.410 14 -14 -4 12 3057.16 205.263 17 -14 -4 12 3746.13 175.685 4 -14 -4 -13 3.54147 88.2862 14 -14 -4 13 85.0351 58.8555 4 -14 -4 13 222.811 108.513 17 -14 -5 0 231.630 78.6892 4 -14 -5 -1 22.6699 76.1931 4 -14 -5 1 7.59701 78.2614 4 -14 -5 -1 106.237 131.054 12 -14 -5 -1 35.0022 128.010 14 -14 -5 -2 5443.72 312.076 12 -14 -5 -2 5961.24 272.255 4 -14 -5 2 5827.13 271.023 4 -14 -5 -2 5726.25 305.685 14 -14 -5 3 2540.05 208.770 12 -14 -5 -3 2591.41 204.042 12 -14 -5 -3 2654.24 195.074 14 -14 -5 -3 2911.52 156.535 4 -14 -5 3 2613.18 155.543 4 -14 -5 4 556.318 88.5434 4 -14 -5 -4 749.683 135.429 14 -14 -5 4 739.995 145.514 12 -14 -5 -4 665.642 138.750 12 -14 -5 5 427.589 81.0938 4 -14 -5 -5 165.000 120.574 14 -14 -5 -5 168.756 121.821 12 -14 -5 5 313.880 136.138 12 -14 -5 -6 826.260 136.969 14 -14 -5 6 1001.52 94.3780 4 -14 -5 -6 931.574 140.428 12 -14 -5 6 763.458 141.483 12 -14 -5 7-66.1915 71.2297 4 -14 -5 -7 186.168 122.147 14 -14 -5 7 203.269 153.796 17 -14 -5 -7 11.6288 112.209 12 -14 -5 7 209.785 117.321 12 -14 -5 8 3364.02 208.073 12 -14 -5 -8 3590.32 209.017 14 -14 -5 8 3193.53 227.845 17 -14 -5 8 3480.31 176.542 4 -14 -5 -9 157.726 109.443 14 -14 -5 9 81.2446 144.675 17 -14 -5 9 123.546 65.1298 4 -14 -5 9 73.4298 96.0900 12 -14 -5 10 15.3985 61.0793 4 -14 -5 -10-4.32088 99.8742 14 -14 -5 10-182.448 135.377 17 -14 -5 -11 2886.83 173.768 14 -14 -5 11 3052.09 193.803 17 -14 -5 11 2825.23 142.651 4 -14 -5 -12 192.185 90.4229 14 -14 -5 12 238.387 114.315 17 -14 -6 0 4049.32 249.367 12 -14 -6 1 2710.10 204.240 12 -14 -6 -1 2633.69 197.329 12 -14 -6 -2 2719.25 189.738 12 -14 -6 -2 1939.54 170.927 14 -14 -6 -3-18.5037 120.607 12 -14 -6 -3-41.9194 118.671 14 -14 -6 -4 2031.87 175.751 12 -14 -6 -4 2620.87 178.242 14 -14 -6 -5 264.642 114.703 12 -14 -6 5 93.6510 123.318 12 -14 -6 -5 191.053 118.286 14 -14 -6 6 5829.72 297.057 12 -14 -6 -6 5572.54 280.964 14 -14 -6 -6 5337.07 283.669 12 -14 -6 -7 416.013 113.755 14 -14 -6 7 393.299 148.020 17 -14 -6 7 441.214 122.246 12 -14 -6 -7 211.515 106.813 12 -14 -6 8 3885.33 212.147 12 -14 -6 -8 3468.63 206.342 14 -14 -6 8 3567.52 229.084 17 -14 -6 -9 78.7096 97.1331 14 -14 -6 9-53.5226 130.165 17 -14 -6 9-85.1339 98.3199 12 -14 -6 -10 4798.57 234.539 14 -14 -6 10 4835.41 252.747 17 -14 -6 10 4630.80 234.950 12 -14 -7 0 43517.9 1767.41 12 -14 -7 -1 187.131 116.035 12 -14 -7 1 312.775 127.139 12 -14 -7 2 19632.8 851.738 12 -14 -7 -2 20617.6 849.856 12 -14 -7 -3 494.901 119.882 12 -14 -7 3 339.462 124.282 12 -14 -7 -4 13481.7 586.230 12 -14 -7 -5 466.653 108.216 12 -14 -7 -6 8207.18 375.226 14 -14 -7 6 7975.13 390.312 17 -14 -7 -6 8752.47 380.480 12 -14 -7 6 8449.26 389.178 12 -14 -7 -7 228.812 95.2955 14 -14 -7 7-17.1887 127.229 17 -14 -7 7 199.457 104.373 12 -14 -7 -8 11811.2 529.192 14 -14 -7 8 13746.2 545.484 12 -14 -8 0 1586.56 142.276 12 -14 -8 1 569.641 112.484 12 -14 -8 -1 241.863 106.186 12 -14 -8 -2 820.910 109.652 12 -14 -8 2 660.373 119.282 12 -14 -8 3 1796.28 146.783 12 -14 -8 -3 1625.87 135.062 12 -14 -8 -4 43.3643 88.3222 12 -14 -8 4 108.672 100.437 12 -15 0 0 42.3500 98.4089 4 -15 0 1-33.0117 98.0508 4 -15 0 -1-4.82870 105.405 14 -15 0 2 494.185 106.787 4 -15 0 -2 432.816 112.575 14 -15 0 3-32.3761 96.9501 4 -15 0 -3 42.4763 104.551 14 -15 0 4 122.876 94.9254 4 -15 0 -4 152.626 101.926 14 -15 0 5 115.997 93.6841 4 -15 0 -5 172.026 101.741 14 -15 0 6 1615.03 128.860 4 -15 0 -6 1484.34 133.967 14 -15 0 -7 114.522 96.5519 14 -15 0 7 16.8502 87.9750 4 -15 0 -8 426.419 98.3403 14 -15 0 8 381.692 96.0278 4 -15 0 -9 82.3997 86.9280 14 -15 0 9 92.2155 83.6272 4 -15 0 -10 218.978 85.1061 14 -15 0 10 255.326 84.9333 4 -15 0 -11 85.9708 74.2126 14 -15 0 11 47.8823 75.8120 4 -15 0 12 5343.05 220.020 4 -15 0 -12 3856.65 207.676 14 -15 -1 0-129.102 100.197 4 -15 -1 0-56.1740 116.039 12 -15 -1 -1 4217.18 254.946 14 -15 -1 1 4695.44 261.514 12 -15 -1 -1 4654.16 266.613 12 -15 -1 -2 72.5033 114.256 14 -15 -1 2 4.54694 98.0198 4 -15 -1 2 171.196 112.406 12 -15 -1 -2 57.8071 116.252 12 -15 -1 -3 4300.60 252.489 14 -15 -1 3 4415.29 253.060 12 -15 -1 4 4.43719 94.1429 4 -15 -1 -4 65.0785 112.265 14 -15 -1 5 32607.2 1226.10 4 -15 -1 -5 27443.9 1226.06 14 -15 -1 6 5649.61 267.258 4 -15 -1 -6 5222.24 274.903 14 -15 -1 7 6479.04 286.256 4 -15 -1 -7 5491.12 292.454 14 -15 -1 8 284.322 87.9352 4 -15 -1 -8 449.807 106.132 14 -15 -1 9 9931.08 394.000 4 -15 -1 -9 7866.32 392.893 14 -15 -1 -10 104.735 93.5670 14 -15 -1 10-3.52463 76.5482 4 -15 -1 -11 5633.23 294.418 14 -15 -1 11 7565.50 300.030 4 -15 -1 -12 206.077 75.1364 14 -15 -1 12 180.158 69.4913 4 -15 2 0 13.1293 90.0842 4 -15 -2 0-56.7286 94.8252 4 -15 -2 0 134.544 122.437 12 -15 -2 -1 19090.9 914.616 14 -15 2 1 23391.5 910.319 4 -15 -2 1 22329.8 908.210 4 -15 2 -1 23791.2 910.195 4 -15 -2 -1 23338.3 909.596 4 -15 -2 1 20292.6 923.304 12 -15 -2 -1 20494.2 925.746 12 -15 -2 -2 47.8672 120.959 14 -15 2 2 69.8703 90.2049 4 -15 -2 2 30.1530 90.6015 4 -15 -2 2 86.1555 115.062 12 -15 -2 -2-32.2056 122.016 12 -15 -2 -3 9942.32 486.109 14 -15 2 3 11480.9 477.790 4 -15 -2 3 11190.6 476.016 4 -15 -2 -3 10751.1 498.614 12 -15 -2 3 11019.2 494.606 12 -15 -2 -4 15.4177 117.765 14 -15 2 4-8.54608 87.1554 4 -15 -2 4 33.4491 88.9322 4 -15 -2 4 171.192 108.094 12 -15 2 5 12500.4 499.674 4 -15 -2 5 11625.6 496.146 4 -15 2 6 221.972 88.2667 4 -15 -2 6 199.656 85.6954 4 -15 -2 -6 98.0868 116.206 14 -15 2 7 15032.4 621.014 4 -15 -2 7 15316.5 620.369 4 -15 -2 -7 13679.5 628.990 14 -15 2 8 543.362 93.2373 4 -15 -2 8 448.346 85.9928 4 -15 -2 -8 361.547 107.146 14 -15 -2 9 17566.2 714.448 4 -15 2 9 18660.9 717.901 4 -15 -2 -10 46.0340 93.2275 14 -15 -2 10-3.26698 73.5720 4 -15 2 10-20.3955 78.1489 4 -15 -2 11 20681.9 799.623 4 -15 2 11 21115.3 801.861 4 -15 3 0-43.3426 80.2134 4 -15 -3 0-23.9167 82.1190 4 -15 -3 0 107.785 121.991 12 -15 -3 -1 690.832 133.976 14 -15 -3 -1 784.088 138.729 12 -15 -3 1 863.492 137.061 12 -15 3 1 701.235 97.0000 4 -15 -3 1 903.253 100.750 4 -15 3 -1 571.891 93.3412 4 -15 -3 -1 673.566 95.7747 4 -15 -3 -2 139.216 127.819 12 -15 -3 2 36.3702 115.840 12 -15 3 -2 19.2285 79.8227 4 -15 -3 -2-23.6755 79.2143 4 -15 3 2-19.7750 80.7206 4 -15 -3 2-27.6577 82.5515 4 -15 -3 3 2647.69 195.273 12 -15 3 3 3122.25 168.361 4 -15 -3 3 3090.17 170.476 4 -15 -3 4 1773.48 159.044 12 -15 3 4 1974.18 133.950 4 -15 -3 4 2025.52 133.766 4 -15 -3 -5 726.827 129.378 12 -15 -3 5 741.381 119.492 12 -15 3 5 605.937 91.1968 4 -15 -3 5 710.907 91.3945 4 -15 3 6 2605.62 152.585 4 -15 -3 6 2626.99 150.670 4 -15 3 7 1956.97 133.904 4 -15 -3 7 2270.15 135.171 4 -15 3 8 554.291 85.9782 4 -15 -3 8 508.034 81.9851 4 -15 -3 9 371.377 77.1633 4 -15 3 9 327.330 75.9663 4 -15 3 10 969.085 89.5471 4 -15 -3 10 1009.25 88.7310 4 -15 -3 11 86.4175 60.0565 4 -15 3 11 126.863 63.5462 4 -15 -4 0-104.771 78.8059 4 -15 4 0-108.232 75.7879 4 -15 -4 1 21873.1 909.278 4 -15 4 -1 22798.6 908.951 4 -15 -4 -1 22221.2 909.579 4 -15 4 1 23067.6 909.994 4 -15 -4 1 20719.5 932.500 12 -15 4 -2 3530.13 181.436 4 -15 -4 -2 3614.18 184.462 4 -15 4 2 3534.44 182.876 4 -15 -4 2 3587.32 184.947 4 -15 -4 2 3318.48 215.506 12 -15 -4 -3 7197.99 345.755 14 -15 4 -3 7191.76 317.379 4 -15 -4 -3 7252.42 321.242 4 -15 4 3 7418.51 320.394 4 -15 -4 3 6887.01 319.890 4 -15 -4 3 6982.93 347.573 12 -15 -4 -4 539.477 121.071 14 -15 4 -4 510.846 77.6328 4 -15 -4 -4 441.169 82.0198 4 -15 4 4 531.534 82.0795 4 -15 -4 4 493.267 83.5774 4 -15 -4 -4 469.516 121.072 12 -15 -4 4 592.425 119.933 12 -15 -4 -5 4321.52 239.607 14 -15 4 -5 4510.20 210.670 4 -15 4 5 4518.70 214.519 4 -15 -4 5 4588.81 215.825 4 -15 -4 -5 4288.10 243.856 12 -15 -4 5 4232.15 238.303 12 -15 -4 -6 85.6545 105.493 14 -15 4 6 95.3388 68.5494 4 -15 -4 6 49.2216 66.6728 4 -15 -4 6 116.897 96.0568 12 -15 -4 7 2947.38 153.885 4 -15 4 7 2970.36 154.267 4 -15 -4 -7 2875.89 180.392 14 -15 -4 -8 209.049 98.9428 14 -15 -4 8 264.506 66.6138 4 -15 -4 -9 5400.55 266.890 14 -15 -4 9 5683.33 249.264 4 -15 -4 -10 1662.22 124.387 14 -15 -4 10 1577.76 96.5111 4 -15 -5 0-41.2070 63.6444 4 -15 -5 1 10594.8 444.541 4 -15 -5 -1 10523.5 443.962 4 -15 -5 2 276.002 67.8421 4 -15 -5 -2 227.960 68.3446 4 -15 -5 -2 235.663 117.047 12 -15 -5 2 239.801 116.400 12 -15 -5 -3 17402.2 689.386 4 -15 -5 3 17224.5 689.151 4 -15 -5 3 15602.4 715.255 12 -15 -5 -3 16178.0 716.296 12 -15 -5 -4 284.315 114.039 14 -15 -5 -4 347.139 65.8729 4 -15 -5 4 318.763 65.8782 4 -15 -5 4 387.716 116.928 12 -15 -5 -4 554.833 119.412 12 -15 -5 -5 20109.9 788.248 4 -15 -5 5 19688.8 788.288 4 -15 -5 -5 19255.4 814.060 12 -15 -5 5 18595.1 811.656 12 -15 -5 -5 18650.4 809.051 14 -15 -5 -6 2726.86 171.514 14 -15 -5 -6 2535.59 134.726 4 -15 -5 6 2887.63 137.667 4 -15 -5 6 2624.24 178.413 17 -15 -5 6 2738.04 169.211 12 -15 -5 -7 15035.0 618.589 14 -15 -5 -7 15334.3 596.375 4 -15 -5 7 15090.1 596.600 4 -15 -5 7 14540.4 617.251 12 -15 -5 8 83.4299 105.573 17 -15 -5 -8-4.84829 42.3856 4 -15 -5 -8 99.3405 90.1450 14 -15 -6 0-19.6724 102.926 12 -15 -6 -1 3269.18 195.992 12 -15 -6 -2 349.619 109.849 12 -15 -6 3 306.781 117.651 17 -15 -6 -3 368.864 104.987 12 -15 -6 4 138.203 114.597 17 -15 -6 -4 104.713 89.9601 12 -15 -6 4 164.240 98.9758 12 -15 -6 5 192.881 109.924 17 -15 -6 5 326.430 95.5364 12 -15 -6 -5 231.017 93.3094 12 -16 0 0 21560.7 884.407 4 -16 0 -1-68.8378 83.9679 4 -16 0 1 40.1313 80.8805 4 -16 0 -2 35808.4 1440.42 4 -16 0 2 35690.2 1440.75 4 -16 0 -3-133.379 87.4253 4 -16 0 3 14.3199 82.6777 4 -16 0 -4 26724.1 1071.64 4 -16 0 4 26020.2 1071.93 4 -16 0 5-95.2043 82.9649 4 -16 0 6 31106.6 1255.30 4 -16 0 7 89.5597 71.5159 4 -16 0 8 45294.6 1808.77 4 -16 -1 0 3379.72 180.862 4 -16 -1 1 3221.50 172.384 4 -16 -1 -1 3125.62 171.650 4 -16 -1 -2 6787.12 305.749 4 -16 -1 2 6702.11 305.250 4 -16 -1 -3 596.334 88.4016 4 -16 -1 3 635.345 89.0870 4 -16 -1 -4 1951.20 127.133 4 -16 -1 4 1998.92 128.102 4 -16 -1 5 373.770 79.2983 4 -16 -1 -5 294.536 88.9429 14 -16 -1 6 1748.06 114.226 4 -16 -1 -6 1558.98 119.366 14 -16 -1 7 1587.78 101.515 4 -16 -1 -7 1059.80 103.382 14 -16 2 0 1540.49 108.344 4 -16 -2 0 1281.23 107.565 4 -16 -2 1 1129.64 102.444 4 -16 2 -1 1304.31 100.984 4 -16 -2 -1 1156.08 100.664 4 -16 2 1 1097.77 101.508 4 -16 2 -2 12300.8 517.392 4 -16 -2 -2 12343.5 518.314 4 -16 2 2 12351.1 518.725 4 -16 -2 2 12261.6 517.952 4 -16 2 -3 30.9929 69.6051 4 -16 -2 -3 22.5076 75.5063 4 -16 2 3 35.4677 73.4804 4 -16 -2 3 3.20562 73.4042 4 -16 2 -4 8020.88 337.471 4 -16 -2 -4 8214.83 340.369 4 -16 2 4 8359.15 341.007 4 -16 -2 4 7900.80 339.334 4 -16 2 -5 1011.09 87.4835 4 -16 2 5 1113.61 93.1939 4 -16 -2 5 1022.02 92.0890 4 -16 -2 -5 1041.80 89.7159 4 -16 -2 -5 790.999 107.574 14 -16 2 6 2381.40 131.108 4 -16 -2 6 2250.14 128.828 4 -16 2 -6 2352.35 126.545 4 -16 -2 7 1399.60 98.0198 4 -16 2 7 1432.71 99.0025 4 -16 -2 -7 1285.53 109.166 14 -16 -3 0 306.516 98.8404 12 -16 3 0 253.157 67.3023 4 -16 -3 0 315.857 70.9435 4 -16 -3 -1 139.540 93.3058 12 -16 -3 1-38.9166 91.9120 12 -16 3 1 42.4209 65.4546 4 -16 -3 1 25.9715 66.7873 4 -16 3 -1 102.905 63.5087 4 -16 -3 -1 86.5878 66.3087 4 -16 -3 2 6137.69 319.321 12 -16 3 -2 7445.04 307.497 4 -16 -3 -2 7145.74 307.817 4 -16 3 2 7089.97 307.130 4 -16 -3 2 6981.24 307.351 4 -16 -3 3 131.759 85.3565 12 -16 3 -3 55.4063 61.1259 4 -16 -3 -3 89.8085 66.0372 4 -16 3 3 196.645 66.5432 4 -16 -3 3 2.78530 64.6895 4 -16 3 -4 16671.4 678.522 4 -16 -3 -4 17067.1 681.091 4 -16 3 4 16802.1 680.295 4 -16 -3 4 15937.8 679.395 4 -16 3 -5 14.4938 57.1784 4 -16 -3 -5-43.4142 60.4465 4 -16 3 5 30.9132 59.5211 4 -16 -3 5 112.661 61.6758 4 -16 -3 -5 144.652 90.7331 14 -16 3 -6 8482.11 351.861 4 -16 3 6 8967.05 355.693 4 -16 -3 6 8656.63 354.509 4 -16 -3 -6 8482.50 353.586 4 -16 -4 0 7517.62 365.590 12 -16 -4 0 8525.75 347.066 4 -16 -4 1 905.739 109.140 12 -16 -4 -1 1115.55 115.574 12 -16 -4 1 1085.75 82.0365 4 -16 -4 -1 1012.01 81.6333 4 -16 -4 2 10431.7 490.700 12 -16 -4 2 11541.4 474.947 4 -16 -4 -2 12049.3 475.685 4 -16 -4 3 479.126 60.4807 4 -16 -4 -3 347.384 60.5741 4 -16 -4 3 572.516 91.5956 12 0 0 0 0.00 0.00 0 TITL exp_135_auto in Pbca REM Pbca (#61, found as Pcab in ba-c setting) CELL 1.54184 13.886251 12.726778 23.275178 90.0000 90.0000 90.0000 ZERR 9.00 0.000896 0.000884 0.001328 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H O F Si S I UNIT 153.00 180.00 27.00 27.00 9.00 9.00 9.00 SIZE 0.04 0.05 0.13 TREF HKLF 4 END ; _shelx_hkl_checksum 10287 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.458 _oxdiff_exptl_absorpt_empirical_full_min 0.609